PRODUCT OVERVIEW
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3 PRODUCT OVERVIEW About US GRABNER INSTRUMENTS, a member of the AMETEK Oil & Gas Business Unit, is considered one of the world s leading developers and manufacturers of automatic petroleum testing equipment. Founded in 1987 by Dr. Werner Grabner, the company became part of AMETEK in 2003. GRABNER INSTRUMENTS success is based on the development of portable, rugged and easy-to-operate analyzers, that help companies test their fuels and solvents in an accurate, fast, safe and economic way. Besides the classical downstream petroleum sector our instruments are dominating the field of automotive, aviation, marine and racing fuel testing. They are highly recommended for testing flavors, fragrances, food, petrochemicals and biofuels, plastics, adhesives, paints and varnishes. They are the preferred analyzers for research and development, for governmental agencies and for accredited laboratories. And they are being used in the mining, the chemical and the pharmaceutical industry, as well as in waste plants, incinerating plants and power plants, both in labs and in the field. AMETEK Oil & Gas is a group of companies specializing in meeting the unique measurement and instrumentation needs of the Oil & Gas Industry. Our portfolio of products offers solutions for the upstream, midstream and downstream segments of the industry. From instruments and equipment for production to petroleum product testing equipment for terminals and consumers, AMETEK Oil & Gas offers many technologies, systems and solutions that are unique to our member companies. We strive to provide the highest level of support and service our customers expect from a world-class manufacturer. Our offices and sales channels span the globe to offer our customers knowledgeable and responsive support through regional or local presence. AMETEK Oil & Gas is a division of AMETEK, Inc. AMETEK is a global leader in electronic instruments and electromechanical devices with colleagues at numerous manufacturing, sales and service locations in the U.S. and in many other countries around the world. AMETEK consists of two operating groups: Electronic Instruments and Electromechanical. Electronic Instruments is a leader in advanced instruments for the process, aerospace, power and industrial markets. Electromechanical is a differentiated supplier of electrical interconnects, precision motion control solutions, specialty metals, thermal management systems, and floor care and specialty motors.
4 About US Product Advantages Highest Precision. Grabner Instruments analyzers are known to be the most precise. They are optimizing customer products and profits. Fast Measurements. Measurements on a Grabner analyzer run faster. They are streamlining customers processes. Small. Light. Portable. The instruments are small and portable. Bring them to the source of sampling or to other laboratories. Highest Safety. Our methods are the safest. For our customers and our environment. Automatic Measurements. Automation reduces operator bias. For assured testing in the laboratory. Minimum sample. Our analyzers help to reduce waste. Because only a minimum sample is required. Robust. We use only robust material of superior quality. To make our instruments reliable working horses for daily testing.
5 VAPOR PRESSURE MINIVAP testers are worldwide market leader for vapor pressure testing in oil and pipeline companies and independent test laboratories, engineered for superior performance and unmatched precision. Gasoline, Aviation Fuels, Crude Oil, LPG, Solvents and Chemicals can be tested according to all major industry standards. MINIVAP analyzers are the only ASTM Round Robin tested reference analyzers for US EPA and CARB, with an installed base of more than 4000 analyzers. Vapor Pressure Automotive Industry The vapor pressure of Gasoline and LPG is measured to check conformance of motor fuels to summer and winter grade specifications and to prevent vapor lock. The vapor pressure at different temperatures is used to determine requirements for the development of motors, carburetors, fuel injection systems, gasoline pumps, tanks and fuels systems. It can be used to analyze, if newly developed motors are able to handle the requirements of future fuels at high temperatures. Aviation Industry The vapor pressure of AVGAS (ASTM D910 or Def Stan 91-90) is determined according to ASTM D5191 or D6378. It is typically lower than the vapor pressure of automotive fuels, to prevent vapor lock at reduced atmospheric pressure in higher altitude. Biofuels Ethanol blends develop nonlinear vapor pressure behaviour, once a critical amount of Ethanol is blended into gasoline. The vapor pressure and the T (V/L) of Ethanol blends is measured to confirm compliance with automotive fuel specifications. The analysis of Ethanol blends plays an important role for the development of new motors, like flex-fuel motor systems. Flavors, Fragrances, Food, Chemicals To ensure compliance with hazardous goods and transport regulations or for completing Material Safety Data Sheets, the absolute vapor pressure of chemicals has to be tested. The Triple Expansion Method is a static method, designed to measure the absolute vapor pressure of liquids. It can be used for measuring single- or multi-compound solvents showing either high or low volatility.
6 VAPOR PRESSURE Vapor Pressure Laboratory Inspection, Environmental In a laboratory, the vapor pressure of Gasoline, Crude Oil, LPG and solvents is tested to certify product compliance with volatility and air pollution regulations. The versatile MINIVAP testers perform according to all major industry standards, such as ASTM D6378, D6377, D6897, D5188, D5191, EN 13016, IP 394 and IP 409. Measurements can be done at various temperatures and Vapor/Liquid ratios. Military Gasoline and Jet Fuel vapor pressure is tested directly in the field. Our instruments are used for monitoring fuel quality in military storage tanks. Petroleum The petroleum industry analyzes the vapor pressure of Gasoline, Crude Oil, LPG and LNG to optimize product blending while ensuring that governmental regulations are being met. Applications may also include studies on vapor lock or the determination of the Bubble Point and the TVP, to protect facilities for fuel storage and transportation. Pharmaceutical Vapor pressure measurements help to evaluate the evaporation behaviour of compounds and agents, to determine storage and transportation requirements, to ensure pollution control and to define product specifications according to the latest ASTM, EN and IP standards. For research and development the vapor pressure versus temperature behavior (ASTM D5188) can be tested with the MINIVAP. Transportation and Storage Gasoline, Crude Oil and LPG vapor pressure is tested to allow proper and safe blending and to determine the product quality prior to transportation. Vapor Pressure is also critical to ensure proper and safe tank storage and to minimize outgassing. Determining the TVP or Bubble Point is extremely important to prevent pumping cavitation in pipelines. Testing the vapor pressure at a Vapor/Liquid ratio of 0.02/1 allows a perfect simulation of conditions in an oil-tanker.
