Biodiesel Testing Equipment

Biodiesel Testing Equipment

About Hoskin or over seventy years, Hoskin Scientific has been a supplier of Ftesting and monitoring instrumentation to the Canadian market. With offices in Vancouver, Burlington, and Montreal our customers are able to receive local sales and technical support in our three major departments. Our Environmental Department provides solutions for monitoring and sampling biological and chemical parameters in the environment. Our team of environmental sales representatives and diverse product range guarantee that you will find the right products for your application. Specific areas include: water quality, water quantity, soil moisture, plant science, weather stations, indoor air quality, aquatic sampling, and oceanography. Whatever the area of specialty, Hoskin Scientific s environmental department can equip you to collect the data you need for your project whether through a purchase or rental. Our Materials Testing Department offers testing equipment for soil, asphalt, petroleum, concrete and cement. Our qualified sales associates focus on providing a sophisticated range of testing equipment complying with the various test methods, ensuring that accurate and consistent test results are always obtained. Our Instrumentation Department focuses on a wide range of products including optical camera systems, transducers and transmitters, data acquisitions and loggers, signal conditioners and indicators, automation sensors and measurement systems. We have technical sales associates that are trained in various areas and willing to help you with your instrumentation requirements. 2

Table of Contents ASTM D93 - APM-8 Pensky-Martens Closed Cup Flash Point Tester............ 4 ASTM D130 - Solid Block Constant Temperature Baths.................... 4 ASTM D189 - ACR-6 Conradson Carbon Residue Tester................... 5 ASTM D445 - miniav Automatic Viscometer.......................... 5 ASTM D524 - Ramsbottom Carbon Residue Apparatus................... 6 ASTM D613 - Cetane Test Engine..................................6 ASTM 874 - Programmable Ash Furnaces............................ 7 ASTM 1160 - Vacuum Distillation Apparatus.......................... 7 ASTM D1796/D2709 - Oil Centrifuge................................8 ASTM D2274 - Liquid Oxidization Bath...............................8 ASTM 2500 DR-4 Automated Cloud Point Analyzer.............................. 9 DR-5 Cold Properties Analyzer....................................9 ASTM D2622 FX-700 Sulfur Analyzer........................................ 10 Sindie 2622 Sulfur Analyzer..................................... 10 ASTM D3828 Setaflash Series 3 ActiveCool Small Scale Flash Point Tester................ 11 MINIFLASH TOUCH Flashpoint Tester............................... 11 ASTM D4294 RX-360SH................................................. 12 ASTM D6584 BioDiesel GC System.......................................... 12 ASTM D4737 K45603 Automatic Distillation Analyzer 5000 Series...................... 13 ASTM D7501 Liquid Bath................................................ 13 Multi Filtration Tester......................................... 14 ASTM D664/D2896-D4739 Potentiometric Titrator........................................ 14 ASTM D6079 Fuel Lubricity Wear Test Machine.................................. 15 ASTM D6751 Oxidization Stability Bath....................................... 15 3

ASTM D93 Test Methods: ISO 2719, ASTM D93/IP34 Model APM-8 is the latest version of the automated Pensky- Martens Closed Cup (PMCC) flash point tester. The cup cover and the stirrer are permanently mounted on a swing-arm assembly, which allows an easy handling of the test cup cover. It makes free from handling the hot cup cover after completing a test. The swing arm assembly can be lifted up to vertical position for easier test cup cleaning. Easy Operation Protection Shield Cover All-in-one chassis design - compact, light-weight Range: ambient to 370 C Ergonomic colour-coordinated display for high visibility and intuitive switch operation Enhanced versatility including a USB port for optional flash memory or keyboard ASTM D130 Test Methods: ASTM D130, D1838, D4814 Annex and ISO 2160 Copper Strip Corrosion by Petroleum Solid Block Constant Temperature Baths Liquid Constant Temperature Baths Temperature Range 30 C to 180 C Temperature Stability of ± 0.2 C We offer a ride range of constant temperature test baths conforming to ASTM D130 copper corrosion test for fuel and related test methods. Liquid baths are offered with capacity for 4, 8, or 12 test bombs held in a vertical position. The same baths may also be used (with a change of support rack) for test tube only procedure accommodating 8, 16, or 24 test tubes. The ASTM D130 test is used at various temperatures for the following samples: Aviation gasoline, aviation turbine fuel, Natural gasoline, Diesel fuel and fuel oils, automotive gasoline, Cleaners and kerosene, Lubricating oils. 4

