Tung Xiao Dan Assistant Chemist Mark Tan Section Head Feedstock Evaluation Department
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1 Sample ID : Lab ID : Date : Client : Chim Sao Crude 2014-FED October 2014 Premier Oil Sample Number : Sample Date : Sample Time : Location : 4/4 10/9/ hrs Run Down Reported by : Approved by : Tung Xiao Dan Assistant Chemist Mark Tan Section Head Feedstock Evaluation Department Disclaimer : This report (including any enclosures and attachments) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for which it is provided. Unless we provide express prior written consent, no part of this report should be reproduced, distributed or communicated to any third party. We do not accept any liability if this report is used for an alternative purpose from which it is intended, nor do we owe any duty of care to any third party in respect of this report. The interpretations or opinions expressed represent the best judgement of Intertek Singapore. Intertek holds no responsibility nor makes any warranty, either expressed or implied, regarding the productivity, proper operation, or profitability of any oil, in connection with which this report is used or relied upon for any reason whatsoever. Our Accreditation are as follows: SAC Singlas ISO 17025:2005 : Chemical and Biological Testing (Cert No: LA A) SAC Singlas: Environmental Testing (Cert No: LA F) LRQA ISO 9001:2000 Certification (Cert No: SNG )
2 Table of Content Section 1. Properties of Whole Crude Page 3 2. Distillation Yield Data and Curves 2.1 Distillation %mass Yield and %volume Yield Data Graph of Cumulative % yield against Temperature, C AET Graph of Cumulative Middle %volume against API Gravity, API Simulated Distillation Data 2.5 Graph of True Boiling Point against Graph of HTSD Assay Summary.. 4. Properties of Cuts 4.1 LPG Naphtha Kerosene Gas Oil VGO Residue Atmospheric Distillation (D86) Report Detailed Hydrocarbon Analysis FED Chim Sao Crude Assay Report.xls Page 2
3 Properties of Crude Sample ID Lab ID Client ID Date Chim Sao Crude 2014-FED Premier Oil 01 October 2014 Test Method Result Unit C kg/l Specific F D API Gravity 42.1 API Arsenic ICPMS <10 wt.ppb Asphaltenes IP143 <0.50 %m/m Carbon Residue - Micro D %m/m Characterisation Factor UOP Chloride - Organic UOP779 <2.0 wt.ppm Flash Point D56 <0 C Gross Calorific Value D MJ/kg Hydrogen Sulphide UOP163 <1 wt.ppm Kinematic C D cst Kinematic C D cst Kinematic C D445 NA 1 cst Mercury Content UOP wt.ppb Metal - Calcium ICPES <3 wt.ppm Metal - Iron ICPES <2 wt.ppm Metal - Lead ICPES <1 wt.ppm Metal - Nickel ICPES 1 wt.ppm Metal - Sodium ICPES 11 wt.ppm Metal - Vanadium ICPES <1 wt.ppm Nitrogen - Total D wt.ppm Pour Point - Upper D C Reid Vapour Pressure D323A (mod) 5.20 psi Salt Content D Ib/1000bbl Sulphur - Total D %mass Total Acid Number D664A <0.05 mg KOH/g Water and Sediment D %volume Wax Content UOP %mass NA 1 - Unable to perform due to sample nature. Test was done at alternative temperature FED Chim Sao Crude Assay Report.xls Page 3
4 Distillation %mass Yield and %volume Yield Cut Range C LPG C %mass Cumulative Cumulative Specific Gravity %volume %mass F Water removed during distillation - 48ml (0.32vol%) Data is based on dewatered sample (Dry Crude) 2014-FED Chim Sao Crude Assay Report.xls Page 4
