Product data sheet VAPODEST 50s / 50s carousel

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VAPODEST 50S / 50S CAROUSEL - Systems in comparison Standard configuration VAP50s VAP50s carousel Automatic addition H 3 BO 3 Automatic addition H 2 O Automatic addition NaOH Programmable reaction time Programmable distillation time Variable steam power 30-100 % Automatic suction of sample waste Automatic suction of the receiver Selection of language Optical and acoustical error messages Main programs any any Stand-by-Function Protection door with safety switch Automatic check of chemical reservoir Kjeldahl digestion tubes can be used 1) Kjeldahl-flasks can be used 1) - Automatic titration Micro dosing pump for titration RS 485 interface USB-interface Connection for scale Result print out Autosampler (carousel) - = Standard configuration 1) = see digestion tubes and Kjeldahl-flasks on page 3 Set of storage tanks - C. Gerhardt GmbH & Co. KG www.gerhardt.de Page 1

Order informations VAPODEST SCOPE OF DELIVERY Typ VAP 50s VAP 50s carousel Distillation system 1 x 1 x Autosampler (carousel) - 1 x KJELDATHERM digestion tube 1 x depending on carousel 20 x, 16 x or 12 x ph-electrode 1 x 1 x Buffer solution ph7 1 x 1 x Buffer solution ph4 1 x 1 x KCL-solution 1 x 1 x CD with VAPODEST Manager 1 x 1 x PC connection set 1 x 1 x Computer: Personal computer and printer are not included the delivery. Operating system: Windows XP, Vista, Windows 7, 1 x USB-interface Tubing set 1 x 1 x TECHNICAL DATA Type VAP 50s VAP 50s carousel Cooling water consumption [l/min] ca. 5 ca. 5 Distillation time [min] 2-4 2-4 Recovery rate [%] > 99,5 > 99,5 Reproducibility [%] +/- 1 +/- 1 Detection limit N [mg] 0,1 0,1 Rated voltage [VAC] 230 230 Frequency [Hz] 50 50 Rated power input [W] 1600 1830 Weight [kg] ca. 37 198 Dimensions W / D / H [mm] 440 / 340 / 690 1010 1) / 670 / 1655 1) 1290 mm with board attached on the side for monitor or printer ORDER INFORMATIONS 12-0040 VAP50s VAPODEST 50s, Distillation system, Version Standard, especially for the Kjeldahl determination 12-0470 VAP50s VAPODEST 50s, Distillation system, Version acid resistant, Equipped with acid resistant pumps 1) 12-0048 VAP50s OT VAPODEST 50s OT, Distillation system, identical to 12-0040, prepared for a possible upgrade to a VAPODEST 50s carousel at a later time 12-0050 VAP50s C VAPODEST 50s carousel, distillation system complete with carousel for 20 x 250/300 ml tubes 12-0051 VAP50s C VAPODEST 50s carousel, distillation system complete with carousel for 16 x 400 ml tubes 12-0052 VAP50s C VAPODEST 50s carousel, distillation system complete with carousel for 12 x 800 ml tubes 12-0053 VAP50s C VAPODEST 50s carousel, distillation system complete with carousel for 16 x BS 400 ml tubes Special voltages on request 1) special for dosing of phosphoric acid max. 85 % and hydrochloric acid max. 5 % - more acids on request Page 2 C. Gerhardt GmbH & Co. KG www.gerhardt.de

Order information accessories and consumables CONSUMABLES AND ACCESSORIES Make sure to use only original C. Gerhardt spare parts in order to obtain the best possible results. These parts have been tested thoroughly for the operation with VAPODEST in the C. Gerhardt application lab. KJELDAHL-DIGESTION TUBES AND KJELDAHL-FLASKS Depending on sample type and sample quantity VAPODEST can use a lot of Kjeldahl-digestion tubes as well as Kjeldahl-flasks. All tubes are made of high standard Duran material. 12-0301 KTG KJELDATHERM -digestion tube, macro 250/300 ml - 10 pcs 12-0306 KTG/E KJELDATHERM -digestion tube, macro 250/300 ml, with constriction + calibrated at 250 ml 12-0308 BS-400 KJELDATHERM -digestion tube, 400 ml, diminished 12-0310 KDD400 Jumbo-digestion tube 400 ml - 4 pcs 12-0311 KDD800 Jumbo-digestion tube 800 ml - 4 pcs 12-0243 KDD1200 1) Jumbo-digestion tube 1.200 ml 12-0304 KMT 1) KJELDATHERM -digestion glas, micro 100 ml - 10 pcs 12-0305 KMT/E 1) KJELDATHERM -digestion glas, micro 100 ml with constriction + calibrated at 100 ml 12-0307 KMT 1) KJELDATHERM -Glas, mikro 100 ml, calibrated at 100 ml + 75 ml 12-0312 KD250 1) Kjeldahl-flask 250 ml, with enlarged neck 12-0313 KD500 1) Kjeldahl-flask 500 ml, with enlarged neck, 4 pcs 12-0314 KD750 1) Kjeldahl-flask 750 ml, with enlarged neck, 4 pcs 1) VAPODEST 50s carousel only possible for single determination with adapter 12-0301 12-0306 12-0308 12-0310 12-0311 12-0243 12-0304 12-0305 12-0307 12-0312 12-0313 12-0314 C. Gerhardt GmbH & Co. KG www.gerhardt.de Page 3