ASTM D189 Test Methods: ASTM D189, IP13, ISO 6615 The ACR-6 Conradson Carbon Residue Tester automates the evaporation and pyrolysis of the oil sample in preparation for determination of the Conradson value for percentage of carbon residue remaining, and is intended to provide some indication of relative coke-forming propensities. Optimum heater output for the prescribed burning process is programmed easily prior to the test. Ignition is determined by sheathed thermocouple. Easy Operation Process control by built-in micro processor Heating device is a Nichrome coil heater, side and bottom or Igniting device, pilot burner system Flame detector Temperature Monitoring System Easy To Clean Modular Design ASTM D445 Test Methods: ASTM D445, ISO 3104, IP 71, ASTM D446, ISO 3105 miniav Automatic Viscometer Convenient and Affordable Automated Testing 100-Fold Range Tubes for Kinematic Viscosities Between 0.3 and 6,000*mm²/s Selectable Temperature Range Between 15 and 100 C Compact Tabletop Unit - 10 W, and less than 21 in H With a single auto sampler provides automatic kinematic viscosity testing within parameters specified by ASTM D445/446 and ISO 3104/3105. The miniav measures flow rates within ±0.001 second by electronically timing the liquid meniscus as it moves between thermistor timing sensors. Bath temperature is controlled with accuracy better than ±0.01 C between 15 and 100, as required by ASTM D445/446. 5

ASTM D524 Test Methods: ASTM D524, D6074; IP 14; ISO 4262; FTM 791-5002; NFT 60-117 Determines the carbon residue left after evaporation and pyrolysis of a sample oil in the Ramsbottom furnace, providing an indication of the deposit forming tendencies of fuels and guidelines for the processing of refinery products. Microprocessor temperature control with digital display and over-temperature cut-off Thermostatically controlled coking furnace for five samples Cast-iron block type furnace reaches the standard test temperature of 550 C (1022 F) rapidly and controls with ±1 C stability Microprocessor temperature control has C/ F switchable digital setpoint and display Communications software (RS232, etc.), ramp-to-set and other enhanced features Heavily insulated stainless steel cabinet with three-layer refractory top provides excellent heat retention. ASTM D613 Test Method: ASTM D613 Switch in mid-test from automated to manual operation Improved data precision ISO traceability is simplified with full documentation Automation for laboratory and on-line engines Test result precision is improved Detailed reports are printed out at end of each test or on command The software automatically records all data (depending on degree of automation) from dual cetane meter, hand wheel position, injection timing, and ignition delay. Data management and data treatment including all calculations and data storage are done by the software in strict accordance with ASTM D613 method. The data is available for transfer to a LIMMS for storage or to a spread sheet for further analysis. Historic data is easily retrievable. 6

ASTM D874 Test Methods: ASTM D482, D874, D5184 Programmable Ash Furnaces determine the amount of ash in distillate and residual fuels, gas turbine fuels, crude oils, lubricating oils, waxes, and other petroleum products. 6 Complete Air Exchanges per Minute Maximum Temperature of 1100 C Digital PID Temperature Control Integrated Timer Incoming air preheated for enhanced temperature uniformity Solid state relays provide for low-noise operation Double walled housing for low external temperatures and stability Housing made of textured sheets of stainless steel Highly durable, high performance cured vacuum fiber module lining Heating from two sides by ceramic heating plates ASTM D1160 Test Method: ASTM D1160 The easy to use Vacuum Distillation Apparatus for the distillation of petroleum products is available in semi or fully automatic models. Fully-Automatic D1160 PC Control with Windows Operating System Automatic Generation of Reports Easily export data Automatic Cleaning Cycle Semi-Automatic D1160 Automatic Heat Control Vapour Temperature Display Pot Temperature Display Automatic Shutdown for high pot or vapour temperature 7