7 Vapor Pressure Instruments Highest Precision Quick Turnaround No Product Give-Away No Operator Bias Minimum Waste G Gasoline, Gasohol Crude Oil Jet Fuels LPG Solvents Chemicals All Standard VP Methods Included Highest Accuracy: r/r = 0.3/0.7 kpa Only 1 ml Sample (excl. rinsing) 5 Minutes Measuring Time DVPE and T (V/L = 20) in One Run Sampling Pro Valve Design Shaker for Rapid Equilibrium Optional Crude Oil or LPG Package Maintenance Free Measuring Cell USB and LIMS Data Transfer USB Printing MINIVAP VPXpert Solvents Chemicals Modern Replacement of ASTM D2879 Isoteniscope Method Low Volatility Measurement up to 100 kpa Static Triple Expansion Method Sampling Pro Valve Design Fully Automated Measurement Unmatched Precision 1 ml Sample (excl. rinsing) Results in 5 Minutes MINIVAP VPXpert-L G Gasoline, Gasohol Crude Oil Jet Fuels Solvents Worldwide Standard Instrument Approved by US EPA and CARB No Vacuum Pump Required No Sample Preparation Optional 6 Position Autosampler Optional Crude Oil Package Portable Field Use with Vehicle Power Converter NSN 6630-01-410-7374 (VPS) MINIVAP VPS / VPSH Upgrade Your Instrument for Crude Oil Analysis 250 ml Floating Piston Cylinder Fixed Pressure Regulator Crude Oil Standard Inlet Tubings for 2000 and 7000 kpa Filling Pressure Tubing for Non-Pressurized Filling Filters for Particle Filtration Crude Oil Package
8 Vapor Pressure Specifications MINIVAP VPXpert Test Methods Temperature Range Temperature Stability Pressure Range Vapor/Liquid Ratio Precision ASTM D5188, 5191, 6377, 6378, 6897; EN 13016; IP 394, 409, 481; GOST 52340, JIS K2258-2, SHT 0769; ASTM D4953 and D323 equivalent 0-120 C (32-248 F) ±0.01 C (±0.02 F) 0-1000 kpa (0-145 psi) 0.02/1 to 100/1, adjustable per selected method 1 ml (2.2 ml per rinsing) Repeatability = ±0.3 kpa, Reproducibility = ±0.7 kpa MINIVAP VPXpert-L Test Methods Temperature Range Temperature Stability Pressure Range Vapor/Liquid Ratio Precision ASTM D5188, 5191, 6377, 6378; EN 13016; IP 394, 409, 481; GOST 52340, JIS K2258-2, SHT 0769; excellent correlation to ASTM D2879 0-120 C (32-248 F) ±0.01 C (±0.02 F) 0-100 kpa (0-15 psi) 0.02/1 to 100/1, adjustable per selected method 1 ml (2.2 ml per rinsing) Repeatability = ±0.1 kpa, Reproducibility: TBD MINIVAP VPS / VPSH Test Methods ASTM D5191, 6377, 6378 Temperature Range Temperature Stability Pressure Range Vapor/Liquid Ratio Precision VPS: 20-60 C (68-140 F) VPSH: 0-100 C (32-212 F) ±0.1 C (±0.2 F) 0-1000 kpa (0-145 psi) VPS: 4/1 VPSH: 0.02/1 to 4/1 1 ml (10 ml incl. rinsing) Repeatability = ±0.3 kpa, Reproducibility = ±0.7 kpa CRude Oil Package Test Method ASTM 6377 Pressure Handling 0-7000 kpa (0-1015 psi)
9 Vapor Pressure Instruments Highest Precision Quick Turnaround No Product Give-Away No Operator Bias Minimum Waste G Gasoline, Gasohol Jet Fuels Solvents Wide Range Single Point: T (V/L) = 20/1 Multi Point: T (V/L) = 4/1 to 100/1 No Rinsing Required No Cross Contamination Results in 5 Minutes Portable MINIVOL LVR LPG Full Automation Highest Accuracy for LPG Maximum Safety in the Lab No Vacuum Pump Fast and Easy to Use Portable and Rugged Results in 5 Minutes MINIVAP LPG G Gasoline, Gasohol Crude Oil Jet Fuels LPG ASTM Compliant, Direct VP Measurement RVPE, DVPE, TVP, T (V/L) = 20 Unmatched Accuracy in Process Up to 2 Sample Streams 7 Minutes Cycle Time Automatic Calibration Variable V/L Ratio Fast & Easy Maintenance Amortization Within Weeks MINIVAP ON-LINE Exchangeable Measuring Cell Measuring Cell Exchange in 1 Minute Fastened with 5 Quick Connectors Fully Configured, Ready to Run Interchangeable between Analyzers ON-LINE Service Unit For Local Calibration and Service Easy to Attach to Measuring Cell Works as Controller for the Cell Offline System Check Communication Protocol Check For Temperature and Pressure Calibration
10 Vapor Pressure Specifications MINIVOL LVR Test Method ASTM D5188, evacuated chamber Temperature Range 20-80 C (68-176 F) Temperature Stability ±0.1 C (±0.2 F) Pressure Range 0-1000 kpa (0-145 psi) Vapor/Liquid Ratio 4/1 to 100/1 15 ml Precision Repeatability = ±0.6 kpa, Reproducibility = ±0.9 kpa MINIVAP LPG Test Methods ASTM D6897; excellent correlation to ASTM D1267 Temperature Range 5-70 C ( 41-158 F) Temperature Stability ±0.1 C (±0.2 F) Pressure Range 0-2000 kpa (0-290 psi) Vapor/Liquid Ratio 1/9 to 9/1 3.3 ml (13 ml incl. rinsing) Precision better than ASTM D6897 and D1267 MINIVAP ON-LINE Test Methods ASTM D5188, 5191, 6377, 6378, 6897; EN 13016; IP 394, 409, 481; ASTM D323 and D4953 equivalent Temperature Range 20-60 C (68-140 F) Temperature Stability ±0.1 C (±0.2 F) Pressure Range Gasoline/Crude Oil: 0-1000 kpa (0-145 psi) LPG: 0-2000 kpa (0-290 psi) Vapor/Liquid Ratio 0.02/1 to 20/1 1 ml (10 ml incl. rinsing) Precision Repeatability = ±0.3 kpa, Reproducibility = ±0.7 kpa Power Supply 100/120/230/240 V AC, 50/60 Hz, 110W WxHxD; Weight 580 x 1060 x 260 mm; 50 kg