5 Temperature, C AET Graph of Cumulative % yield against Temperature, C AET Temperature Cumulative Cumulative C AET %mass %volume Cumulative % yield Graph of Cumulative %mass against AET, C Graph of Cumulative %volume against AET, C 2014-FED Chim Sao Crude Assay Report.xls Page 5
6 Graph of Cumulative Middle %volume against API Gravity, API API Gravity, API Temperature API Gravity Cumulative C AET API Middle %volume Cumulative Middle %volume 2014-FED Chim Sao Crude Assay Report.xls Page 6
7 C < <36 < Temperature %mass Temperature C C Simulated Distillation Data %mass <36 %mass IBP Temperature FED Chim Sao Crude Assay Report.xls Page 7
8 %mass Graph of True Boiling Point against Graph of HTSD Temperature Temperature %mass C C %mass 1 #REF! #REF! 0 #REF! #REF! #REF! 0 #REF! #REF! #REF! 0 #REF! #REF! #REF! 0 #REF! #REF! #REF! #REF! #REF! #REF! #REF! #REF! #REF! #REF! #REF! Temperature C #REF! #REF! Temperature, C AET Cumulative %mass TBP HTSD 2014-FED Chim Sao Crude Assay Report.xls Page 8
9 Sample ID Lab ID Client ID Date Chim Sao Crude 2014-FED Premier Oil 01 October 2014 Whole LPG C5-95 C Cut Range Test Method Unit Mass Yield %mass D2892 / D5236 Volume Yield %volume C kg/l D5002/ D4052/ Specific F D2598 API Gravity API Aniline Point D611 C Arsenic ICPMS wt.ppb <10 Ash D482 %mass <0.001 <0.001 < Asphaltenes IP143 %m/m <0.50 <0.50 <0.50 <0.50 <0.50 Carbon Residue - Micro D4530 %m/m 1.18 < Cetane Index D4737 (Proc.A) Characterisation Factor UOP Chloride - Organic UOP779 wt.ppm <2.0 Cloud Point D2500 C Cold Filter Plugging Point IP309 C Colour - ASTM D L D8.0 Colour - Saybolt D Copper Corrosion D130-1a 1a 1a 1a DHA - Paraffins D6730 %mass DHA - Olefins D6730 %mass <0.1 <0.1 <0.1 DHA - Naphthenes D6730 %mass DHA - Aromatics D6730 %mass DHA - Unknowns D6730 %mass < FIA - Aromatics D1319 %volume Flash Point D56/ IP170/ D93A C < Freeze Point D5972 C < Gross Calorific Value D240 MJ/kg Hydrogen Sulphide UOP163 wt.ppm <1 Kinematic C D445 cst Kinematic C D445 cst Kinematic C D445 cst Kinematic C D445 cst NA Kinematic C D445 cst Mercury Content UOP938 wt.ppb 42.0 Metal - Calcium ICPES wt.ppm <3 <3 <3 <3 4 Metal - Iron ICPES wt.ppm <2 <2 <2 <2 8 Metal - Lead ICPES wt.ppm <1 <1 <1 <1 <1 Metal - Nickel ICPES wt.ppm 1 <1 <1 <1 8 Metal - Sodium ICPES wt.ppm 11 <1 <1 <1 85 Metal - Vanadium ICPES wt.ppm <1 <1 <1 <1 <1 Naphthalenes D1840 %volume Nitrogen - Total D4629/ D5762 wt.ppm 320 <1 <1 <1 <1 < Octane Number - Research Calculation Octane Number - Motor D NA 2 Octane Number - Research D NA 2 PNA - Paraffins D5443 Ext %mass PNA - Naphthenes D5443 Ext %mass PNA - Aromatics D5443 Ext %mass PNA - High Boiling D5443 Ext %mass 0.49 Pour Point - Upper D5853 C +33 Pour Point D97 C Reid Vapour Pressure D323A (mod) psi 5.20 Reid Vapour Pressure D323A psi Refractive C D NA 3 Salt Content D3230 Ib/1000bbl 11 Smoke Point D1322 mm Softening Point D36 C NA Sulphur - Mercaptan D3227 wt.ppm <3 <3 <3 <3 <3 <3 Sulphur - Total D4294 %mass <0.0016<0.0016<0.0016<0.0016< Total Acid Number D3242/ D974/ D664A mg KOH/g < <0.05 <0.05 <0.05 <0.05 Water and Sediment D4007 %volume 0 Wax Content UOP46 %mass 22.4 Note : NA 1 - Unable to perform due to sample nature. Test was done at alternative temperature. NA 2 - Insufficient cut yield to perform test. NA 3 - Colour ASTM >4.0, not applicable for D1747. NA 4 - Unable to perform, out of method scope C C C C C C C C C + C 2014-FED Chim Sao Crude Assay Report.xls Page 9
