PMP HD Validation Exercise and Round Robin

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JRC Brussels 25 October 2007 1 PMP HD Validation Exercise and Round Robin G. Martini, B. Giechaskiel, M. Carriero

JRC Brussels 25 October 2007 2 PMP Heavy Duty Validation Exercise and Round Robin Both coordinated by the JRC PMP HD Validation Exercise Golden Engine-1 Golden Systems Golden Engineer Same fuel and lubricant Both full flow system and partial flow system Participant: JRC, UTAC, AVL MTC, EMPA, PMP HD Round Robin exercise Golden Engine-2 Instrument chosen by each lab No Golden Engineer Standard ref. fuel/lubricant Both full flow system and partial flow system 10 laboratories from EU, Japan Korea, Canada

JRC Brussels 25 October 2007 3 PMP Heavy Duty Validation Exercise and Round Robin Both coordinated by the JRC PMP HD Round Robin exercise Golden Engine-2 : DC Engine provided by ACEA Each lab will use its own instrument No Golden Engineer Standard ref. fuel/lubricant Both full flow system and partial flow system 10 laboratories from EU, Japan Korea, Canada Expected start: after the exploratory work

JRC Brussels 25 October 2007 4 PMP Heavy Duty Validation Exercise and Round Robin Both coordinated by the JRC PMP HD Validation Exercise Golden Engine-1 : IVECO Cursor 8 Euro III + CRT Golden Systems : 2 SPCS from HORIBA Golden Engineer: Jon Andersson (Ricardo) Fuel: RF06-03 PMP (10 ppm sulphur) Lubricant: BP Vanellus E8 Ultra 5W-30

JRC Brussels 25 October 2007 5 PMP Heavy Duty Validation Exercise and Round Robin Both coordinated by the JRC PMP HD Validation Exercise Total flow dilution system Partial flow system 1 : AVL Smart Sampler Partial flow system 2: PSS-20 Control System

JRC Brussels 25 October 2007 6 PMP HD Validation Exercise: Current status Upgrade of the test cell completed Golden Engine installed and running Lubricant and fuel OK Test protocol revised by the Golden Engineer Golden Instruments installed Exploratory work started

JRC Brussels 25 October 2007 7 PMP HD Validation Exercise Works required for the test cell upgrade Upgrade of the test cell software in order to run the WHDC cycles Dilution air filtration system: checked and OK Secondary dilution air pump: HEPA filter added Use of heating blankets to control the temperature in the secondary dilution tunnel Installation of a cyclone in the PM sampling line Replacement of the 70 mm filter holders with 47 mm filter holders New sampling points for the particle counter systems Upgrade of the partial flow system

JRC Brussels 25 October 2007 8 PMP HD revised protocol

JRC Brussels 25 October 2007 9 PMP HD Validation Exercise Golden engine

JRC Brussels 25 October 2007 10 PMP HD Validation Exercise After-treatment Device

JRC Brussels 25 October 2007 11 Preliminary results of exploratory work in JRC

JRC Brussels 25 October 2007 12 Tasks Background mass/number Primary / Secondary tunnel Partial flow systems Preconditioning Mass 47 C (how we achieve, dilution air, mixed flow?) 47mm or 70mm filters Filter material Backup filter Cyclone

JRC Brussels 25 October 2007 13 Tasks Number SPCS at the same position Different sampling temperatures (47ºC or 192ºC) Evaporation tube temperature Partial Full flow comparisons AVL Control Sistem PSS 20 Look ahead Decisions on positions, flowrates etc

JRC Brussels 25 October 2007 14 Tasks Background mass/number Primary / Secondary tunnel Partial flow systems Preconditioning Mass 47 C (how we achieve, dilution air, mixed flow?) 47mm or 70mm filters Filter material Backup filter Cyclone

JRC Brussels 25 October 2007 15 Reference filter and weighting procedure Balance Precision of 1μg for a reference weight No, Sartorius M5P (we wanted to measure 47 and 70mm filters at the same balance) Weighting room T: 22 ±3 C 23 ±3 C RH: 45 ±8% 51 ±1.5% Conditioning of filters 8 to 80 h 2 to 24 h Neutraliser yes Reference Filter: 89.934 ±0.005 (min/max) (or 0.0035 for 1 stdev)

