EESTI AKREDITEERIMISKESKUS

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Leht 1(7) EESTI AKREDITEERIMISKESKUS LISA OÜ TT Labor akrediteerimistunnistusele nr. L063 ANNEX to accreditation certificate L063 of OÜ TT Labor 1. Akrediteerimisulatus on : Accreditation scope is : 1. te koguste määramine/arvutamine s quantity measurement and calculation 2. te sügavuste mõõtmine statsionaarsetes mahutites Gauging of petroleum product in tanks 3. te proovivõtmine Sampling of petroleum products 4. te temperatuuri mõõtmine elektroonilise termomeetriga Static temperature determination using portable electronic thermometers 5. te koguste mõõtmine raudtee mahutites Gauging of petroleum products in tank cars Koguse mõõtmine Measurement of quantity of products API MPMS Chapter 12.1.1. Calculation of Static Petroleum Quantities API MPMS Ch.3 - Tank Gauging. Sec.1A-Standard Practice for the Manual. Gauging of Petroleum and Petroleum Product API MPMS Ch.8 Sampling Sec.1 - Manual Sampling of Petroleum and Petroleum Products ISO 3170 Petroleum liquides-manual sampling D 4057 Petroleum and petroleum products. Manual sampling. API MPMS Ch.7 Temperature Determination. Section 3 Static Temperature Determination Using Portable Electronic Thermometers Инструктивные указания по определению веса наливных грузов в цистернах МПС РФ, 2003 Tables of calibration tank wagons *Mõõtevõime *Measurement capability U = 0,5 % (k=2) mõõtetulemusest (0,2 25 ) m U = 3 mm (k=2) (-20 35) o C U = 0,3 o C (k=2) U = 0,7 % (k=2) mõõtetulemusest/ from measurement result

Leht 2(7) 6. Tihedus Density 7. Oktaaniarv mootorimeetodil, MON Motor Octane Number of Spark-Ignition Engine Fuel 8. Oktaaniarv uurimismeetodil, RON Research Octane Number of Spark- Ignition Engine Fuel 9. Väävlisisalduse määramine UV Fluerescents meetodil Determination of sulfur content of automotive fuels UV fluorescence method 10. Leekpunkt Pensky-Martensi suletud testril Flash Point by Pensky-Martens Closed Tester 11. Tsetaaniindeks Calculated Cetane Index by Four Variable Equation Vedelkütuste katsetused Measurement of parametres of petroleum products D 1298 EN ISO 3675 Autobensiin, diislikütus, kg/m 3 700 900 D 4052 EN ISO 12185 kerge kütteõli kg/m 3 600 1200 EN ISO 5163 D 2700 Autobensiin Oktaaniarv EN ISO 5164 D 2699 Autobensiin Oktaaniarv EN ISO 20846 D 93 EN ISO 2719 EN ISO 4264 Diislikütus, autobensiin, kerge kütteõli Kerge kütteõli, petrool, diislikütus Diislikütus mg/kg 70 100 76 100 1 60 60 200 o C 20 150 Indeks

Leht 3(7) 12. Filtreeritavuspunkt Cold Filter Plugging Point 13. Fraktsioonkoostis Distillation characteristics EN 116 IP 309 D 86 EVS-EN ISO 3405 EN ISO 3405 Diislikütus, kerge kütteõli Autobensiin (manual) o C, IBP 10 30 90 o C -35 15 (0 400) ºC (20 70) ºC (35 95) ºC (65 220) ºC (110 245) ºC Diislikütus, kerge kütteõli (automaat) FBP o C, IBP 10 50 90 95 FBP (135 260) ºC (145 220) ºC (160 265) ºC (170 295) ºC (180 340) ºC (260 340) ºC (195 365) ºC (E70 E180) ºC (R200 R300) ºC diesel Autobensiin (automaat) o C, IBP 10 30 90 FBP (0 400) ºC (20 70) ºC (35 95) ºC (65 220)ºC (110 245) ºC (135 260)ºC