10 Sample ID Lab ID Cut Range Date Chim Sao Crude 2014-FED LPG 01 October 2014 Test Method Result Unit Mass Yield 1.7 %mass D2892 Volume Yield 2.2 %volume C kg/l Specific F D API Gravity API Ethane Propane n-butane Isobutane D2421 / D2598 / n-pentane D %mass Isopentane ,2-dimethylpropane C FED Chim Sao Crude Assay Report.xls Page 10
11 Sample ID Lab ID Client ID Date Test Chim Sao Crude 2014-FED Premier Oil 01 October 2014 Method Unit Naphtha C5-95 C C C Mass Yield %mass D2892 Volume Yield %volume C kg/l Specific F D API Gravity API Colour - Saybolt D DHA - Paraffins D6730 %mass DHA - Olefins D6730 %mass <0.1 <0.1 <0.1 DHA - Naphthenes D6730 %mass DHA - Aromatics D6730 %mass DHA - Unknowns D6730 %mass < Flash Point IP170 C 26.5 Freeze Point D5972 C <-60 Kinematic C D445 cst Nitrogen - Total D4629 wt.ppm <1 <1 <1 Octane Number - Research Calculation Octane Number - Motor D NA 2 Octane Number - Research D NA 2 Reid Vapour Pressure D323A psi Smoke Point D1322 mm 25.5 Sulphur - Mercaptan D3227 wt.ppm <3 <3 <3 Sulphur - Total D4294 %mass < < < Total Acid Number D3242 mg KOH/g Note : NA 2 - Insufficient cut yield to perform test FED Chim Sao Crude Assay Report.xls Page 11
12 Sample ID Lab ID Client ID Date Test Chim Sao Crude 2014-FED Premier Oil 01 October 2014 Method Unit Kerosene C C Mass Yield %mass D2892 Volume Yield %volume C kg/l Specific F D API Gravity API Aniline Point D611 C Cetane Index D4737 (Proc.A) Colour - Saybolt D Copper Corrosion D130-1a 1a FIA - Aromatics D1319 %volume 9.2 Flash Point IP170 C Freeze Point D5972 C Kinematic C D445 cst Naphthalenes D1840 %volume Nitrogen - Total D4629 wt.ppm <1 <1 PNA - Paraffins D5443 Ext %mass PNA - Naphthenes D5443 Ext %mass PNA - Aromatics D5443 Ext %mass PNA - High Boiling D5443 Ext %mass 0.49 Smoke Point D1322 mm Sulphur - Mercaptan D3227 wt.ppm <3 <3 Sulphur - Total D4294 %mass < < Total Acid Number D3242 mg KOH/g FED Chim Sao Crude Assay Report.xls Page 12
13 Sample ID Lab ID Client ID Date Chim Sao Crude Gas Oil 2014-FED Premier Oil 01 October 2014 Test Method Unit C C Mass Yield %mass D2892 Volume Yield %volume C kg/l Specific F D API Gravity API Aniline Point D611 C Cetane Index D4737 (Proc.A) Cloud Point D2500 C Cold Filter Plugging Point IP309 C Colour - ASTM D L0.5 Colour - Saybolt D Copper Corrosion D130-1a 1a FIA - Aromatics D1319 %volume 10.0 Flash Point D93A C Freeze Point D5972 C Kinematic C D445 cst Naphthalenes D1840 %volume 5.52 Nitrogen - Total D4629 wt.ppm Pour Point D97 C Refractive C D Smoke Point D1322 mm 24.5 Sulphur - Mercaptan D3227 wt.ppm <3 Sulphur - Total D4294 %mass Total Acid Number D3242/ D974 mg KOH/g FED Chim Sao Crude Assay Report.xls Page 13
14 Sample ID Lab ID Client ID Date Test Chim Sao Crude 2014-FED Premier Oil 01 October 2014 Method Unit Vacuum Gas Oil C C C Mass Yield %mass D5236 Volume Yield %volume C kg/l Specific F D API Gravity API Aniline Point D611 C Ash D482 %mass <0.001 <0.001 <0.001 Asphaltenes IP143 %m/m <0.50 <0.50 <0.50 Carbon Residue - Micro D4530 %m/m < Colour - ASTM D D8.0 Flash Point D93A C Kinematic C D445 cst Kinematic C D445 cst Kinematic C D445 cst Metal - Calcium ICPES wt.ppm <3 <3 <3 Metal - Iron ICPES wt.ppm <2 <2 <2 Metal - Lead ICPES wt.ppm <1 <1 <1 Metal - Nickel ICPES wt.ppm <1 <1 <1 Metal - Sodium ICPES wt.ppm <1 <1 <1 Metal - Vanadium ICPES wt.ppm <1 <1 <1 Nitrogen - Total D5762 wt.ppm Pour Point D97 C Refractive C D NA 3 Softening Point D36 C NA 4 Sulphur - Total D4294 %mass Total Acid Number D664A mg KOH/g <0.05 <0.05 <0.05 Note : NA 3 - Colour ASTM >4.0, not applicable for D1747. NA 4 - Unable to perform, out of method scope FED Chim Sao Crude Assay Report.xls Page 14
