एमआरप एल ग णव नय ण य गश ल उप दन व श:२०१७ MRPL QC LABORATORY

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1 एमआरप एल ग णव नय ण य गश ल उप दन व श:२०१७ MRPL QC LABORATORY PRODUCTS SPECIFICATIONS:2017

2 INDIAN STANDARD (IS) SPECIFICATIONS FOR DOMESTIC PRODUCTS: 2017 S.No Product Name Specification Number 1 Liquefied Petroleum Gases (LPG) 2 Motor Gasoline MG 91 BSIV IS 4576: 1999-Second Revision, Reaffirmed 2014, Amendment 1,2003 IS 2796:2014-5th Revision (Amendment No.1) April Aviation Turbine Fuel (ATF) Kerosene Type, Jet A-1 IS 1571:2008, 8 revision, reaffirmed 2013 and Defence Standard , Issue 9,dated & JIG(AFQRJOS) Issue 29,October Kerosine-SKO IS 1459: 2016, 3 rd Revision 5 Automotive Diesel Fuel (HSD)- BS IV/EURO IV IS 1460: 2005,5 th Revision (Amendment No.3) September 2012,reaffirmed Automotive Diesel Fuel IS 1460: th Revision 7 Fuel Oil- MV2 Grade IS 1593: 1982, Reaffirmed 2014, Second Revision, Amendment 1 & 2 8 Paving Bitumen -VG 30 IS 73: 2013, 4 th Revision 9 Paving Bitumen -VG 10 IS 73: 2013, 4 th Revision

3 SPECIFICATION FOR LIQUEFIED PETROLEUM GAS (Commercial Butane-Propane Mixture) IS Density@ 15 C g/ml Report ASTM D Vapour pressure at 40 C kpa 1050 Max. ASTM D Composition, Liquid - ASTM D 2163 i. C2 Hydrocarbons (Ethane) Vol% Report - ii. C3 Hydrocarbons (Propane) Vol% Report - iii. C4 Hydrocarbons (Iso- Butane) Vol% Report - iv. C4 Hydrocarbons (n- Butane) Vol% Report - v. C5 Hydrocarbons & Heavier Vol% Max vi. Unsaturated Hydrocarbons Vol% Report - OR - - Volatility evaporation temperature in C for 95 % by vol. at 760 mm Hg pressure C Max +2 ASTM D Total Volatile Sulphur ppm Max ASTM D Copper 38 C, for 1 hour. Not worse than No. 1 ASTM D Hydrogen Sulfide Pass ASTM D Free water Content None VISUAL

4 SPECIFICATION FOR MOTOR GASOLINE (UNLEADED REGULAR)MG 91 BHARAT STAGE IV IS Grade BS IV MG 91 (Unleaded regular) 2 Color Visual Orange Visual 3 Density at 15 C Kg/m3 Range ASTM D DISTILLATION: - ISO3405/ASTM D86 Recovery up to 70 C, {E70} Vol % Range Recovery up to 100 C, {E100] Vol % Range Recovery up to 150 C, {E150] Vol % Min 75 - Final Boiling Point (FBP) C Max Residue Vol % Max Research Octane Number (RON) Min 91.0 ASTM D Motor Octane Number (MON) Min 81.0 ASTM D Gum Content(solvent Washed) g/m3 Max 40.0 ASTM D Sulphur (Total ) mg/kg Max 50 ASTM D Lead Content (as Pb) g/l Max ASTM D Reid Vapour pressure 38 C kpa Max Vapour Lock Index {VLI) (VLI=10*RVP + 7*E7O} a) Summer a) Other months IS 1448 P:39/ASTM D Max 750 Max 950 Calculation 12 Benzene percent by Volume Vol % Max 1.0 ASTM D Copper strip corrosion (for 3 hrs at 50 C) Water tolerance of Gasoline- Alcohol, blends temp. For Phase separation Not more than 1 - IS 1448, P: 15 / ISO 2160/ ASTM D 130 As per IS Annex B a) Summer C Max 10 - b) Winter C Max Zero - 15 Oxidation Stability Minutes Min Olefin Content Vol % Max 21.0 IS 1448: P:28 / ISO 7536/D 525 IS 1448:P:23/ ASTM D 1319

5 17 Aromatic Content Vol % Max 35.0 IS 1448:P: 23/ ASTM D Oxygen Content Mass % Max 2.7 ISO Oxygenates* Vol % ASTM D 4815/Annex C 20 Ethanol Content % Mass Max 4.75±0.25 ASTM D 4815/Annex E 21 Engine intake system cleanliness mg/kg Report - MFA used - Note: 1. * Contains no Oxygenates 2. Summer : May to July.