Leht 4(7) 14. Auruluku indeks (10RVP + 7E70) Factor (10RVP + 7E70) TT-M34:11.2011 Autobensiin 15. Induktsiooniperiood Oxidation Stability of Gasoline D 525 EN ISO 7536 Autobensiin min <480 16. Korrosiivsus vaskplaadikatse Detection of Copper Corrosion from Petroleum Products by the Copper Strip Tarnish Test 17. Kinemaatiline viskoossus Kinematic Viscosity of Transparent and Opaque Liquids D 130 EN ISO 2160 Autobensiin, diislikütus D 445 EN ISO 3104 Kerge ja raske kütteõli, diislikütus, masuut mm²/s 1 4 1 200

Leht 5(7) 18. Oksüdatsiooniline stabiilsus Oxidation Stability 19. 10 % jäägi koksiarv Conradson Carbon Residue on 10% distillation 20. Tuhasus Ash from Petroleum Products 21. Seotud vesi Determination of Water. Coulometric K. Fischer tetration method 22. Tahked osised Determination of contamination in middle distillates Tahked osised Determination of sediment extraction method 23. Vaba vesi Free water 24. Alumine ja eripõlemissoojus Estimation of Net and Gross Heat of Combustion of Burner and Diesel Fuels 25. Hägustumispunkt Cloud Point of s D 2274 EN ISO 12205 Diislikütus D 189 EN ISO 10370 Diislikütus, kerge kütteõli D 482 EN ISO 6245 Kerge ja raske kütteõli, petrool, diislikütus EN ISO 12937 Diislikütus, kerge kütteõli, petrool D 473 EN 12662 ISO 3735 Diislikütus kerge kütteõli, petrool ISO 3733 Diislikütus, kerge kütteõli, raske kütteõli, masuut D 4868 Arvutuslik Kerge ja raske kütteõli, masuut D 2500 EN 23015 ISO 3015 Diislikütus, kerge ja raske kütteõli g/m 3 0 5 5 10 10 20 20 55 massi % massi % 0,1 30 0,001 0,079 0,080 0,180 mg/kg 30 1000 mg/kg massi % 0 50 0,01 0,04 0,03 25 MJ/kg 0 100 C -38 50

Leht 6(7) 26. Määrimisomaduste hindamine HFRR seadmega Assessment of lubricity using the high-frequency reciprocating ring (HFRR) 27. Polüaromaatsete süsivesinike määranine Determination of aromatic hydrocarbon types in middle distillates HPLC metod with refractive index detection 28. Erimärgistutatud vedelkütuse kindlakstegemine Determination of Solvent Yellow 124 Automate Red NR Automate Blue 8GHF 29. Küllastunud aururõhu määramine Vapor Pressure of Petroleum D 5191 ISO 12156-1 Diislikütus, petrooleum, kerge kütteõli μm 300 500 EN 12916 Diislikütus massi % Määrus nr 194 08.07.2003 Diislikütus, kerge kütteõli mg/l MAH 4 40 DAH 0,5 20 T+AH 0 6 POLY-AH 0,5 26 TAH 4 65 0,5 20 EVS EN 13016-1 Bensiin kpa 9,0 150 Products *mõõtevõime on väljendatud laiendmääramatusena U (k=2) ja demonstreerib labori mõõtevõimet, mida ta võib mõõtemetoodikas määratletud tingimustel mõõtmistel saavutada *measurement capability is expressed as the expanded uncertainty U (k=2) and represents laboratory s measurement capability which is achieved in routine measurements carried out according to the measurement method

2. Katsetamist teostav struktuuriüksus: TT Labor OÜ Part of legal entity that provides testing: Aadress: Kärkna, Tartu vald, Tartumaa. Address: Kärkna, Tartu vald, Tartumaa. Leht 7(7) 3. Labor on akrediteeritud standardi EVS-EN ISO/IEC 17025:2006 nõuete suhtes Laboratory is accredited against the requirements of standard EVS-EN ISO/IEC 17025:2006 Märkus: käesolev lisa asendab 2.09.2016 välja antud lisa seoses uushindamisega. This annex replaces the annex issued on 2.09.2016 due to the reaccreditation. Kristiina Saarniit EAK juhataja Director of EAK Kalju Anni Peaassessor Lead Assessor Tallinn, 28.11.2016.