11 FlashPoint MINIFLASH is a uniquely designed flashpoint tester series that uses the continuously closed cup method to determine the flash point of petroleum products, liquids and solids with only 1 ml of sample. The Grabner method is the safest and most economic flashpoint method that also offers the highest repeatability and reproducibility, an excellent and ASTM proven correlation to the D93 Pensky-Martens method and delivers results equivalent to other closed cup standards. Flashpoint Automotive and Aviation Industry MINIFLASH testers are used for safe and fast flashpoint testing of Diesel and Aviation Turbine fuels, for the assessment of fuel contamination, and for the development and and quality control of motor oils. The analyzers measure according to ASTM D6450 and D7094, results are rated equivalent to the D93A Pensky Martens method and correlate well to Abel, TAG and small scale methods. Construction and Mining Flashpoint measurements help to monitor the quality of Diesel and lubricating oils. The MINIFLASH also includes a fuel dilution feature, which is used to verify fuel contamination into oil for heavy duty machinery. A portable flashpoint tester is a perfect testing tool for remote areas, that offer only a minimum of infrastructure. Companies like CATERPILLAR are using the MINIFLASH. Flavors and Fragrances, Chemicals MINIFLASH is the world wide market leader in the Flavors & Fragrances industry. Only 1-2 ml sample is required! Further applications include testing of solvents, paints, adhesives and other chemicals. The determination of the flashpoint is required to document compliance with transport regulations, for defining product specifications and to complete material safety data sheets. Energy In conventional and nuclear power plants, flashpoint tests are being used for analysing the quality of hydraulic and transformer oils.
12 FlashPoint Laboratory Inspection Flashpoint Our instruments are used for accurate flashpoint determination of petrochemicals, lube and used oils, solvents, paints and chemicals, according to the modern flashpoint standards ASTM D6450 and D7094, in excellent correlation to ASTM D93, D56, ISO 2719, ISO 3679 and ISO 3680 standards. D7094 is being considered as an alternative method for ASTM Diesel Fuel specifications. The MINIFLASH is approved by US D.O.T. for analysing class 3 flammable liquids for transportation in commerce. Lubricants, Greases The flashpoint of lubricants has to be tested to determine product specification and to verify compliance with transport regulations. For laboratories with a high throughput, that require testing of more than 20,000 samples per year, Grabner Instruments designed the 8-position sampler MINIFLASH FLAH. Military and Marine Fuels Military vessels navigating the oceans around the globe use the portable MINI- FLASH flashpoint tester to check the quality of their fuels and oils. The fuel dilution measurement method in the MINIFLASH was developed to test the level of fuel contamination in oil onboard Navy ships. This method can also be used for leak detection in lubricated bearings. Petroleum and Biofuels Strict safety regulations in refinery laboratories speak against using open flames near highly flammable liquids. The MINIFLASH is the safest flashpoint tester available, very user friendly, efficient and strong enough to last even in an offshore environment. It is used for testing Petrochemicals, Diesel, Lube and Used Oils, Biofuels, Blends and for analyzing oily waste water in upstream exploration. Waste For safe thermal disposal or for storage of flammable liquids, the flashpoint of liquid and solid waste, used oil, oily waste water and pharmaceutical waste water has to be analyzed. The versatile MINIFLASH is highly recommended by disposal plants and approved by RCRA.
13 Flashpoint Instruments Saves Test Costs Reduces Hazardous Waste Eliminates Safety Risks Increases Turnaround Reduces Cleaning Petroleum, Biofuels Chemicals Flavors & Fragrances Lube & Used Oils Paints & Varnishes Solids, Bitumen The Most Economic Flashpoint Test Method Includes all MINIFLASH Advantages plus - Equilibrium Flashpoint Methods - Automatic Ignition Cleaning - Full Remote Operation via Web Browser - Remote Diagnostics and Support - Direct USB, LAN, LIMS and PC Connection - Intuitive Menu Navigation on 8.4 Touch Screen - Microsoft Windows Software - Extended Temperature Range - Front USB Port for Convenient Data Transfer MINIFLASH FLP/H TOUCH Petroleum, Biofuels Chemicals Flavors & Fragrances Lube & Used Oils Paints & Varnishes Solids, Bitumen Advanced Standards ASTM D6450 and D7094 No Bias to ASTM D93A Best Repeatability and Reproducibility Highest Safety: No Open Flame Smallest Sample Size: 1 or 2 ml Fastest Turnaround: Peltier Cooling Portable, Easy to Clean and Durable Design Approved by US DOT, RCRA, NATO, US Navy NSN 6630-25-145-3256 (FLPH) MINIFLASH FLP/H/L D Diesel Jet Fuels Lube & Used Oils Marine Fuels ASTM D6450 and D7094 US Marine Aviation Fuel Acceptance Protocols US Navy-Specs Protocols (NAVIFLASH) Oil/Diesel Contamination Detection F-76 Fuel Dilution of 9250 Oil JP-5 Fuel Dilution of 9250 Oil JP-5, JP-8, Jet A1, Diesel and DF-2 Specs Ideal for Shipboard Testing NSN 6625-01-472-6783 (NAVIFLASH) NSN 6630-01-534-1774 (MARFLASH) MARFLASH / NAVIFLASH Petroleum, Biofuels Chemicals Flavors & Fragrances Lube & Used Oils Paints & Varnishes Solids, Bitumen Fully Integrated 8 Position Sampler Fast and Unattended Operation Up to 80 per Day Fast Cleaning Fast Thermoelectric Cooling Easy Programming Dialogue NSN 6630-25-146-0895 (FLAH) MINIFLASH FLA/H