Order information accessories and consumables ph-combined electrode 12-0555 ET-KCL ph-combined electrode KCL, require regularly filling with KCL 12-0355 ET-GEL ph-combined electrode gel electrolyte, maintenance free KCL and Buffer solution 1000178 Electrolyte solution KCL 1000176 Buffer solution ph 4 1000177 Buffer solution ph 7 Tank level control Illustration Position in tank 1009310 NIV50 Universal level control set for 3 chemical tanks, 1 sample waste tank and and 1 titration tank, consisting of: - 2 x Universal level control for chemicals, no. 1005098-1 x Universal level control for H 3 BO 3, no. 1005276-1 x Universal level control for sample waste, no. 1005721-1 x Storage tank 5 L for titration acid, incl. level control Storage tanks 1005849 KAN10 Tank made of HDPE, 10 L 1005850 KAN20 Tank made of HDPE, 20 L Page 4 C. Gerhardt GmbH & Co. KG www.gerhardt.de

Order information accessories and consumables Anschlussstopfen Viton Bestellnr. Typ Beschreibung 12-0477 Connection stopper viton, suitable for distribution heads with connection pipe Ø 32,7 mm e.g: PP-distribution head, no.: 1005828 12-0351 Connection stopper viton, suitable for distribution heads with connection pipe Ø 32,7 mm e.g: - distribution head glass, no.: 12-0587 and - PP-distribution head, no.: 1003795 12-0567 Connection stopper viton, special version suitable for upgrade kit Büchi, no. 12-0568 Connection stopper, Micro 12-0352 Connection stopper VK, Isoversinic micro, special edition for the use of micro digestion tubes 100 ml Upgrade kit Büchi Order No Type Description 12-0568 Büchi - Upgrade kit, complete with: 1 x Viton-connection stopper, No. 12-0351, version standard 1 x Viton-connection stopper, No. 12-0567, version Büchi 1 x Adapter PP-nature PP Distribution head 1005828 PP Distribution head, New version as from 2012 1003795 PP-Distribution head, Version before 2012 1005063 PP-Distribution head upgrade kit, complete with: Connection stopper viton, holder, fastening screws C. Gerhardt GmbH & Co. KG www.gerhardt.de Page 5

Order information accessories and consumables Insert racks for digestion tubes Insert racks made of stainless steel, best for collecting the single digestion tubes, e.g. for direct distillation. 12-0269 EG625 Insert rack 6-place for tubes 250 ml 12-0273 EG125 Insert rack 12-place for tubes 250 ml 12-0271 EG440 Insert rack 4-place for tubes 400 ml 12-0272 EG480 Insert rack 4-place for tubes 800 ml 12-0277 EG12-100 Insert rack 12-place for tubes 100 ml Please see the product data sheet KJELDATHERM for more insert racks and variants. Distillation condenser glass 1000059 DKPP Distillation condenser glass with short outlet pipe, for PP-distribution head 1003795 with connecting piece for ventilation valve 1000058 DK8 Distillation condenser glass with long outlet pipe, for glass distribution head 1004455 with connecting piece for ventilation valve 1000036 Ventilation valve for distillation condenser GL-Screw caps + seals 1004320 Screw cap GL14, nat. white 1004321 Screw cap GL18, nat. white 1004322 Screw cap GL 32, nat. white 1000358 Silicone seal GL 14 with connection, straight 1000356 Silicone-seal GL 18 1000357 Silicone-seal GL 32 RECIRCULATING COOLER FL 10-0045 FL1201 Recirculating cooler 230 V / 50 Hz, 1200 W, for economical and environmentally friendly cooling water supply of VAPODEST 10-0047 FL1201 Identical to 10-0045, but in version 115 V / 60 Hz Page 6 C. Gerhardt GmbH & Co. KG www.gerhardt.de

Order information accessories and consumables Guide cage Carousel 1001797 Sample tube guide cage compl. for 250 ml tubes 1001804 Sample tube guide cage compl. for 400 ml tubes 1001807 Sample tube guide cage compl. for 800 ml tubes Carousel Upgrade Kits For the use of different glass tubes C. Gerhardt offers upgrade kits with suitable carousel inserts and sample tube guide cages. 12-0231 KIT800 Upgrade Kit for carousel 12x800 for tubes 800 ml, complete with: - Sample tube guide cage, 800 ml - carousel 12-place, PP-nature Ø 415 mm 12-0230 KIT400 Upgrade Kit Carousel 16x400, for tubes 400 ml and BS 400 ml, complete with: - Sample tube guide cage 400 - carousel 16-place, PP-nature Ø 415 mm 12-0229 KIT250 Upgrade Kit Carousel 20x250 for tubes 250/300 ml, complete with: - Sample tube guide cage 250 - carousel 20-place, PP-nature Ø 415 mm Tubes / Cable 1000394 Water inlet tube 10/17, 2 m long, 90bar, 3/8 x 1/2 + 3/8 x 3/4 1000047* PVC-tubing, 8 x 12 mm 1000500* PVC-tubing 4 x 7 mm 1000499* Verpren-tubing 8 x 12 mm, Ø außen 12 mm 1000567 PVC-pipe 400 mm long, 10,2 x 1,4 mm 1000566 PVC-pipe 400 mm long, 6 x 1 mm 10-0058 Mains cable, 3 m 1004365 USB-cable, 2 m 10-0193 Data cable DK45, RS232, connection adapter PC 5 m *length needed when order C. Gerhardt GmbH & Co. KG www.gerhardt.de Page 7

