SensoLyt 700 SensoLyt 700 SW

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Operating manual SensoLyt 700 SensoLyt 700 SW SensoLyt 700 SensoLyt 700 SW ph/orp armature with impedance converter and temperature sensor ba15307e04 12/2005

SensoLyt 700 (SW) Accuracy when going to press The use of advanced technology and the high quality standard of our instruments are the result of continuous development. This may result in differences between this operating manual and your instrument. Also, we cannot guarantee that there are absolutely no errors in this manual. Therefore, we are sure you will understand that we cannot accept any legal claims resulting from the data, figures or descriptions. Note The latest version of the present operating manual can be found on the Internet under www.wtw.com. Copyright Weilheim 2005, WTW GmbH Reprinting - even as excerpts - is only allowed with the explicit written authorization of WTW GmbH, Weilheim. Printed in Germany. 26

SensoLyt 700 (SW) Contents SensoLyt 700 (SW) - Contents 1 Overview..................................... 28 1.1 Structure of the SensoLyt 700 (SW) ph/orp armature 28 1.2 Recommended fields of application................ 28 2 Safety....................................... 29 2.1 General information on safety.................... 29 2.2 Authorized use................................ 30 2.3 User qualifications............................. 30 2.4 General safety instructions....................... 30 3 Commissioning............................... 32 3.1 Scope of delivery.............................. 32 3.2 Installation................................... 32 3.3 Commissioning / Getting the instrument ready for measuring................................... 33 4 Measuring / Operation.......................... 36 4.1 Calibration................................... 36 4.2 Measuring................................... 36 5 Maintenance and changing the electrode.......... 37 5.1 General maintenance instructions................. 37 5.2 Replacing the combination electrode............... 37 5.3 Cleaning..................................... 41 5.4 Disposal..................................... 41 6 Replacement parts and accessories.............. 42 6.1 Combination electrodes......................... 42 6.2 General accessories........................... 42 7 What to do if................................... 43 8 Technical data................................ 44 8.1 Measurement characteristics..................... 44 8.2 Application characteristics....................... 44 8.3 General data................................. 46 8.4 Electrical data................................. 48 ba15307e04 12/2005 27

Overview SensoLyt 700 (SW) 1 Overview 1.1 Structure of the SensoLyt 700 (SW) ph/orp armature 1 2 3 4 5 Fig. 1-1 Structure of the ph/orp armature (example, SensoLyt 700) 1 Protective hood 2 Temperature sensor 3 Electrode (not contained in the scope of delivery) 4 Electrode receptacle 5 Armature shaft Note The ph combination electrodes that can be used are available as accessories (see chapter 6 REPLACEMENT PARTS AND ACCESSORIES). Impedance converter Glass breakage monitoring An impedance converter integrated in the armature shaft converts the high-impedance measurement signal of the electrode into a lowimpedance signal. This ensures an interference-free signal transmission even over greater distances. The sensor is equipped with a SensCheck function for monitoring glass breakage. 1.2 Recommended fields of application SensoLyt 700 SensoLyt 700 SW In conjunction with the SensoLyt SEA, SensoLyt DWA and SensoLyt ECA ph combination electrodes as well as the SensoLyt PtA ORP combination electrode, the SensoLyt 700 (SW) ph/orp armature is suitable for stationary ph or ORP measurement in the following fields: Stationary measurements in water/wastewater applications. Stationary measurements in seawater and brackish water, aquaculture. 28 ba15307e04 12/2005

SensoLyt 700 (SW) Safety 2 Safety 2.1 General information on safety These safety instructions contain all instructions that have to be followed for a safe operation of the SensoLyt 700 (SW) ph/orp armature. Before starting any work with the SensoLyt 700 (SW), carefully read the safety instructions and strictly follow all protective measures mentioned. Always keep this operating manual in the vicinity of the armature. General safety instructions Safety instructions in this operating manual can be recognized by the warning symbol (triangle) in the left column. The signal word (e. g. "Caution") indicates the level of the danger: Warning indicates instructions that must be followed precisely in order to prevent serious dangers to persons. Caution indicates instructions that must be followed precisely in order to avoid slight injuries or damage to the instrument or the environment. Other labels Note indicates notes that draw your attention to special features. Note indicates cross-references to other documents, e.g. operating manuals. ba15307e04 12/2005 29