6 SPECIFICATION FOR AVIATION TURBINE FUEL JET A-1 IS DOMESTIC Also Meets Def Stan Issue 9 and AFQRJOS issue 29, dated ` 1) APPEARENCE a) Visual Appearance b) Colour c) d) 2) Particulate Contamination, at point of manufacture, mg/l Particulate cumulative channel particle counts, ISO code as per table 1 of ISO 4406:1999 4um(c) 6um(c) 14um(c) 21um(c) 25um(c) 30um(c) COMPOSITION Number mg/l ISO code and counts Clear & Bright free from Solid matter & un dissolved water at ambient temperature. Report Max 1.0 Visual ASTM D 156/D 6045 IP 423/ASTM D 5452 Report IP a) Total Acidity, mg KOH/g, Max mg KOH/g Max IS 1448 P:113 b) Aromatics % vol, Max. Vol % 25.0 (22.0- Defence) IS 1448 P:23 c) Sulphur, Total % m/m, Max d) e) Sulphur Mercaptan, percent by mass, Max or Doctor Test, REFINING COMPONENT AT THE POINT OF MANUFACTURE. 1. Non Hydro processed components, % v/v 2.Severely Hydro processed component, % v/v Mass % Mass % Vol % Vol % Max (0.002 Defence) or Doctor Negative Report Report ASTM D 4294/P:34 IS 1448 P:109/P:19

7 3) VOLATILITY - - a) Distillation IS 1448 P:18 Initial Boiling Point, at C, C Report 10 percent recovery, at C, v/v, Max. C Max percent recovery at C,v/v C Report 90 percent recovery at C, v/v C Report Final Boiling Point C, Max. C Max Residue percent by volume, Max. Vol % Max Loss% volume, Max. Vol % Max b) Flash Point, C. Min. C Min 38.0 IS 1448 P:20 (Method B) c) 15 C, kg/m3 Kg/m3 Range IS 1448 P:16 4) FLUIDITY - - a) Freezing point, C, Max. C Max Minus 47 IS 1448 P:11 b) 5) Kin. Viscosity at minus 20 C, mm 2 /s Max. COMBUSTION a) Specific energy MJ/kg, Min Or Product of API gravity and Aniline point, Min cst MJ/kg Max IS 1448 P:25 Min IS 1448 P:6/D 3338 Min 4800 IS 1448 P:3 b) Smoke point, mm, Min OR mm Min 25.0 ISO 3014/P:31 i) Smoke Point,mm, Min and mm Min 19.0 ISO 3014/P:31 ii) Naphthalene, percent v/v, Max. Vol % Max 3.00 P:118

8 6) 7) a) CORROSION Cu strip corrosion for 2 hrs at 100 C Thermal Stability, JFTOT at control Temperature of 260 C Filter pressure differential, mmhg, Max b) Tube Rating, visual 8) CONTAMINANTS a) b) c) Existent gum, mg/100 ml, Max. OR Existent gum with Air, mg /100 ml, Max Water Reaction Interface rating, Max. Micro Separator rating at point of Manufacture Number Not worse than No:1 IS 1448 P : 15 mmhg Max 25 Less than 3, No peacock or Abnormal colour deposits IS 1448 P : 97, ISO 6294 mg/100 ml Max 7 IS 1448 P: 29 Number 1b IS 1448 P :42 i) MSEP without SDA, Min OR Number Min 85 ii) MSEP with SDA, Min Number Min 70 9) CONDUCTIVITY 10) Electrical Conductivity ps/m (at the point,time and temp of delivery to the purchaser) LUBRICITY Wear Scar Diameter, mm max 11) ADDITIVES ps/m mm Range Max 0.85(0.65 Defence) IS 1448 P : 142 ISO 6297 ASTM D 5001 i) ii) Static dissipater additive,mg/l #SDA 450(RDE/A/621),Max Anti oxidant, mg/l #$(RDE/A/609) mg/l Max 3.0 mg/l Range 17-24