15 Sample ID Lab ID Client ID Date Chim Sao Crude Residue 2014-FED Premier Oil 01 October 2014 Test Method Unit Mass Yield %mass 11.1 D5236 Volume Yield %volume 9.8 C kg/l Specific F D API Gravity API Ash D482 %mass Asphaltenes IP143 %m/m <0.50 Carbon Residue - Micro D4530 %m/m 10.9 Kinematic C D445 cst Kinematic C D445 cst Metal - Calcium ICPES wt.ppm 4 Metal - Iron ICPES wt.ppm 8 Metal - Lead ICPES wt.ppm <1 Metal - Nickel ICPES wt.ppm 8 Metal - Sodium ICPES wt.ppm 85 Metal - Vanadium ICPES wt.ppm <1 Nitrogen - Total D5762 wt.ppm 2100 Softening Point D36 C 70.6 Sulphur - Total D4294 %mass Total Acid Number D664A mg KOH/g < C 2014-FED Chim Sao Crude Assay Report.xls Page 15
16 Distillation Report (ASTM D86) Sample ID Lab ID Client ID Date Chim Sao Crude 2014-FED Premier Oil 01 October 2014 Cut Range C C C C Description C C C C IBP % % % % % % % % % % % % % FBP % vol % vol % vol % vol Total Recovered Residue Loss FED Chim Sao Crude Assay Report.xls Page 16
17 Detailed Hydrocarbon Analysis Boiling Range C Yield mass % vol % C Component mass % vol % n-butane ,2-dimethylpropane i-pentane n-pentane ,2-dimethylbutane cyclopentane ,3-dimethylbutane methylpentane methylpentane n-hexane ,2-dimethylpentane methylcyclopentane ,4-dimethylpentane ,2,3-trimethylbutane benzene ,3-dimethylpentane cyclohexane methylhexane ,3-dimethylpentane ,1-dimethylcyclopentane methylhexane c,3-dimethylcyclopentane t,3-dimethylcyclopentane ethylpentane t,2-dimethylcyclopentane n-heptane methylcyclohexane ,2-dimethylhexane ethylcyclopentane ,5-dimethylhexane ,4-dimethylhexane c,2t,4-trimethylcyclopentane t,2c,3-trimethylcyclopentane toluene FED Chim Sao Crude Assay Report.xls Page 17
18 Boiling Range Yield C mass % vol % C Component mass % vol % Class Summary n-paraffins Iso-Paraffins Naphthenes Aromatics Olefins Unidentified Average Molecular Weight : Relative Density : Vapor Pressure, 8.41 calc. RVP (EPA method) 100F Octane Number (calculated) : Percent Carbon : Percent Hydrogen : FED Chim Sao Crude Assay Report.xls Page 18
19 Totals by Group Type & Carbon Number (in Mass Percent) Paraffins: I-paraffins: Olefins: Naphthenes: Aromatics: Total: C1: C2: C3: C4: C5: C6: C7: C8: C9: C10: C11: C12: C13: Total : Oxygenates : Total C14+ : Unknowns : Grand Total : Totals by Group Type & Carbon Number (in Volume Percent) Paraffins: I-paraffins: Olefins: Naphthenes: Aromatics: Total: C1: C2: C3: C4: C5: C6: C7: C8: C9: C10: C11: C12: C13: Total : Oxygenates : Total C14+ : Unknowns : Grand Total : FED Chim Sao Crude Assay Report.xls Page 19
20 Detailed Hydrocarbon Analysis Boiling Range C Yield mass % vol % Component mass % vol % i-pentane n-pentane ,3-dimethylbutane methylpentane methylpentane n-hexane ,2-dimethylpentane methylcyclopentane ,4-dimethylpentane ,2,3-trimethylbutane benzene ,3-dimethylpentane cyclohexane methylhexane ,3-dimethylpentane ,1-dimethylcyclopentane methylhexane c,3-dimethylcyclopentane t,3-dimethylcyclopentane ethylpentane t,2-dimethylcyclopentane n-heptane methylcyclohexane ,2-dimethylhexane ethylcyclopentane ,5-dimethylhexane ,4-dimethylhexane c,2t,4-trimethylcyclopentane ,3-dimethylhexane t,2c,3-trimethylcyclopentane ,3,4-trimethylpentane toluene ,3-dimethylhexane methyl-3-ethylpentane methylheptane methylheptane methyl-3-ethylpentane ,4-dimethylhexane FED Chim Sao Crude Assay Report.xls Page 20