Safety SensoLyt 700 (SW) 2.2 Authorized use The authorized use of the SensoLyt 700 (SW) consists of the stationary measurement of ph or ORP and temperature in conjunction with a ph or ORP combination electrode. The technical specifications according to chapter 8 TECHNICAL DATA must be observed. Only operation according to the instructions given in this operating manual is considered to be authorized. Any other use is considered to be unauthorized. Unauthorized use invalidates any claims with regard to the guarantee. 2.3 User qualifications Calibrating the SensoLyt 700 (SW) requires the handling of chemicals. Thus, we assume that the relevant personnel are familiar with the necessary precautions to take when dealing with chemicals as a result of their professional training and experience. 2.4 General safety instructions Function and operational safety The armature left the factory in a safe and secure technical condition. The failure-free function and operational safety of the armature is only guaranteed if the generally applicable safety measures and the special safety instructions in this operating manual are followed during its use. The smooth functioning and operational safety of the armature can only be guaranteed under the environmental conditions that are specified in chapter 8 TECHNICAL DATA. The specified temperature (chapter 8 TECHNICAL DATA) must be maintained during the application and transport of the armature. Protect the armature, particularly against frost or overheating. 30 ba15307e04 12/2005

SensoLyt 700 (SW) Safety Safe operation If safe operation is no longer possible, the armature must be taken out of operation and secured against inadvertent operation. Safe operation is no longer possible if the armature: has been damaged in transport has been stored under adverse conditions for a lengthy period of time is visibly damaged no longer operates as described in this manual. If you are in any doubt, contact the supplier of your armature. Obligations of the operator The operator of the armature must ensure that the following rules and regulations are followed when dealing with hazardous substances: EEC directives for protective labor legislation National protective labor legislation Safety regulations Safety data sheets of the chemical manufacturer. Caution All changes of the SensoLyt 700 (SW) that exceed the work described in this operating manual are not allowed. Repair work may only be carried out by WTW Weilheim. ba15307e04 12/2005 31

Commissioning SensoLyt 700 (SW) 3 Commissioning 3.1 Scope of delivery SensoLyt 700 (SW) ph/orp armature The armature is equipped with a protective hood and protection caps Operating manual. 3.2 Installation Caution The SensoLyt 700 (SW) ph/orp armature may only be submersed in conjunction with a mounted combination electrode. When exchanging the electrode, no moisture may get into the armature, as otherwise the armature will be destroyed. Which electrodes can be used together with the SensoLyt 700 (SW) ph/ ORP armature is given in section 6.1 COMBINATION ELECTRODES. Connection to the measuring transmitter The connection cable of the SensoLyt 700 (SW) is ready to be connected to the terminal strip of a measuring transmitter with highimpedance ph/orp input. For all further information please refer to the operating manual of the measuring transmitter. The assignment of the cable wires of the SensoLyt 700 (SW) can be found in the chapter 8 TECHNICAL DATA of this operating manual. Note Do not suspend the sensor on the sensor connection cable. Use an armature or electrode holder. Information on this and other accessories is given in the WTW catalog and on the Internet. 32 ba15307e04 12/2005

SensoLyt 700 (SW) Commissioning 3.3 Commissioning / Getting the instrument ready for measuring Note A KCI-filled plastic cap is mounted on the tip of the sensor to keep the electrode active during storage (or during longer pauses in measuring). The cap must be removed for measuring. Mounting the combination electrode 1 Unscrew the protective hood from the armature. 2 Pull off the blind plug from the plug head socket of the armature. 3 Screw off the protective cap of the plug head connector of the electrode. ba15307e04 12/2005 33

Commissioning SensoLyt 700 (SW) 4 Screw the electrode into the plug head socket of the armature. 5 Push the unit into the armature up to the stop. Caution Push the connected electrode into the armature right up to the stop so that the connection is watertight. 6 Pull the KCI-filled plastic cap off the electrode for measuring. 34 ba15307e04 12/2005

SensoLyt 700 (SW) Commissioning 7 Screw the protective hood onto the armature. 8 Make the settings for the electrode on the measuring transmitter. Subsequently, calibrate the measuring system (see section 4.1 CALIBRATION). ba15307e04 12/2005 35

Measuring / Operation SensoLyt 700 (SW) 4 Measuring / Operation Note Calibrate the measuring system after the initial commissioning and at regular intervals (depending on the application). 4.1 Calibration Why calibrate? When to calibrate? Calibration procedures During the operation of a ph electrode, the slope and asymmetry of the electrode changes with time. The calibration procedure determines the current slope and asymmetry of the electrode. Calibrate before measuring and at regular intervals (depending on the application). The available calibration procedures depend on the measuring transmitter used. The individual steps for the calibration are comprehensively described in the operating manual of the measuring transmitter. 4.2 Measuring Warning Contact with the sample can lead to danger to the user! Depending on the type of sample, suitable protective measures must be taken (protective clothing, protective goggles, etc.). Please pay attention to: the minimum immersion depth of the armature (> 40 mm) the measuring range of the electrode used (see operating manual of the electrode). 36 ba15307e04 12/2005

