ASTM D Test to Low ppb. Contact us today for a copy of the Southwest Research Institute D-5453 Fitness for Use Report.

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D-1319 to D-2500 D-5453 Test to Low ppb Contact us today for a copy of the Southwest Research Institute D-5453 Fitness for Use Report. AccuStandard s Low Standards Quick analysis using ANTEK s 9000 Series new UVF technology developments enable unprecedented sensitivity no matrix effects more sensitive than x-ray, safer and cleaner than lead acetate D5453 (UVF) technology recongnized by CARB and US EPA Visit www.antekhou.com or call 800) 365-2143 or (281) 580-0339 Low Standards on following pages 7

Standards for Methods D-2622-98, D-3120-96, D-3246-96, D-4294-98, D-5453-00, D-6334-98, D-6445-99 & Proposed Methods AccuStandard offers the Petroleum Industry the most complete line of calibration standards designed for today s Proposed & Promulgated test methods for analysis. These calibration standards are designed specifically for the analysis of in a wide variety of matrices such as #2 diesel fuel, white mineral oil, kerosene, gasoline, crude oil & residual oil. Traceability, Quality and Certification All standards are manufactured from the highest quality raw materials, including well characterized starting materials & the lowest sulfur matrices available from the Petrochemical market. All standards are manufactured on a weight / weight basis using balances which are calibrated and verified daily against reference mass standards directly traceable to NIST under test No. 822/ 254480. The concentration of these working level standards have established traceability links to NIST SRM s where available. Convenient Packaging Since applicable concentration ranges will vary based on the instrumentation used & the nature of the sample the standards can be ordered as complete sets, individual bottles, or Ready-to-Aspirate AccuShots. AccuShots... Packaged to improve analytical standard integrity AccuStandard is the first standard manufacturer to provide sulfur standards in convenient and Ready-to-Aspirate AccuShot 20 ml sealed ampules. Each 20 ml AccuShot provides the necessary material for calibration curve development or daily QA/QC. By purchasing AccuShots the analytical chemist uses only a small portion of the standard & minimizes contamination or evaporation. Methods in Mineral Oil in Heavy Weight Mineral Oil (75 cst) in White Mineral Oil AccuShots Blank 0.000 SWMO-BL-4 SWMO-BL-SHOT 100 0.010 SWMO-1X-4 SWMO-1X-SHOT 200 0.020 SWMO-2X-4 SWMO-2X-SHOT 300 0.030 SWMO-3X-4 SWMO-3X-SHOT 400 0.040 SWMO-4X-4 SWMO-4X-SHOT 500 0.050 SWMO-5X-4 SWMO-5X-SHOT 750 0.075 SWMO-7.5X-4 SWMO-7.5X-SHOT 1,000 0.10 SWMO-10X-4 SWMO-10X-SHOT 1,500 0.15 SWMO-15X-4 SWMO-15X-SHOT 2,000 0.20 -------------------- -------------------------- 3,000 0.30 SWMO-30X-4 SWMO-30X-SHOT 4,000 0.40 -------------------- -------------------------- 5,000 0.50 SWMO-50X-4 SWMO-50X-SHOT 7,000 0.70 SWMO-70X-4 SWMO-70X-SHOT 10,000 1.00 SWMO-100X-4 SWMO-100X-SHOT 15,000 1.50 SWMO-150X-4 SWMO-150X-SHOT 20,000 2.00 SWMO-200X-4 SWMO-200X-SHOT 30,000 3.00 SWMO-300X-4 SWMO-300X-SHOT 40,000 4.00 SWMO-400X-4 SWMO-400X-SHOT 50,000 5.00 SWMO-500X-4 SWMO-500X-SHOT 60,000 6.00 SWMO-600X-4 