14 Flashpoint Specifications MINIFLASH FLP/H TOUCH Test Methods Temperature Range Temperature Stability Sample Throughput ASTM D6450, D7094 excellent correlation to ASTM D93, D56, D3828, ISO 2719, 3679, 3680 FLP TOUCH: 0-200 C (32-392 F) FLPH TOUCH: 0-400 C (32-752 F); tab water cooling ±0.1 C (±0.2 F) 1 ml (ASTM D6450) 2 ml (ASTM D7094) up to 12 samples/h MINIFLASH FLP/H/L Test Methods ASTM D6450, D7094; excellent correlation to ASTM D93, D56, ISO 2719 Temperature Range Temperature Stability Sample Throughput FLP: 0 to 200 C (32 to 392 F) FLPH: 10 to 400 C (50 to 752 F) FLPL: -25 to 100 C (-13 to 212 F) ±0.1 C (±0.2 F) 1 ml (ASTM D6450) 2 ml (ASTM D7094) up to 12 samples/h MARFLASH / NAVIFLASH Test Methods Temperature Range Temperature Stability Sample Throughput ASTM D6450, D7094 MARFLASH: 0-200 C (32-392 F) NAVIFLASH: 0-400 C (32-752 F) ±0.1 C (±0.2 F) 1 ml (ASTM D6450) 2 ml (ASTM D7094) up to 12 samples/h MINIFLASH FLA/H Test Methods ASTM D6450, D7094; excellent correlation to ASTM D93, D56, ISO 2719 Temperature Range Temperature Stability Sample Throughput FLA: 0 to 200 C (32 to 392 F) FLAH: 10 to 400 C (50 to 752 F) ±0.1 C (±0.2 F) 1 ml (ASTM D6450) 2 ml (ASTM D7094) up to 12 samples/h
15 FUEL ANALYSIS The Grabner fuel analyzers are the ultimate solution for monitoring and optimizing refining and blending, to assess compliance with automotive fuel specifications, to control product contamination and adulteration, for fuel research and for motor development. The product line is headed by the MINISCAN IRXpert, the first portable FTIR multi-fuel analyzer for Gasoline, Diesel and Biofuel Blends, which combines the advantages of mid-ir and near-ir spectroscopy for utmost measurement accuracy. Automotive Industry The small sample volume of the Grabner analyzers allows quality checks on small amounts of residual fuels found in the fuel feed line, to clarify warranty issues. The analyzer is used for detecting fuel contamination or adulteration in fuels and to check compliance with Oxygen, Benzene and MMT specifications. Further applications include the analysis of alternative fuels for motor development and the product control in motor racing. FUEL ANALYSIS Aviation Industry FTIR measurements are a fast and cost effective way to check the quality of Aviation Turbine Fuels and Aviation Gasoline. Biofuels MINISCAN IRXpert and IROX are designed for the analysis of biofuels content in Gasoline and Diesel. Up to 25% Ethanol and up to 40% FAME in Diesel can be measured according to the international standards EN 14078 and ASTM D7806. Important fuel properties such as Octane and Cetane number, Density and Methanol content are determined within minutes. Construction and Mining Fuel Adulteration and Fuel Contamination is a widespread problem in the construction and in the mining business. The MINISCAN IRXpert Diesel analyzer allows portable contamination and adulteration analysis of Diesel fuels. Key fuel parameters such as Cetane Number, Cetane Index, Cetane Improver, Density, Aromatics, Distillation Properties and Biodiesel content are checked within minutes.
16 FUEL ANALYSIS Laboratory Inspection The Grabner fuel analyzers allow a comprehensive analysis on fuel quality. Octane Number, Octane Boosters, MMT, Benzene, Oxygenates, Aromatics, Cetane Number, Cetane Improver, Density, Distillation and Vapor Pressure are analyzed within minutes. Compliance with Oxygen, Benzene, Ethanol or FAME limits can be assessed easily, fuel contamination and adulteration is readily identified. Military FUEL ANALYSIS The portable and robust MINISCAN IRXpert and IROX fuel analyzers are an ideal solution for inspection of military stock fuels directly in the field. Petroleum The petroleum industry uses our quick and accurate fuel analyzers to adjust their blending process and to ensure that product quality is maintained. Compared to gas chromatography, FTIR instruments are a faster, more cost effective and more versatile way to test fuels in refineries, at terminals and in pipelines. Transportation and Storage Adulteration is a widespread problem, especially in developing countries. Fuel contamination on the other hand can be a costly issue for every pipeline operator. Portable fuel analyzers are perfectly suited for monitoring product quality throughout the distribution system. For product comparison, results can be transferred via web to the next sample point.