JRC Brussels 25 October 2007 16 Background (Smart Sampler)

JRC Brussels 25 October 2007 17 Background (Primary tunnel)

JRC Brussels 25 October 2007 18 Background (secondary tunnel) Flow direction 60 m 3 /min LEPA HEPA act. act. carbon ENGINE OFF dilution dilution tunnel tunnel dilution tunnel Dilution air HEPA 20 lpm Dilution air HEPA 30 lpm 47mm TX40 Pre-baked at 52 C No flow -3 (+3) μg (30 min) 45 C 45 C 47mm PM 40 no lpm flow ~19 7 (-4) (+4) μg (30 min) 70mm PM PM no 60 flow lpm -7 ~23 (-3) (-10) μg μg (30 (30 min)

JRC Brussels 25 October 2007 19 Particle Mass Results Emission [mg/kwh] 8 7 6 5 4 3 2 1 0-1 WHSC 70mm TX40 (60lpm, 43cm/s) Backup Filter Main Filter Leakage! BG WHSC BG WHSC BG WHSC BG WHSC BG 47mm TX40 47mm TX40 47mm TX40 baked 47mm Teflo (60lpm, 100cm/s) 70cm/s) (40lpm, 100cm/s) 70cm/s) (40lpm, 100cm/s) 70cm/s) (40lpm, 100cm/s) 70cm/s)

JRC Brussels 25 October 2007 20 Particle Number Measurements 3

JRC Brussels 25 October 2007 21 Importance of preconditioning 1.0E+05 Solids #10 #1 1.0E+04 #10 N [#/cc] #7 #8 1.0E+03 #1 modes 7, 9, 11 #3 #2 #2 #8 #3 #1 1.0E+02-1680 -1440-1200 -960-720 -480-240 0 240 480 Time [s]

JRC Brussels 25 October 2007 22 Regeneration-Loading 1.0E+05 #10 (10min) #7 (20min) #2 #8 #3 #1 levels tend to stabilise 1.0E+04 c N [#/cc] d b 1.0E+03 a 1.0E+02-1680 -1440-1200 -960-720 -480-240 0 240 480 Solids Time [s]

JRC Brussels 25 October 2007 23 Regeneration-Loading 1.0E+05 mode#10 (15min) mode#7 (30min) #2 #8 #3 #1 1.0E+04 10min b a d N [#/cc] c 1.0E+03 1.0E+02-2640 -2400-2160 -1920-1680 -1440-1200 -960-720 -480-240 0 240 480 Solids Time [s]

JRC Brussels 25 October 2007 24 Total - Solids 1.0E+06 1.0E+05 EJ+3025A N [#/cc] 1.0E+04 1.0E+03 EJ+TD+3010 #2 #8 #3 #1 1.0E+02-1680 -1440-1200 -960-720 -480-240 0 240 480 Time [s]

JRC Brussels 25 October 2007 25 1.0E+05 PN at CVS [cm -3 ] 1.0E+04 1.0E+03 1.0E+02 3025A at CVS TD+EJ+3010 at CVS ETC 1.0E+01 0 500 1000 1500 1.0E+04 2000 Time [s] 3025A at CVS TD+EJ+3010 at CVS ESC PN at CVS [cm -3 ] 1.0E+03 1.0E+02 1.0E+01 0 500 1000 1500 2000 Time [s]

JRC Brussels 25 October 2007 26 Conclusions -Weighting procedure extremely important for DPF engines -Background mass in the order of 20μg (30min) -Background number ~1#/cc -Lower PM emissions with 47mm compared to 70mm (due to higher filter face velocity) -No effect of 40 to 60 lpm flows on mass emissions -Mass results close to background levels although low DRs were used. --Preconditioning important for particle measurements -There are a lot of volatiles even with low sulfur fuel

JRC Brussels 25 October 2007 27 Acknowledgements -Jon Andersson from RICARDO for his helpful advice while acting as the Golden Engineer of the PMP programme. -Stefano Alessandrini and Forni Fausto for their excellent work and long hours put in during the tests in the laboratory

JRC Brussels 25 October 2007 28 Thank you for your attention!