SWMO-600X-SHOT SWMO-CAL-SET-4 Each AccuShot product in Light Weight Mineral Oil (20 cst) in White Mineral Oil AccuShots Blank 0.000 SWMO-LT-BL-4 SWMO-LT-BL-SHOT 100 0.010 SWMO-LT-1X-4 SWMO-LT-1X-SHOT 200 0.020 SWMO-LT-2X-4 SWMO-LT-2X-SHOT 300 0.030 SWMO-LT-3X-4 SWMO-LT-3X-SHOT 400 0.040 SWMO-LT-4X-4 SWMO-LT-4X-SHOT 500 0.050 SWMO-LT-5X-4 SWMO-LT-5X-SHOT 750 0.075 SWMO-LT-7.5X-4 SWMO-LT-7.5X-SHOT 1,000 0.10 SWMO-LT-10X-4 SWMO-LT-10X-SHOT 1,500 0.15 SWMO-LT-15X-4 SWMO-LT-15X-SHOT 2,000 0.20 -------------------- -------------------------- 3,000 0.30 SWMO-LT-30X-4 SWMO-LT-30X-SHOT 4,000 0.40 -------------------- -------------------------- 5,000 0.50 SWMO-LT-50X-4 SWMO-LT-50X-SHOT 7,000 0.70 SWMO-LT-70X-4 SWMO-LT-70X-SHOT 10,000 1.00 SWMO-LT-100X-4 SWMO-LT-100X-SHOT 15,000 1.50 SWMO-LT-150X-4 SWMO-LT-150X-SHOT 20,000 2.00 SWMO-LT-200X-4 SWMO-LT-200X-SHOT 30,000 3.00 SWMO-LT-300X-4 SWMO-LT-300X-SHOT 40,000 4.00 SWMO-LT-400X-4 SWMO-LT-400X-SHOT 50,000 5.00 SWMO-LT-500X-4 SWMO-LT-500X-SHOT 60,000 6.00 SWMO-LT-600X-4 SWMO-LT-600X-SHOT SWMO-LT-CAL-SET-4 Each AccuShot product concentration calculated from % sulfur in di-n-butyl sulfide Standards of Interest For the mandatory real world QC samples stipulated in the Method, see page 2 8 Quality System is Certified to comply with the International ISO 9001 Quality Standard

Standards for Methods D-2622-98, D-3120-96, D-3246-96, D-4294-98, D-5453-00, D-6334-98, D-6445-99 & Proposed Methods Methods in #2 Diesel Fuel in #2 Diesel Fuel AccuShots Blank 0.000 SDF-BL-4 SDF-BL-SHOT 100 0.010 SDF-1X-4 SDF-1X-SHOT 200 0.020 SDF-2X-4 SDF-2X-SHOT 300 0.030 SDF-3X-4 SDF-3X-SHOT 400 0.040 SDF-4X-4 SDF-4X-SHOT 500 0.050 SDF-5X-4 SDF-5X-SHOT 750 0.075 SDF-7.5X-4 SDF-7.5X-SHOT 1,000 0.10 SDF-10X-4 SDF-10X-SHOT 1,500 0.15 SDF-15X-4 SDF-15X-SHOT 2,000 0.20 3,000 0.30 SDF-30X-4 SDF-30X-SHOT 4,000 0.40 5,000 0.50 SDF-50X-4 SDF-50X-SHOT 7,000 0.70 SDF-70X-4 SDF-70X-SHOT 10,000 1.00 SDF-100X-4 SDF-100X-SHOT 15,000 1.50 SDF-150X-4 SDF-150X-SHOT 20,000 2.00 SDF-200X-4 SDF-200X-SHOT 30,000 3.00 SDF-300X-4 SDF-300X-SHOT 40,000 4.00 SDF-400X-4 SDF-400X-SHOT 50,000 5.00 SDF-500X-4 SDF-500X-SHOT 60,000 6.00 SDF-600X-4 SDF-600X-SHOT SDF-CAL-SET-4 Each AccuShot product AccuShots...Conveniently packaged to improve analytical standard integrity. - Minimize Contamination - Minimize Evaporation Each 20 ml AccuShot provides the necessary material for calibration curve development or daily QA/QC. By purchasing AccuShots the analytical chemist uses only a small portion of the standard & minimizes contamination and evaporation. concentration calculated from % sulfur in di-n-butyl sulfide Methods Methods in Kerosene in Light Distillate Kerosene in Light Distillate Kerosene AccuShots µg/g wt. % Cat. No. Cat. No. Blank 0.000 SK-BL-4 SK-BL-SHOT 100 0.010 SK-1X-4 SK-1X-SHOT 200 0.020 --------------- 300 0.030 SK-3X-4 SK-3X-SHOT 400 0.040 --------------- 500 0.050 SK-5X-4 SK-5X-SHOT 750 0.075 SK-7.5X-4 SK-7.5X-SHOT 1,000 0.10 SK-10X-4 SK-10X-SHOT 1,500 0.15 --------------- 2,000 0.20 SK-20X-4 SK-20X-SHOT 3,000 0.30 SK-30X-4 SK-30X-SHOT 4,000 0.40 SK-40X-4 SK-40X-SHOT 5,000 0.50 SK-50X-4 SK-50X-SHOT 7,000 0.70 --------------- 10,000 1.00 SK-100X-4 SK-100X-SHOT 15,000 1.50 --------------- 20,000 2.00 