17 Fuel Analysis Instruments Monitor Quality Optimize Products Detect Contamination Save Laboratory Costs Save Test Time D G Biofuel Blends Diesel Gasoline, Gasohol Fuel Adulteration Portable Mid- and Near-FTIR Fuel Analyzer Laser- and Temperature Controlled System Superior Resolution: 2 cm-1 Self Learning Chemometrics 8.4 Full Color Touch Screen Full Network and LIMS Integration 70+ Fuel Parameters Analyzed: Oxygenates (ASTM D5845) Aromatics, PNA and Benzene (D6277, EN 238) Biodiesel (FAME) Content (EN 14078, D7806) Octane Booster and Cetane Improver Total Aromatics, Olefins, Saturates, Oxygen Octane Number: RON, MON, AKI Cetane Number, Cetane Index Distillation and Vapor Pressure Driveability, Vapor Lock and VOC Analysis Built-In Temperature Controlled Density MINISCAN IRXpert G Gasoline, Gasohol Fuel Adulteration Portable Mid-FTIR Spectrometer Complete Gasoline Analysis in 3 Minutes 9 Specific Oxygenates 14 Specific Aromatics and Benzene Total Aromatics, Oxygen, Olefins, Saturates Octane Number and AKI Octane Booster Determination Vapor Pressure and Distillation Properties Built-In Density Meter Fast and Easy On-Site Calibration Automatic Sampling Optional 6 Position Sampler Available IROX 2000 D Biofuel Blends Diesel Fuel Adulteration Portable Mid-FTIR spectrometer Complete Diesel Analysis in 3 Minutes Cetane Number and Cetane Index Cetane Improver Total Aromatics, Polynuclear Aromatics FAME (Biodiesel) in Diesel Distillation Properties Built-In Density Meter Fast and Easy On-Site Calibration Automatic Sampling Optional 6 Position Sampler Available IROX Diesel
18 Fuel analysis Specifications MINISCAN IRXpert Test Methods ASTM D5845, D6277, D7777, D7806; EN 238, EN 14078; ISO 15212 Property Prediction based on Temperature Stability Scanning Time ASTM D86, D323, D5191, D6378, D613, D2699, D2700; ISO 3405, 5163, 5164, 5165; EN 13016; ±0.1 C (±0.2 F) Less than 15 ml 80s (Multiple Scans) IROX 2000 Test Methods ASTM D5845, D6277, D7777; EN 238 Property Prediction based on ASTM D86, D5191, D6378, D2699, D2700 Temperature Stability ±0.1 C (±0.2 F) Less than 15 ml Measuring Time 3 min. IROX Diesel Test Methods ASTM D7777, D7806; EN 14078 Property Prediction based on ASTM D86, D613 Temperature Stability ±0.1 C (±0.2 F) Less than 15 ml Measuring Time 3 min.
19 DISTILLATION MINIDIS ADXpert is a portable, true atmospheric and automatic distillation analyzer, designed for laboratory and field use. Fast and highly precise distillation runs make the MINIDIS ADXpert a smart alternative to classical D86 testing, for biofuels testing and for determining the true boiling point of liquids. The instrument is specified for use of gasoline, jet fuel and diesel products (groups 0-4), biofuels, solvents, aromatics, organic liquids, chemicals and contaminated or blended samples, using a resolution twice as good as classical apparatus. A distillation run on light products takes just 15 minutes and requires only a 6 ml sample. Automotive Industry Our compact, fast and fully automatic distillation unit is an ideal tool for testing Gasoline, Diesel, Biofuels and Solvents for compliance with specifications and for contamination detection. In the MINIDIS ADXpert measurements are performed according to ASTM D7344 and correlate well to ASTM D86 and ISO 3405. Aviation Industry Distillation properties of Aviation Gasolines, Aviation Turbine Fuels and Synthetic Fuels are accurately determined by the MINIDIS ADXpert. DISTILLATION Biofuels The Grabner analyzer is used to verify distillation properties on high Ethanol blends and B100 Biodiesel. Small and portable, the instrument offers excellent precision and better repeatability on B100 than the classical ASTM D1160 vacuum distillation method as well as better repeatability on the T50 of Ethanol blends than the D86 method. Chemicals and Pharmaceuticals The MINIDIS ADXpert is a unique analyzer that measures both, the True Boiling Point or D86 / ISO3405 distillation properties, of Chemicals, Solvents and Organic Liquids. A complete analysis on initial boiling point, distillation curve and final boiling point of solvents is delivered within minutes.
20 DistilLation Construction and Mining Distillation properties are key in determining the quality of Diesel. Distillation yields important information to prevent the use of non-spec fuels and subsequently damage expensive machinery, used for mining and construction work. Because of its automatic heater regulation, the use of the MINIDIS ADXpert is not limited to Diesel: Difficult samples, like raffinates and mining solvents can also be distilled with this instrument. Laboratory Inspection The MINIDIS ADXpert is a versatile distillation unit for testing Gasoline, Naphta, Diesel, Jet Fuels, Biofuels, Chemicals, Solvents, Spirits, Narrow Boiling Products and Organic Liquids. Measurements are performed according to ASTM D7344, the instrument yields either ASTM D86 or True Boiling Point results. Measurements on B100 show excellent correlation and better repeatability, when compared to ASTM D1160. The portable instrument is ideal for mobile testing at the point of sale. Military DISTILLATION A compact, robust and reliable distillation unit is a must have for military personnel testing stock fuels directly in the field. The MINIDIS ADXpert guarantees highest safety, neither glassware nor a fire extinguisher is required for this distillation method. Petroleum Our portable analyzer is used to analyze distillation properties of petroleum products in the lab or in the field, to monitor product and pipeline specifications or to simulate fractional distillation. True Boiling Point or ASTM D86 distillation properties are determined automatically, pure Biodiesel is measured with the highest repeatability. Due to the nature of the instrument, the resolution is twice as good as in classical D86 apparatus. Transportation and Storage Manufacturers and distributors of petroleum products have to verify product quality and test compliance with transport regulations by means of distillation. A portable distillation analyzer can easily be moved to terminals, retail outlets, tank farms or pipeline sample points, that are scattered over a wide area.