Order information support and service SUPPORT AND SERVICE In addition to its high quality instruments, C. Gerhardt offers comprehensive services to maintain the functionality and effeciency of your equipment. INSTALLATION / EQUIPMENT QUALIFICATION Order no Type Description 99-0202 ABI-VAP Installation and Instruction VAPODEST - Installation and connection of the unit - functional check - operating instructions 99-0211 GQF-VAP Equipment Qualification (IQ/OQ) VAPODEST - Installation of the unit and instruction - Installation Qualification IQ and Operational Qualification OQ, Guidance for Performance Qualification PQ - Training of laboratory personnel with certificate - Individual training certificates, if reqested SERVICING AND MAINTENANCE CONCEPTS For detailed information on servicing and maintenance concepts, please contact your local authorised C. Gerhardt representative. WORKSHOPS / SEMINARS / APPLICATIONS TRAINING For detailed information on trainings and workshops, please contact your local authorised C. Gerhardt representative. Page 8 C. Gerhardt GmbH & Co. KG www.gerhardt.de

Order information application data sheet APPLICATION SERVICE The following listed applications are examples from our comprehensive application data base. Please contact your local C. Gerhardt representative or write to application@gerhardt.de to ask for one of the listed application data sheets or to ask for an application which is not yet listed. ANALYSIS OF FEED- AND FOODSTUFFS Selection Description ( ) Non Protein content in Meat ( ) Nitrogen in bread and rolls ( ) Total Nitrogen in Raw Material for Breweries ( ) Solulable Nitrogen Content Wort ( ) Raw Protein Determination in Eggs ( ) Total Protein in Margarine ( ) Tomato puree and Ketchup ( ) Nitrogen in Milk and Dairy Products ( ) Nitrogen in Cream ( ) Protein in Milk Powder ( ) Non-Protein in Milk and Dairy Products ( ) Raw Protein in Meat and Meat Products ( ) Raw Protein in Grain and Grain Products ( ) Raw Protein in Beer and Wort acc. to Lochner ( ) Total Nitrogen in Sugar at very low N-content ( ) Nitrogen in Starch ( ) Nitrogen in Fish and Fish Products ( ) Nitrogen in Chocolate ( ) Total Protein in Fresh Yeast ( ) Raw Protein in Feed ( ) Volatile Acids in Wine ( ) Sulphur Dioxide in Food ( ) Sorbic acid in wine ( ) TVBN in Fish and Fish Products ( ) Vicinal Diketones in Beer ( ) Alcohol in Beverages and Intermediates ENVIRONMENTAL ANALYTICS / OTHER Selection Description ( ) Coagulated Nitrogen ( ) Nitrogen Determination in Fertilizers with Nitrate ( ) Fertilizers without Nitrate Content ( ) Ammonium Determination in Fertilizers ( ) Water soluable Ammonium nitrogen in Fertilizers ( ) Determination of Nitrat and Ammonium Nitrogen fert ( ) Total Nitrogen in Xanthan ( ) Total Nitrogen in Water ( ) Total Nitrogen in Soil ( ) Total Nitrogen in Grass and Plant Material ( ) Total Nitrogen in Coal ( ) Phenol Index in Soils and Water ( ) Ammonium in Solid Samples ( ) Ammonium in Aqueous Samples ( ) Nitrate in Aqueous Samples and Eluates ( ) Total Cyanide in Water, Soil and Sludge ( ) Volatile Organic Acids in Sludge ( ) Total Formaldehyde in Aminoplast Adhesive C. Gerhardt GmbH & Co. KG www.gerhardt.de Page 9

TABLE OF CONFIGURATION Please arrange the required system DISTILLATION SYSTEM / TYPE Quantity CONSUMABLES / ACCESSORIES Quantity SUPPORT AND SERVICE Quantity Send offer to: Customer No. Company Name Address Tel. E-Mail Web Page 10 C. Gerhardt GmbH & Co. KG www.gerhardt.de

C. Gerhardt GmbH & Co. KG www.gerhardt.de Page 11

Presented by: C. Gerhardt GmbH & Co. KG Cäsariusstraße 97 53639 Königswinter, Germany Tel.: +49 (0) 2223 2999-0 www.gerhardt.de