ASTM D1796/D2709 Test Methods: ASTM D91, D96, D893, D1796, D2273, D2711, D2709, D4007, D5546, API 2542, API 2548, BS 4385 Main Applications: Determination of water and sediment on mineral oils. Characterization of mineral oils. Heated up to 80ºC. 4 /8 places conical, pear, trace and finger tubes. tubes positioned in vertical at rest pre-heating program which warms the chamber before centrifugation microprocessor controlled, maintenance free TFT Touch colorful screen, easy use Lid lock system Rotor recognition Max. Speed3.000 RPM/ 2.425 x g. Duly isolated, avoid heat lost Accessories designed and produced specially for oily samples Different tubes can be run just replacing the adapters and/or rotors ASTM D2274 Test Methods: ASTM D943, D2274, D2893, D4310 Digital indicating temperature control maintains ±0.1 C stability Agitated liquid bath with 4 to 60 test positions Overall dimension 22 x 18 x 23 (55x 45x 58 cm) Temperature range of 40 to 120 C Supplied with eight flow meters Low level safety cut off switch Each test position has one float-in-tube flowmeter positioned in front. The oxygen flow rate is maintained at 3 ± 0.1 L/hr with a micro precision valve. An oxygen pressure regulator is optionally available. Temperature control is provided by a digital display PID controller providing stability of ± 0.2º C or better. In the event of primary controller failure the bath is protected by a secondary high limit controller. 8

ASTM D2500 Test Method: Fully Conforms to the Manual ASTM D2500 The dimensions of the glassware, the metal test jacket, position of probes, cooling profile, and other parameters are identical as specified by the manual method. The analyzer software confirms cloud point when the fiber optics detects reduction of the pulsing green light reflected from the bottom of the silvered test tube. The test cup (metal jacket) for cloud point, pour point, or CFPP is directly cooled by the refrigerant, thus replacing the middle step of first cooling the flammable alcohol and then pumping the cold alcohol to the test jacket. DR4 series coolers are available in 1 or 2 test positions with lowest temperature of either -34 or -70 C. No Cryostat required No Hazardous alcohol required Fully Automated Self Contained Test Methods: ASTM D97, D2500, D6371 The DR5 is a cold properties analyzer. A unique interchangeable cartridge system allows cloud, pour, and CFPP on the same machine. The DR5 is single position. There are three types of cartridges: cloud, pour, and CFPP. Each DR5 comes with a single cartridge. Upon ordering, please specify which cartridge type to include. Additional cartridges can be bought as accessories. The DR5 s state-of-the-art cooling system allows temperatures from -120 C to 60 C. It cools at a rate of 1 C in 5 seconds or less. It maintains temperature of +- 1 C. Only 11 inches wide High res tablet touch display Fully contained maintenance free refrigeration system View current test in real-time from PC, tablet, or phone via Wifi. Easily export test data to flash drive, web browser, or to in-house LIMS system 9

ASTM D2622 Test Methods: ASTM D2622, ISO 20884, JIS K2541-7 Model FX-700 determines total sulfur in ultra low sulfur (ULS) fuels using wavelength dispersive X-ray fluorescence (WDXRF) method to detect sulfur in oil content of a 3-4 ml sample. The FX-700 uses a gas-filled proportional counter to detect the presence of sulfur in quantities of as little as 1 ppm. The front panel display provides test status, sample name, raw count data, and sulfur content. Data from the last 50 tests are stored in RAM. The FX-700 includes a built-in thermal type printer and an RS- 232C 1 channel port for optional output to the user's Laboratory Information Management System (LIMS). Simple operation Stand alone unit Minimal utilities No external PC is required for operation Built-In Printer Test Methods: AASTM D2622, D7039, ISO 20884 The Sindie 2622 bench-top analyzer complies with ASTM D2622, D7039 and ISO 20884 methods, enabling complete flexibility in sulfur analysis. No compromises in detection, performance and reliability - the SINDIE 2622 analyzer is the ideal sulfur analytical solution from ultra low sulfur diesel and gasoline to heavy fuel oil and crudes. One analyzer three compliance solutions. LOD: 0.4 ppm at 300 s. Dynamic Range: 0.4 ppm to 10% Plug-it-in and measure: power is only utility. Touch Screen user interface. User programmable measurement time: 30-900 s. Two calibrations covers both gasoline and diesel matrices over full dynamic range: - 0.4 3000 ppm wt - 0.3 10% wt No conversion gasses, heating elements, quartz tubes or columns. 75 W air-cooled excitation tube. Robust polyamide window for easy cleaning. 10