21 Distillation Instrument Fast Results Small Sample Low Running Costs Unmatched Versatility No Manual Cleaning Highest Safety D G Biofuels Chemicals Diesel Fuel Contamination Gasoline, Gasohol Jet Fuels Solvents Most Versatile: Determines D7344 True Boiling Point Delivers D86 Results Tests B100 Biodiesel Tests Unknown Tests Refinery Residue Detects Dry Point Portable for Field Use Features: True Atmospheric Distillation 6 ml No Glassware 15 min. Distillation on Light Automatic Filling & Cleaning Automatic Temperature Optimization Automatic Final Heat Adjustment Best in Class Volume Detection Highest Safety Low on Consumables MINIDIS ADXpert MEASURING PRINCIPLE A disposable sample cup (2) is filled with anti bumping granules to avoid a boil-up effect of the sample. The cup is placed into the cup holder that contains the heating element (1). Finally the filling tube of the MINIDIS ADXpert is placed into the sample and the RUN button is pressed. The cup is automatically lifted and pressed against the stainless steel distillation column (3). By moving down the piston of the receiving system, a vacuum is generated and monitored for a few seconds to verify the precise positioning and tightness of the sample cup, ensuring no escape of flammable vapors. A 6 ml sample is transferred from the temperature controlled filling system to the sample cup (2) and heated with the low mass electric heating element (1). The temperature of the released vapor is measured with a NiCr/Ni thermocouple (4). Vapor passes through a condenser tube into a thermostated chamber (5), whose temperature is controlled by a Peltier element. The vapor condenses and the volume of the condensate is monitored using a combination of a stationary optical meniscus detector (6) and a receiver cell (7), whose volume can be changed by a piston driven by the high precision stepper motor. Once the final boiling point is reached, the sample cup is cooled down to a safe temperature, then removed and weighed using the built-in balance. Residue is determined from the weight difference before and after the distillation. 3 2 1 4 5 6 7
22 Distillation Specifications MINIDIS ADXpert Test Method ASTM D7344 Exellent Correlation to ASTM D86, D1160, D850, D1078; ISO 3405 Temperature Range 0 to 400 C (32 to 752 F) Temperature Stability ±0.1 C (±0.2 F) 6 ml Measuring Time 15 min. (light samples)
23 VISCOSITY MINIVIS testers are small and portable viscometers - an ideal solution for the fast and automatic measurement of the dynamic and kinematic viscosity of Newtonian liquids over a wide temperature range. MINITEST FFK automatically determines the flow-pressure properties of lubricating grease at low temperatures down to -60 C by means of the Kesternich test. The original and time-consuming method is now fully automated and the measuring range is extended far below the original one, resulting in a considerably improved precision. Automotive, Aviation, Ball Bearing The viscosity of fuels and lubricants is an important parameter for quality control, research and production. The Grabner viscometers deliver results wit excellent correlation to ASTM D445 and ISO 3104. The MINIVIS 445 is able to measure the Viscosity Index at 40 and 100 C in one run, and facilitates Aviation Turbine Fuels testing down to -20 C with water cooling. Biofuels Viscosity measurement of Biofuels is required for compliance with Biofuel specifications, and can also be used for monitoring the Biofuels production process. The MINIVIS testers quickly determine the Kinematic Viscosity of Biodiesel and blends, in excellent correlation to the ASTM D445 / ISO 3104 method. Chemicals, Food, Pharmaceuticals Falling Ball Micro-Viscometers are a simple, robust and accurate method for the determination of the dynamic viscosity, the kinematic viscosity and the Viscosity Index. Typically very little sample is required: The MINIVIS II operates with only 400 µl sample per test, MINIVIS 445 requires a slightly bigger volume in order to perform automatic rinsings. Our viscometers are designed for measuring clear and opaque liquids: as dark as heavy-oil, black ink and blood can be measured. VISCOSITY Construction and Mining The viscosity of lubricants is tested to ensure that correct, fresh lubricant is used when oil has to be refilled. A viscosity measurement serves as an indicator, whether used oil is still within specifications or has to be replaced. This is an important parameter for predictive maintenance programs for machinery, in order to prevent costly engine breakdowns.
24 VISCOSITY Energy For energy processing, the viscosity of insulating, hydraulic and transformer oils is a critical parameter. Oils are used for insulation and cooling of power generators and distribution systems, for tansformers, regulators, reactors, circuitbreakers, switchgear and other equipment.the viscosity of oils is important for facilitating energy processing conditions. It should be regularly checked by field maintenance. If the viscosity of oils is too high, transformers may encounter difficulties during a cold start. Laboratory Inspection In the laboratory, the kinematic and the dynamic viscosity as well as the Viscosity Index of fuels and chemicals is measured. MINIVIS results show excellent correlation to ASTM D445 and ISO 3104 measurements. Petroleum, Lubricants, Greases MINIVIS testers are a smart solution for monitoring viscosity on fuels and lubricants in order to determine product specifications or to ensure compliance with transport regulations. The MINITEST FFK is a unique tester for measuring the flow properties of lubricating greases according to Kesternich down to -60 C. No cryostate is required, the automated instrument reduces original test times by a factor of 10 and considerably improves test precision. No tubings, only the nozzle has to be cleaned! VISCOSITY Military MINIVIS testers facilitate viscosity analysis in the field - anywhere and at any time. For mobile use, only a 12V converter is required to connect the instrument to a vehicle battery. Robust and portable, the kinematic viscosity of Jet Fuels, Diesel and Lubricants can be analysed in a wide temperature range from -20 to +110 C. Paints, Coatings, Varnishes Falling Ball Micro Viscometers can be used to determine the viscosity of transparent paints, thinners, solvents, coatings and varnishes. Knowledge of proper filling, product hardening and rinsing solutions is required for testing these samples.