9 SPECIFICATION FOR KEROSINE IS C g/ml Report IS 1448, P: 16 2 Colour (Saybolt) Number Min Plus 10 IS 1448 P:14 3 DISTILLATION Percent Recovered below 200 C % Vol Min 20.0 Final Boiling Point (FBP) C Max IS 1448, P: 18 4 Flash point (Abel) C Min 35.0 IS 1448, P: 20 5 Smoke point mm Min 18.0 IS 1448, P: 31 6 BURNING QUALITY - IS 1448, P: 5 Char value mg/kg of oil consumed Bloom on glass chimney, Colour, mg/kg Max Visual Not darker than Grey 7 Acidity, Inorganic mg KOH/g Nil IS 1448, P: 2 8 Total Sulphur % Mass Max Copper Corrosion for 3 hrs at 50 deg. C. Number Not worse than No: 1 - ASTM D 4294/ISO 8754 IS 1448, P: 15

10 SPECIFICATION FOR AUTOMOTIVE DIESEL FUEL (BHARAT STAGE IV) IS Acidity,Inorganic mg KOH/g Nil IS 1448, P: 2 2 Acidity,Total mg KOH/g To Report IS 1448, P: 2 3 Ash % Mass Max 0.01 IS 1448, P: Carbon residue (Ramsbottom) On 10% Residue Note: Winter months: November to February % Mass Max 0.30 IS 1448, P:8 Cetane Number Number Min 51.0 IS 1448, P: 9 / ISO Cetane Index Number Min 46.0 ASTM D Pour Point Copper strip Corrosion for 3 50 deg. C Distillation, % v/v, C C Max 3 C, for winter C Max 15 C, for summer ASTM D 5949/D5950 Not worse than No.1 IS 1448, P: 15 % Vol Min 95.0 ISO Flash Point (Abel/PMC) C Min 35.0/66.0 IS 1448, P: 20/P:21 11 Kinematic Viscosity@ 40 deg. C cst Range 2.0 to 4.5 IS 1448, P: Sediments % Mass - P Total Contamination mg/kg Max 24.0 EN deg. C Kg/m3 Range ASTM D Total Sulphur mg/kg Max 50 ASTM D 5453/D Water content mg/kg Max 200 ISO Cold Filter Plugging Point (CFPP) Lubricity corrected wear scar diameter(wsd 1.4) at 60 C C Max 6 C for winter C Max 18 C for Summer ASTM D 6371 Microns Max 460 ISO /Cor 1 19 Oxidation Stability g/m3 Max 25.0 ASTM D Polycyclic Aromatic hydrocarbons (PAH) % Mass Max 11.0 IP Oxygen Content % Mass Max 0.6 Annex B

11 SPECIFICATION FOR AUTOMOTIVE DIESEL FUEL (HIGH FLASH) IS Acidity,Inorganic mg KOH/gm Nil IS 1448, P: 2 2 Acidity,Total mg KOH/gm Max 0.20 IS 1448, P: 2 3 Ash % Mass Max 0.01 IS 1448, P: Carbon residue (Ramsbottom) On 10% Residue % Mass Max 0.30 IS 1448, P: 8 Cetane Number OR Min 48.0 IS 1448, P: 9 6 Cetane Index Min 46.0 ASTM D Pour Point Copper strip Corrosion for deg. C Distillation, % v/v, recovered: at 350 C at 370 C C C Max 12 C, for winter Max 18 C, for summer Not worse than No.1 % Vol Min 85.0 Min 95.0 IS 1448, P: 10 IS 1448, P: 15 IS 1448, P: Flash Point (PMC) C Min 66.0 IS 1448, P: Kinematic 40 deg. C cst Range 2.0 to 5.0 IS 1448, P: Sediment % Mass Max 0.05 IS 1448,P: deg. C kg/m3 Range IS 1448,P:16 14 Total Sulphur % Mass Max 0.25 ASTM D Water content % Vol Max 0.05 IS 1448,P:40 16 Cold Filter Plugging Point (CFPP) C C Max 6 C for winter Max 18 C for Summer IP Total Sediments mg/100ml Max 1.5 ASTM D 2274