ASTM D3828 Test Methods: ASTM D1655, ASTM D3278, ASTM D3828, ASTM D7236, ASTM E502, BIS IS 1448 Part 20, BS 3900 Part A13, BS 6664 Parts 3 & 4, BS EN 456, CHIPS Regulations, Classification of Dangerous Goods for Carriage: Viscous and Non-viscous Liquids, DEF STAN 91-91, EPA 1020 A & B, IP 303 (obs), IP 523, IP 524, IP 534, ISO 3679, ISO 3680, UN Class 3 Non-viscous Flammable Liquids The Setaflash Series 3 ActiveCool Small Scale Flash Point Tester has been designed to rapidly and efficiently carry out Flash/No Flash tests to determine the flash point of liquids and semi-solids in the 10 to 130 C (50 to 266 F) temperature range. Flash point test in less than 2 minutes Small sample size (2 or 4ml) Automatic flash detection Electronic peltier cooling Audible and on-screen prompts Portable operation C or F display Corrosion resistant cup insert Test Methods: ASTM D6450, D7094, ASTMD93/ISO 2719, ASTM D56, ISO 13736, IP 170, ISO 3679, ISO 3680 MINIFLASH TOUCH is a uniquely designed flash point tester for the determination of flashpoint s of liquids and solids, using the Grabner flash point detection method of measuring the instantaneous pressure increase inside the continuously closed chamber, triggered by an energy-controlled electric arc. Heating the test chamber from the top avoids condensation of high volatile compounds, significantly improving the test results. Its continuously closed cup design and small sample volume of only 1-2 ml offers maximum safety, avoids offensive fumes in the testing area and reduces sample waste. The fast thermoelectric cooling at the end of a test and the fast and easy handling of the instrument save expensive labour time. Advanced flashpoint methods Combustion Analysis Peltier Protection Technology Automatic ignition cleaning program Maximum safety 11

ASTM D4294 Test Methods: ASTM D4294-03, ISO 8754 RX-360SH determines total sulfur in petroleum products, such as gas oil, fuel oil, crude oil and naphtha, using energy dispersive X-ray fluorescence (EDXRF) method, which is an accurate, non destructive, economical and yet quick method prescribed in ISO 8754 and ASTM D4294-03. Digital pulse height analysis is automatically carried out at each measurement to adjust the system. Patented Diamond Parameter Method - wide range of samples of different C/H ratios with uncompromising precision. Ambient Temperature and Barometric Pressure Compensation Set certified calibration standards and start automatic calibration program Minimum numbers of membrane switches are located on the operation panel along with an LCD for easy dialogue type operation. Compact design unit with carrying handle and 2-way power source (100-240VAC*1 or 12VDC battery*2) allows such applications as spot-checking in the field. ASTM D6584 Test Method: ASTM 6584 The BioDiesel GC System is configured to perform ASTM 6584 (residual free and bound Glycerin in BioFuel). Analysis takes about 25 minutes and is simple enough for an untrained operator to perform in the lab or in the field. The included PeakSimple Data System displays the calibrated r sults directly without off-line calculations. This gas chromatograph satisfies all of the requirements of ASTM 6584 for a fraction of the cost of compet tive instruments and includes 4 hours of operator training and a 2 year warranty. 8610C or 310 GC chassis FID Detector On-column injector 15 meter wide-bore capillary column PeakSimple Data System Perfect for testing BioDiesel at low cost 12

ASTM D4737 Test Methods: ASTM D86, D285, D850, D1078, D4737; D189 Section 10; DIN 51751; ISO 3405; IP123; JIS J2254; NF M 07-002 The Koehler Automatic Distillation Analyzer is designed to perform optimal distillation analyses of gasolines, fuels, oils, solvents, aromatics, napthas, kerosenes, hydrocarbons, and other volatile products to ensure conformity to rigid quality control standards. Pt-100 RTD probe with automatic temperature calibration system ( C or F) Windows -based software package for PC control with LIMS export capabilities Automatic determination of initial boiling point (IBP), final boiling point (FBP), dry point and barometric and residue corrections Automatic temperature and volume calibration Programmable distillation rate (2-15mL/min) Ready for distillation groups 0-4 Networking for up to 32 units Powerful CFC-free cooling & heating system Receiver chamber heating system to 60 C Precision level follower system with optical meniscus detector ASTM D7501 Test Methods: ASTM D7501 (formerly ASTM D6751 Annex) Cold Soak Filtration Test (CSFT) In order to accommodate six (6) 500 ml jars, typically available refrigerated baths get wider and deeper as size is increased. The design is specific for this test method resulting in a smaller size and less than 5 gallons (20 L) bath medium. The insulated bath is cooled by one compressor. Temperature control is handled by a digital indicating controller. Liquid Bath from ambient to -30ºC, 6 positions Digital indicating temperature controller with +/- 0.1ºC stability Included accessories: rack, receiving flask, safety flask, ground wire, funnel and funnel base, six (6) 500 ml sample jars with lid Vacuum system: pump, regulator, gauge, stand 13