25 VISCOSITY Instruments Fast Throughput Minimal Waste Easy to Operate Easy to Clean D Biofuels Chemicals Diesel, Fuels Flavors & Fragrances Food Jet Fuels Lube & Used Oils Paints & Varnishes Pharmaceuticals Portable Rolling Ball Viscometer - Dynamic Viscosity - Kinematic Viscosity - Viscosity Index Wide Temperature Range: -20 to 110 C (w/ water cooling) Peltier Temperature Control Transparent and Opaque Integrated Automatic Density Meter Easy Cleaning NSN 6630-01-565-6697 MINIVIS 445 D Biofuels Chemicals Diesel, Fuels Flavors & Fragrances Food Jet Fuels Lube & Used Oils Paints & Varnishes Pharmaceuticals Portable Micro-Viscometer Fast Measurement Fully Automatic Easy Cleaning Wide Application Range Peltier Temperature Control Process Application with On-Line Insert MINIVIS II Greases Automatic Detection of Flow Pressure Fast 2-Stage-Peltier Cooling No Cryostate Needed Fit for Field Use Highest Accuracy Easy Handling Portable Design MINITEST FFK
26 Viscosity Specifications MINIVIS 445 Excellent Correlation to ASTM D445, D2270; ISO 12058; DIN 53015 Test Methods Density: ASTM D7777; ISO 15212 Temperature Range -20 to 110 C (-4 to 230 F) Temperature Resolution ±0.01 C (±0.02 F) Measuring Range 0.2-1500 mm2/s, cst (mpas) Measuring Time Diesel 3 min. Measuring Time VI 15 min. (Viscosity Index at 40 + 100 C) 25 ml Precision Repeatability: 0.3% @ 1 mpas, Reproducibility: 0.5% @ 1 mpas Repeatability Density 0.0005 g/cm3 MINIVIS ii Excellent Correlation to Temperature Range Temperature Resolution Measuring Range Measuring Time Diesel Precision ISO 12058; DIN 53015; ASTM D445 (w/ known density) 0 to 100 C (32 to 212 F) ±0.01 C (±0.02 F) 0.2-1500 mm2/s, cst (mpas) 3 min. 0.4 ml Repeatability: 0.3% @ 1 mpas, Reproducibility: 0.5% @ 1 mpas MINITEST FFK Test Method DIN 51805 (Kesternich Method) Temperature Range -60 to 30 C (-76 to +86 F) Tab Water Cooling for below -30 C (-22 F) Temperature Resolution ±0.1 C (±0.2 F) Pressure Range 0 to 200 kpa Pressure Resolution ±0.1 kpa Precision better than DIN 51805
27 WATER CONTENT MINIHYD coulometric Karl Fischer titrators have been specifically designed for the determination of water content in oils. Combining coulometry with the Karl Fischer method, MINIHYD KF titrators determine the water content of samples by measuring the amount of electrolysis current necessary to produce the required iodine. This is an absolute technique which does not require the calibration of reagents. The built-in battery and optional carry case provide the versatility required by the laboratory and also the ease of use and portability required by the field engineer. Bitumen, Asphalt Coulometric titration allows a cost efficient analysis of water content in bitumen emulsions. Automotive, Aviation, Lubricants The determination of water content is required in fuel and lubricating oil specifications. Total water content analysis of lubricating and used oils can be used for quality control. Controlling the water content of lubricating oils prevents premature corrosion, diminished lubrication and premature filter plugging as well as unwanted effects of water on additives. Biofuels Biofuel specifications require the determination of the total water content in Ethanol (e.g. ASTM E1064) and Biodiesel (e.g. ISO 12937). Removing water implies removing the support of bacterial growth in Biofuels and guarantees oxidation stability to prevent formating of deposits, which could damage the fuel injection system. Chemical Applications include the low level water determination (10 μg 200 mg absolute water content) in chemicals by coulometric Karl Fischer titration. Titration is also used for the measurement of adherent and enclosed moisture in basic chemicals. WATER CONTENT
28 WATER CONTENT Construction and Mining The measurement of the water content of Diesel and Lubricants used for heavy duty machinery helps to identify water contamination and is an important quality parameter. Energy Karl Fischer titration is the preferred method for the analysis of water in hydraulic, insulating, transformer and turbine oils, used in power plants, generators, transmitters and distributor of electrical energy using insulating oil. Water determination is also an important quality criterium for third party maintenance. Military Because it is portable, robust and easy to use, the MINIHYD is a good choice for analyzing the water content of military stock fuels and lubricants. Petroleum and Laboratory Inspection WATER CONTENT The water content of hydrocarbons is determined by coulometric Karl Fischer Titration according to ASTM D5133, D4928, D6304 and other international standards. Water content limits are used for specification for the purchase, sale or transfer of petroleum products, lubricating oils and additives. Water also has an economic impact: The amount of water in crude oils affects the cost of the oil at the well head, the pipeline and the refinery. Pharmaceutical Water content determination is of great importance in pharmaceutical analysis. Water has an essential influence on the quality, shelf life and release of active pharmaceutical agents in medications.
29 WATER CONTENT Instrument Easy To Use Fast, Precise, Robust No Calibration Required Premixed Chemicals D Biofuels Crude Oil Diesel Fuel Contamination Lube & Used Oils Simple, Fast and Precise Water Content Determination Easy One Button Operation ACE - Automatically Compensated Errors Low Drift Cell Design Results Manager Software & Statistics Built-In Printer Portable for Field Use Optional With 1 Year Reagents Kit MINIHYD MEASURING PRINCIPLE Karl Fischer titration is simply a means to measure water content of samples. Modern instruments, such as the MINIHYD, use the coulometric principle, whereby the water present in the sample is coulometrically titrated to a predefined end point at which there is a minute excess of free iodine present. Stoichiometrically, 1 mole of water will react with 1 mole of iodine, so that 1 milligram of water is equivalent to 10.71 coulombs of electricity. Combining the coulometric technique with Karl Fischer titration, MINIHYD titrators determine the water content of the sample by measuring the amount of electrolysis current necessary to produce the required iodine. This is an absolute technique which does not require calibration of the reagents. 1 2 3 I2+SO2+3C5H5N+H2O SO2 C5H5N +CH3OH O 2I - 2e Electrolysis current SO2 2C5H5N.HI+C5H5 N C5 H5 N I2 O SO4CH3 H Detector Signal Using the latest pulse current technology and the patented ACE control system (Patent No.GB2370641), the MINIHYD automatically selects the appropriate titration speed dependent upon the amount of water present in the sample. The titration speed is reduced as the end point is approached, and when the titration is completed the instrument prints out and displays the results. Start End Start End