SK-200X-4 SK-200X-SHOT 30,000 3.00 --------------- 40,000 4.00 --------------- 50,000 5.00 --------------- 60,000 6.00 --------------- SK-CAL-SET-4 Each AccuShot product Cat. No. # s 12 x 4 oz. $ 500 contains 5 x 20 ml in Heavy Distillate Kerosene in Heavy Distillate Kerosene µg/g wt. % Cat. No. Blank 0.000 SK-HD-BL-4 100 0.010 SK-HD-1X-4 200 0.020 SK-HD-2X-4 300 0.030 SK-HD-3X-4 400 0.040 SK-HD-4X-4 500 0.050 SK-HD-5X-4 750 0.075 SK-HD-7.5X-4 1,000 0.10 SK-HD-10X-4 1,500 0.15 SK-HD-15X-4 2,000 0.20 SK-HD-20X-4 3,000 0.30 SK-HD-30X-4 4,000 0.40 SK-HD-40X-4 5,000 0.50 SK-HD-50X-4 7,000 0.70 SK-HD-70X-4 10,000 1.00 SK-HD-100X-4 15,000 1.50 SK-HD-150X-4 20,000 2.00 SK-HD-200X-4 30,000 3.00 SK-HD-300X-4 40,000 4.00 SK-HD-400X-4 50,000 5.00 SK-HD-500X-4 60,000 6.00 SK-HD-600X-4 SK-HD-CAL-SET-4 Cat. No. # s 21 x 4 oz. $ 950 concentration calculated from % sulfur in di-n-butyl sulfide 9

Standards for Methods D-2622-98, D-3120-96, D-3246-96, D-4294-98, D-5453-00, D-6334-98, D-6445-99 & Proposed Methods D-2622-98, D-4294-98 Calibration Standards Calibration Standards in Isooctane for Gasoline & Reformulated Gasoline Analysis 1 to 4 units $ 60 each per Standard 5 to 10 units $ 55 each per Standard $ 50 each per Standard Cat. No. Conc. Wt. % Unit STP-BL-4 Blank 0.0 4 oz. STP-1X-4 10 µg/g 0.001 4 oz. STP-2X-4 20 µg/g 0.002 4 oz. STP-3X-4 30 µg/g 0.003 4 oz. STP-5X-4 50 µg/g 0.005 4 oz. STP-10X-4 100 µg/g 0.010 4 oz. STP-20X-4 200 µg/g 0.020 4 oz. STP-30X-4 300 µg/g 0.030 4 oz. STP-40X-4 400 µg/g 0.040 4 oz. STP-60X-4 600 µg/g 0.060 4 oz. STP-100X-4 1000 µg/g 0.10 4 oz. STP-200X-4 2000 µg/g 0.20 4 oz. STP-300X-4 3000 µg/g 0.30 4 oz. STP-CAL-SET In Isooctane $ 650 / set of 13 x 4 oz. Set contains the above 13 individual bottles A well characterized di-n-butyl sulfide starting material is used with a low sulfur Isooctane matrix for the RFG/gasoline sulfur standards. D-2622-98, D-6334-98, D-6445-99 Low Level Calibration Standards for use on XRF Energy Dispersive or Wavelength Instruments 1 to 4 units $ 60 each per Standard 5 to 10 units $ 55 each per Standard $ 50 each per Standard Cat. No. Conc. Wt. % Unit D-2622-LL-BL-4 Blank 0.0 4 oz. D-2622-LL-5X-4 5 µg/g 0.0005 4 oz. D-2622-LL-10X-4 10 µg/g 0.0010 4 oz. D-2622-LL-30X-4 30 µg/g 0.0030 4 oz. D-2622-LL-50X-4 50 µg/g 0.0050 4 oz. D-2622-LL-75X-4 75 µg/g 0.0075 4 oz. D-2622-LL-100X-4 100 µg/g 0.010 4 oz. D-2622-LL-300X-4 300 µg/g 0.030 4 oz. D-2622-LL-500X-4 500 µg/g 0.050 4 oz. D-2622-LL-1000X-4 1000 µg/g 0.100 4 oz. D-2622-LL-CAL-SET $ 450 / 10 x 4 oz. In Isooctane : Toluene (3:1) Set contains the above 10 individual bottles Low Level Calibration Standards Well characterized Thiophene & 2-Methyl thiophene are used in a low sulfur Isooctane/Toluene matrix for this calibration set. D-3120-96, D-3246-96 Calibration Set D-3120-92-CAL-SET In Isooctane Calibration Set $ 75 / set of 8 x 1 ml Cat. No. Conc. Wt. % D-3120-92-BL Blank D-3120-92-1X 1 µg/g 0.0001 D-3120-92-3X 3 µg/g 0.0003 D-3120-92-10X 10 µg/g 0.0010 D-3120-92-30X 30 µg/g 0.0030 D-3120-92-50X 50 µg/g 0.0050 D-3120-92-75X 75 µg/g 0.0075 D-3120-92-100X 100 µg/g 0.010 Well characterized di-n-butyl sulfide is used in a low sulfur Isooctane matrix for this calibration set. Standards of Interest For