12 SPECIFICATION FOR FURNACE OIL MV2 Grade IS Acidity, Inorganic Mg KOH/gm Nil IS 1448, P: 2 2 Ash % Mass Max 0.1 IS 1448, P: 4 3 Gross Calorific Value Cal/gm Report IS 1448, P: 7 4 Relative 15/15 C g/ml Report IS 1448, P: 32 5 Flash Point (PMC) C Min 66.0 IS 1448, P: 21 6 Kinematic Viscosity at 50 C cst Max 180 IS 1448, P: 25 7 Sediment % Mass Max 0.25 IS 1448, P: 30 8 Total Sulphur % Mass Max 4.0 NOTE: Tests indicated in Sl. No is as per customer requirements. ASTM D 4294 IS 1448,P:33 9 Water content % Vol Max 1 0 IS 1448, P: Pour Point C Report ASTM D Cleanliness Number Report ASTM D Micro Carbon Residue % Mass Report ASTM D Asphaltenes % Mass Report IP Net calorific value Cal/gm Report IS 1448 P:6

13 SPECIFICATION FOR PAVING BITUMEN (VG 30) IS Sl. No. TESTS UNIT REQUIREMENT TEST METHOD 1 Density at 27 C g/ml Report IS 1202 Density at 15 C g/ml Report IS Absolute Viscosity at 60 C poises Range IS 1206(Part 2) 3 Kinematic viscosity at 135 C cst Min 350 IS 1206(Part 3) 4 Flash Point (COC) C Min 220 IS 1448 P: Solubility in Trichloroethylene Penetration at 25 C,100 g,5 sec % Min 99.0 IS : mm Min 45 I S: Softening Point (R&B) C Min 47 I S: Tests on Residue from thin film oven tests/ RTFOT i) Viscosity ratio at 60 C Calculation Max 4.0 IS 1206(Part 2) ii) Ductility at 25 C, cm, after Rotating thin film oven test cm Min 40 IS 1208

14 SPECIFICATION FOR PAVING BITUMEN (VG 10) IS Density at 27 C g/ml Report IS 1202 Density at 15 C g/ml Report 2 Absolute Viscosity at 60 C poises Range IS 1206(Part 2) 3 Kinematic viscosity at 135 C cst Min 250 IS 1206(Part 3) 4 Flash Point (COC) C Min 220 IS 1448, P: Solubility in Trichloroethylene Penetration at 25 C,100 g,5 sec % Min 99.0 IS : mm Min 80 I S: Softening Point (R&B) C Min 40 I S: Tests on Residue from thin film oven tests/ RTFOT i) Viscosity ratio at 60 C Calculation Max 4.0 IS 1206(Part 2) ii) Ductility at 25 C, cm, after Rotating thin film oven test cm Min 75 IS 1208

15 SPECIFICATION FOR PAVING BITUMEN (VG 40) IS Sl. No. TESTS UNIT REQUIREMENT TEST METHOD 1 Density at 27 C g/ml Report IS 1202 Density at 15 C g/ml Report IS Absolute Viscosity at 60 C poises Range IS 1206(Part 2) 3 Kinematic viscosity at 135 C cst Min 400 IS 1206(Part 3) 4 Flash Point (COC) C Min 220 IS 1448 P: Solubility in Trichloroethylene Penetration at 25 C,100 g,5 sec % Min 99.0 IS : mm Min 35 I S: Softening Point (R&B) C Min 50 I S: Tests on Residue from thin film oven tests/ RTFOT i) Viscosity ratio at 60 C Calculation Max 4.0 IS 1206(Part 2) ii) Ductility at 25 C, cm, after Rotating thin film oven test cm Min 25 IS 1208

एमआरप एल ग णव नय ण य गश ल आई.एस एस.उप दन व श:२०१ MRPL QC LABORATORY IS PRODUCTS SPECIFICATION:2018. Page 1 of 16

एमआरप एल ग णव नय ण य गश ल आई.एस एस.उप दन व श:२०१ २०१८ MRPL QC LABORATORY IS PRODUCTS SPECIFICATION:2018 Page 1 of 16 INDIAN STANDARD (IS) SPECIFICATION FOR DOMESTIC PRODUCTS: 2018 S. No Product Name Specification