ASTM D7501 Test Methods: ASTM D2068; IP 387 (A, B); IP PM-EA; CEN N 403 The Multi Filtration Tester (MFT) fully conforms to the latest cold soak filterability test requirements for FAME and bio diesel to be used with the Seta Cold Soak Test Bath (91665-0) for IP PM-EA. A unique and versatile instrument designed to test the Filter Blocking Tendency (FBT) of diesel, biodiesel (B100 & B5/7/20/30), gas oil, gas turbine fuel and kerosene. Test parameters for IP 387 and ASTM D2068 are pre-programmed. FBT analysis is achieved by measuring the pressure differential across a disposable filter. Fuels which have a high FBT could potentially block filters in the distribution network or during use in a vehicle or power plant. Portable test for filterability/blocking tendency IP 387 and D2068 test parameters are pre-programmed Compact and easy to use Result in less than 15 mins Interface for PC or Printer ASTM D664-D2896-D4739 Test Methods: ASTM D664, D2896, D4739 Total Acid Number and Total Base Number Performs ph, acid/base, complexometric, redox, non-aqueous titrations & ISE measurements Determines TAN/TBN in oils and p and m alkalinity Optional extra buret available. Note: Pump still common Optional impact printer or thermal printer Linked methods are available - up to three (3) per titration One-touch calculations - including statistics package Over thirty (30) files of built-in method memory Built-in memory of up to 50 results or via external computer link. Balance and computer serial port interfaces for ISO documentation. PC Software no extra cost 14

ASTM D6079 Test Methods: ASTM D6079; ISO 12156 The two-station Fuel Lubricity Wear Test Machine incorporates two test positions with heater pads and mounting arrangements for fuel lubricity test specimens. Load is applied manually by means of dead weights directly to the fixed ball specimen carrier by means of a loading yoke. Machine controls are limited to speed control of the drive motor to give the required frequency, temperature control of the specimen bath and test duration. Test data is limited to post test wear scar measurement only and no facilities are provided for friction force measurement. The electro-mechanical drive is used to achieve a wide range of frequencies, and the 1 mm stroke is generated with a cam. This ensures that the amplitude remains constant as friction forces vary in the contact. ASTM D6751 Test Method: EN-14112, ASTM D6751, ISO 6886 The oxidation stability baths conform to the requirements of EN-14122 test method, incorporated in ASTM D6751 specifications for B100 fatty acid methyl esters (FAME) for biodiesel blending. They employ an aluminum block configured to fit the specified test tube holding 3.0 gm of FAME (fatty acid methyl esters). When the sample reaches test temperature of 110 C filtered, dry air is sparged at 10 ± 1L/hr. to each test specimen. Multiple models available Automated operation Windows PC Data Acquisition Software Operating temperature from 40 to 150 C Temperature stability of ±0.1 C 15

Hoskin Scientific Limited has been supplying testing and monitoring instruments since 1946. Although our range is broad, we focus on three major markets including: Geotechnical & Materials Testing Environmental Monitoring Test & Measurement Instrumentation Hoskin Scientific operates out of three offices within Canada: Hoskin - Vancouver 3735 Myrtle Street Burnaby, BC V5C 4E7 T: (604) 872-7894 F: (604) 872-0281 salesv@hoskin.ca Hoskin - Burlington 4210 Morris Drive Burlington, ON L7L 5L6 T: (905) 333-5510 F: (905) 333-4976 salesb@hoskin.ca Hoskin - Montréal 300 Rue Stinson Saint-Laurent, QC H4N 2E7 T: (514) 735-5267 F: (514) 735-3454 salesm@hoskin.ca