SensoLyt 700 (SW) Maintenance and changing the electrode 5 Maintenance and changing the electrode 5.1 General maintenance instructions The SensoLyt 700 (SW) ph/orp armature works maintenance-free. Please read the maintenance of the electrode in the relevant operating manual of the electrode. 5.2 Replacing the combination electrode Warning Contact with the sample can lead to danger to the user! Depending on the type of sample, suitable protective measures must be taken (protective clothing, protective goggles, etc.). Caution If the glass of the ph electrode breaks, there is a danger of cuts from the splinters of glass! If it is necessary to replace an electrode, proceed as follows: 1 Unscrew the protective hood from the armature. ba15307e04 12/2005 37

Maintenance and changing the electrode SensoLyt 700 (SW) 2 Use the protective hood as a tool to lever out the electrode. 3 Carefully pull out the electrode until the plug head screwed fitting can be seen. 4 Unscrew the combination electrode from the plug head socket (for disposal, see section 5.4). 38 ba15307e04 12/2005

SensoLyt 700 (SW) Maintenance and changing the electrode 5 Screw in a new electrode. 6 Push the unit into the armature up to the stop. Caution Push the connected electrode into the armature right up to the stop so that the connection is watertight. 7 Pull the KCI-filled plastic cap off the electrode for measuring. 8 Screw the protective hood onto the armature. ba15307e04 12/2005 39

Maintenance and changing the electrode SensoLyt 700 (SW) 9 Calibrate the measuring system (see section 4.1 CALIBRATION). 40 ba15307e04 12/2005

SensoLyt 700 (SW) Maintenance and changing the electrode 5.3 Cleaning For normal operation (e.g. municipal wastewater), exterior cleaning and calibration are strongly recommended: in the case of pollution (according to visual check) if there is a suspicion of erroneous measured values if the measured value lies outside the range of precision required by the user during the function check. Exterior cleaning Contamination For sludge and loosely adhering dirt, or biological deposits Salt and / or lime deposits Cleaning agents Soft cloth or soft sponge, warm tapwater with detergent Acetic acid (volume percentage = 20 %), soft cloth or soft sponge Note Please also observe the instructions on cleaning the electrode in the respective operating manual. 5.4 Disposal Armature Combination electrodes We recommend disposing of the armature as electronic refuse. If no official regulations apply to the contrary, used and defective electrodes can be treated as household waste. ba15307e04 12/2005 41

Replacement parts and accessories SensoLyt 700 (SW) 6 Replacement parts and accessories 6.1 Combination electrodes Caution The pressure resistance of the operable ph/orp armature can be restricted by the pressure resistance of the electrode (see chapter 8 TECHNICAL DATA). When selecting the electrode please make sure it is suitable for the pressure range and temperature range planned. ph combination electrodes Model SensoLyt SEA SensoLyt DWA SensoLyt ECA SensoLyt SEA-HP Order no. 109 115 109 119 109 117 109 118 ORP combination electrode SensoLyt PtA 109 125 6.2 General accessories Technical buffer solutions for ph calibration Buffer (bottles of 1 liter) ph value Order no. TEP 4 TEP 7 TEP 10 4,01 7,0 10,0 108 700 108 702 108 704 Protective hood Model Order no. SensoLyt 700 SK 109 194 Note Information on further accessories is given in the WTW catalog and on the Internet. 42 ba15307e04 12/2005

SensoLyt 700 (SW) What to do if... 7 What to do if... Measurement delivers no or wrong measured values Cause Remedy Armature not connected Check connection to meter Electrode not connected or defective Check electrode and electrode connection Watering cap still on the electrode No or wrong calibration performed Pull off watering cap and calibrate Calibrate Electrode contaminated Clean electrode Liquid has penetrated the armature Armature defective, return to WTW Instrument setting incorrect Correct instrument setting System cannot be calibrated Cause Remedy Slope of the electrode too low Replace electrode Asymmetry of the electrode too high Armature is operated with ORP electrode Replace electrode Use ph electrode ba15307e04 12/2005 43