the mandatory real world QC samples stipulated in many Methods, see page 2 D-2622-98, D-6334-98, D-6445-99 Mid Level Calibration Standards New Requested Additions for use on XRF Energy Dispersive or Wavelength Instruments 1 to 4 units $ 60 each per Standard 5 to 10 units $ 55 each per Standard $ 50 each per Standard Cat. No. Conc. Wt. % Unit D-2622-LL-200X-4 200 µg/g 0.020 4 oz D-2622-LL-400X-4 400 µg/g 0.040 4 oz D-2622-LL-600X-4 600 µg/g 0.060 4 oz D-2622-LL-700X-4 700 µg/g 0.070 4 oz D-2622-LL-800X-4 800 µg/g 0.080 4 oz D-2622-LL-900X-4 900 µg/g 0.090 4 oz D-2622-LL-1100X-4 1100 µg/g 0.110 4 oz D-2622-LL-1200X-4 1200 µg/g 0.120 4 oz Well characterized Thiophene & 2-Methyl thiophene are used in a low sulfur Isooctane/Toluene matrix for this calibration set. 10 Quality System is Certified to comply with the International ISO 9001 Quality Standard

Standards for Methods D-2622-98, D-3120-96, D-3246-96, D-4294-98, D-5453-00, D-6334-98, D-6445-99 & Proposed Methods Methods Calibration Standards in Crude Oil Standards Total in Aromatic Compounds by Hydrogenolysis & Rateometric Colorimetry -P-0010-PAK 1000 µg/ml in Toluene in Crude Oil µg/g Wt. % Cat. No. 1,000 0.10 SCO-10X-4 2,500 0.25 SCO-25X-4 5,000 0.50 SCO-50X-4 10,000 1.00 SCO-100X-4 20,000 2.00 SCO-200X-4 30,000 3.00 SCO-300X-4 40,000 4.00 SCO-400X-4 50,000 5.00 SCO-500X-4 SCO-CAL-SET-4 Cat. No. s 8 x 4 oz. $ 500 Standards 4 oz Bottle $ 75 ea $ 65 ea Methods Standards $ 75 / 5 x 1 ml in Residual Oil Standards Standards 4 oz Bottle $ 75 ea $ 65 ea Trace Quantities of in Liquid Aromatic Hydrocarbons by Oxidative Microcoulometry -P-0020-PAK 1000 µg/ml in Xylenes in Crude Oil µg/g Wt. % Cat. No. 3,500 0.35 SRO-35X-4 7,000 0.70 SRO-70X-4 10,000 1.00 SRO-100X-4 15,000 1.50 SRO-150X-4 20,000 2.00 SRO-200X-4 30,000 3.00 SRO-300X-4 40,000 4.00 SRO-400X-4 SRO-CAL-SET-4 Cat. No. s 7 x 4 oz. $ 450 $ 75 / 5 x 1 ml AccuStandard's Technical Service Dept. can provide Ready-to-Inject working level calibration standards to meet unique laboratory applications call or fax us your standard requirements. Methods (as Thiophene) -SSTD-A/B-SET $ 100 / 10 x 2 ml The set contains the following 10 standards in isooctane (as Dibenzothiophene) NEW Cat. No. Description Unit -SSTDA-BL Blank 2 ml -SSTDA-01 @ 0.5 µg/g in Isooctane 2 ml -SSTDA-02 @ 1.0 µg/g in Isooctane 2 ml -SSTDA-03 @ 2.5 µg/g in Isooctane 2 ml -SSTDA-04 @ 5.0 µg/g in Isooctane 2 ml -SSTDB-BL Blank 2 ml -SSTDB-04 @ 5.0 µg/g in Isooctane 2 ml -SSTDB-05 @ 10.0 µg/g in Isooctane 2 ml -SSTDB-06 @ 25.0 µg/g in Isooctane 2 ml -SSTDB-07 @ 50.0 µg/g in Isooctane 2 ml D-2789-95 Hydrocarbon Types in Low Olefinic Gasoline by MS Composition Test Mix D-2789-CTM D-2789-CTM-PAK (Vol. %) 2-Methylpentane 7.2 2,4-Dimethylpentane 9.4 n-octane 16.6 Methylcyclopentane 7.1 Methylcyclohexane 10 $ 40 / 1 x 1 ml SAVE 20% $ 160 / 5 x 1 ml 9 comps. (Vol. %) cis-1,2-dimethylcyclohexane 15.5 Benzene 7.7 Toluene 10 p-xylene 16.5 Custom Formulations AccuStandard can formulate customer specific standards for this method. Fax AccuStandards Technical Department (1-203-786-5287) or check out our website for custom requests. Both the actual volume % ratio and the final weight fractions for each analyte will be listed on the certificate. 11