30 WATER CONTENT Specifications MINIHYD Test Methods Moisture Range Measuring Range Measuring Time Precision Max. Titration Speed Max. Current Results Calculation ASTM D1533, D4928, D6304; IP 386, IP 438; IEC60814; ISO 10101-3, 10337, 12937 1 ppm to 100% water Possible: 1µg 200 mg Water Typical: 1µg 10 mg Water 0-30 min, user selectable 1 ml 10µg to 1mg Water = ± 3µg more than 1mg Water = ± 0.3% 2.24 mg/min. 400 ma w/w, w/k, v/sg, v/v Method Overview METHOD Category Pages ASTM D56 Flashpoint 12, 14 ASTM D86 Distillation 18, 19, 20, 21, 22 ASTM D93 Flashpoint 11, 12, 13, 14 ASTM D323 Vapor Pressure 6, 8, 10, 18 ASTM D445 Viscosity 23, 24, 26 ASTM D613 Fuel Analysis 18 ASTM D850 Distillation 22 ASTM D910 Fuel Analysis 5 ASTM D1078 Distillation 22 ASTM D1160 Distillation 19, 20, 22 ASTM D1267 Vapor Pressure 6, 10 ASTM D1533 Water Content 30 ASTM D2270 Viscosity 26 ASTM D2699 Fuel Analysis 18 ASTM D2700 Fuel Analysis 18 ASTM D2879 Vapor Pressure 7, 8 ASTM D3828 Flashpoint 14 ASTM D4928 Water Content 28, 30 ASTM D4953 Vapor Pressure 6, 8, 10 ASTM D5133 Water Content 28 ASTM D5188 Vapor Pressure 6, 8, 10 ASTM D5191 Vapor Pressure 5, 6, 8, 10, 18 ASTM D5845 Fuel Analysis 17, 18 ASTM D6277 Fuel Analysis 17, 18 ASTM D6304 Water Content 28, 30 ASTM D6377 Vapor Pressure 6, 8, 10 ASTM D6378 Vapor Pressure 5, 6, 8, 10, 18 ASTM D6450 Flashpoint 11, 12, 13, 14 ASTM D6897 Vapor Pressure 6, 8, 10 ASTM D7094 Flashpoint 11, 12, 13, 14 ASTM D7344 Distillation 19, 20, 21, 22 ASTM D7777 Fuel Analysis, Viscosity 18, 26 ASTM D7806 Fuel Analysis 15, 17, 18 ASTM E1064 Water Content 27 MEthod Category Pages EN 238 Fuel Analysis 17, 18 EN 13016 Vapor Pressure 8, 18 EN 14078 Fuel Analysis 15, 17, 18 ISO 2719 Flashpoint 12, 14 ISO 3104 Viscosity 23, 24 ISO 3405 Distillation 18, 19, 22 ISO 3679 Flashpoint 12, 14 ISO 3680 Flashpoint 12, 14 ISO 5163 Fuel Analysis 18 ISO 5164 Fuel Analysis 18 ISO 5165 Fuel Analysis 18 ISO 10101-3 Water Content 30 ISO 10337 Water Content 30 ISO 12058 Viscosity 26 ISO 12937 Water Content 27, 30 ISO 15212 Fuel Analysis, Viscosity 18, 26 Def.Stan 91-90 Vapor Pressure 5 IP 386 Water Content 30 IP 394 Vapor Pressure 6, 8 IP 409 Vapor Pressure 6, 8 IP 438 Water Content 30 IP 481 Vapor Pressure 8 GOST 52340 Vapor Pressure 8 JIS K2258 Vapor Pressure 8 SHT 0769 Vapor Pressure 8 DIN 53105 Viscosity 26 DIN 51805 Viscosity 26 IEC 60814 Water Content 30
31 MOBILE FUEL LAB Fully Equipped Modular Configuration Ready to Measure The MOBILE FUEL LAB is the ideal solution for fast and precise fuel quality checks in the field. Equipped with the portable, rugged and fully automated analyzers of Grabner Instruments, a detailed fuel analysis can be performed in 30 minutes by a single person directly on-site. D G Biofuels Crude Oil Diesel Fuel Contamination Gasoline, Gasohol Jet Fuels LPG Total Quality Control Directly at Site Complete Set of Instruments Complete Fuel Analysis in 30 min. Flexible Instrument Configuration Shock Proof Installation Instruments Secured for Transport Water and Power Supply Air Conditioned Anti-Skid Flooring PC Network Optional Sleeper Department MOBILE FUEL LAB Marine Fuels Total Quality Control on the move The Mobile Fuel Lab is the best example to highlight our competence: Get results, where you need them. Our instruments are made to sustain the demands on the road: they are small, robust and reliable. The Mobile Fuel Lab is built and equipped according to your requirements. Select a vehicle and choose the appropriate lab size. Available labs are: 3.8m standard lab 4.8m lab with sleeper compartment 7.0m Super Mobile Lab, including an office 13.5 m Articulate Truck, including a living area and fire extinguishing systems in accordance with local regulations, a generator, worktops, benches and cupboards. An optional fume-hood is available. Choose from our large selection of on-board instruments. All instruments are mounted on specially designed shock-absorbers. We are flexible when it comes to integrating your choice of printer, PC or GPS navigation system. All labs are equipped with air-conditioning, ventilation, ducted warm air heating system, a sink with cold and hot water, anti-skid flooring, fire detection MOBILE FUEL LAB
INNOVATION The driving force behind any instrument from Grabner Instruments is the customer. We achieve solutions for our customers needs. We are unrestrained by limits of current standards when trying to make things faster, easier and more accurate. Our ability to define state of the art technology is pushing our progress and gives us an edge over market competitors. And several new ASTM, ISO, GOST, and EN standards, worldwide patents and awards reflect that commitment. QUALITY We are providing customers with products of highest possible standard and quality. In 1993 Grabner Instruments was the first manufacturer of petroleum testing equipment to be certified according to ISO 9001. The excellence of our instruments results from many years of experience, the outstanding know-how of our engineers and the desire to create better solutions for you. CUSTOMER SATISFACTION You can count on our competence and flexibility. The lean structure of Grabner Instruments allows us to react fast and find flexible solutions for our customers. With well trained sales and service engineers in more than 50 countries we provide fast and effective service and short delivery times.