Technical data SensoLyt 700 (SW) 8 Technical data 8.1 Measurement characteristics Measuring principle Measuring range Potentiometric measurement using a combination electrode. Signal amplifier integrated in the sensor for low impedance signal transmission Depending on the built-in electrode Temperature measurement Sensor accuracy Response time ± 0.3 K t 99 (99 % of the final value display after) < 15 s 8.2 Application characteristics Temperature range Measuring medium Storage/transport 0 C... + 60 C (32... 140 F) - 5 C... + 65 C (23... 149 F) Allowed ph range of the test sample 4... 12 Pressure resistance Max. allowed overpressure (sensor including connection cable): with installed combination electrode, SensoLyt SEA, DWA, PtA with installed combination electrode, SensoLyt ECA with installed combination electrode, SensoLyt SEA-HP 10 6 Pa (10 bar) * 6 x10 5 Pa (6 bar) * 10 6 Pa (10 bar) ** * temperature dependent (see safety instruction below) ** in the entire temperature range The SensoLyt 700 (SW) meets the requirements according to article 3(3) of the directive, 97/23/EC ("pressure equipment directive"). 44 ba15307e04 12/2005

SensoLyt 700 (SW) Technical data Immersion depth with installed combination electrode, SensoLyt SEA, DWA, PtA with installed combination electrode, SensoLyt ECA with installed combination electrode, SensoLyt SEA-HP min. 40 mm; max. 100 m * or to cable end min. 40 mm; max. 60 m * or to cable end min. 40 mm; max. 100 m ** or to cable end * temperature dependent (see safety instruction below) ** in the entire temperature range Caution The pressure resistance of the operable ph/orp armature can be reduced by the pressure resistance of the combination electrode. When selecting the combination electrode make sure it is suitable for the intended pressure and temperature range. Type of protection Armature with integrated electrode including connection cable IP 68, 10 bar (10 6 Pa) Plug connector IP 65 Operating position Any Fields of application SensoLyt 700 SensoLyt 700 SW Stationary measurements in water/wastewater applications Stationary measurements in seawater and brackish water, aquaculture Automatic sensor monitoring (SensCheck function) Function for glass breakage monitoring of the ph electrode by the measuring transmitter ba15307e04 12/2005 45

Technical data SensoLyt 700 (SW) 8.3 General data Dimensions Weight (without sensor connection cable and combination electrode) SensoLyt 700 SensoLyt 700 SW approx. 320 g approx. 880 g Electrodes that can be integrated ph combination electrodes ORP electrodes SensoLyt SEA, SEA-HP, DWA, ECA SensoLyt PtA Connection technique Connection cable permanently mounted on the sensor. Connection to the measuring transmitter via 7-pole screw plug. 46 ba15307e04 12/2005

SensoLyt 700 (SW) Technical data Material Shaft Shaft screw: SensoLyt 700 SensoLyt 700 SW Protective hood Electrode receptacle Temperature sensor: SensoLyt 700 SensoLyt 700 SW Closing head Protection ring Cable gland: SensoLyt 700 SensoLyt 700 SW Cable sheath POM V4A stainless steel 1.4571 Titan Grade 2 PVC POM V4A stainless steel 1.4571 V4A stainless steel 1.4571, KTLcoated POM POM V4A stainless steel 1.4571 Titan Grade 2 PUR Connection cable Length: SensoLyt 700 SensoLyt 700 SW Diameter Smallest allowed bend radius 7 m (special lengths on request) 15 m 8.6 mm Permanent bend: 130 mm Short time bend: 80 mm Instrument safety Applicable norms EN 61010-1 UL 3111-1 CAN/CSA C22.2 No. 1010.1 Electromagnetic compatibility Test certificates according to EN 61326 class B and FCC class A UL, cul ba15307e04 12/2005 47

Technical data SensoLyt 700 (SW) 8.4 Electrical data Pin assignment Pin Assignment Voltage Max. current 1 Ua (output signal) --- --- 2 0 V --- --- 3 Ub+ + 10 V < 1 ma 4 Ub- - 10 V < 1 ma 5 NTC < 3.5 V < 0.15 ma 6 NTC < 3.5 V < 0.15 ma 7 --- --- --- Plug from the front: 3 4 2 7 5 1 6 48 ba15307e04 12/2005

SensoLyt 700 (SW) Technical data ba15307e04 12/2005 49

Wissenschaftlich-Technische Werkstätten GmbH Dr.-Karl-Slevogt-Straße 1 D-82362 Weilheim Germany Tel: +49 (0) 881 183-0 +49 (0) 881 183-100 Fax: +49 (0) 881 183-420 E-Mail: Info@WTW.com Internet: http://www.wtw.com