21 Boiling Range C Yield mass % vol % Component mass % vol % 1c,2c,4-trimethylcyclopentane methylheptane c,2t,3-trimethylcyclopentane t,4-dimethylcyclohexane ,1-dimethylcyclohexane ,2,5-trimethylhexane c-ethylmethylcyclopentane t-ethylmethylcyclopentane t-ethylmethylcyclopentane ,1-methylethylcyclopentane t,2-dimethylcyclohexane n-octane i-propylcyclopentane N ,3,4-trimethylhexane N N c,2-dimethylcyclohexane ,3,5-trimethylhexane ,1,4-trimethylcyclohexane ,2,3-trimethylhexane ,4-dimethylheptane ,4-dimethylheptane n-propylcyclopentane *1c,3c,5-trimethylcyclohexane ,5-dimethylheptane ,6-dimethylheptane ,1,3-trimethylcyclohexane N ethylbenzene c,2t,4t-trimethylcyclohexane I ,3-dimethylbenzene ,4-dimethylbenzene ,3-dimethylheptane ,4-dimethylheptane N methyloctane methyloctane FED Chim Sao Crude Assay Report.xls Page 21
22 Boiling Range C Yield mass % vol % Component mass % vol % 1c,2t,3-trimethylcyclohexane ethylheptane methyloctane c,2t,4c-trimethylcyclohexane ,2-dimethylbenzene N N I i-butylcyclopentane N23/t-nonene I n-nonane N i-propylbenzene N i-propylcyclohexane I ,2-dimethyloctane ,4-dimethyloctane ,6-dimethyloctane ,5-dimethyloctane ,3-dimethyloctane n-propylbenzene ,3-methylethylbenzene ,4-methylethylbenzene ,3,5-trimethylbenzene methylnonane ,2,4-trimethylbenzene FED Chim Sao Crude Assay Report.xls Page 22
23 Boiling Range Yield C mass % vol % Component mass % vol % Class Summary n-paraffins Iso-Paraffins Naphthenes Aromatics Olefins Unidentified Average Molecular Weight : Relative Density : Vapor Pressure, 0.60 calc. RVP (EPA method) 100F Octane Number (calculated) : Percent Carbon : Percent Hydrogen : FED Chim Sao Crude Assay Report.xls Page 23
24 Totals by Group Type & Carbon Number (in Mass Percent) Paraffins: I-paraffins: Olefins: Naphthenes: Aromatics: Total: C1: C2: C3: C4: C5: C6: C7: C8: C9: C10: C11: C12: C13: Total : Oxygenates : Total C14+ : Unknowns : Grand Total : Totals by Group Type & Carbon Number (in Volume Percent) Paraffins: I-paraffins: Olefins: Naphthenes: Aromatics: Total: C1: C2: C3: C4: C5: C6: C7: C8: C9: C10: C11: C12: C13: Total : Oxygenates : Total C14+ : Unknowns : Grand Total : FED Chim Sao Crude Assay Report.xls Page 24
25 Detailed Hydrocarbon Analysis Boiling Range C Yield mass % vol % Component mass % vol % n-heptane methylcyclohexane ,2-dimethylhexane ethylcyclopentane ,5-dimethylhexane ,4-dimethylhexane c,2t,4-trimethylcyclopentane ,3-dimethylhexane t,2c,3-trimethylcyclopentane toluene ,3-dimethylhexane methylheptane methylheptane ,4-dimethylhexane c,3-dimethylcyclohexane methylheptane c,2t,3-trimethylcyclopentane t,4-dimethylcyclohexane ,1-dimethylcyclohexane ,2,5-trimethylhexane c-ethylmethylcyclopentane t-ethylmethylcyclopentane t-ethylmethylcyclopentane ,1-methylethylcyclopentane t,2-dimethylcyclohexane n-octane i-propylcyclopentane N ,3,4-trimethylhexane N c,2-dimethylcyclohexane ,3,5-trimethylhexane ,2-dimethylheptane ,1,4-trimethylcyclohexane ,2,3-trimethylhexane ,4-dimethylheptane ,4-dimethylheptane n-propylcyclopentane *1c,3c,5-trimethylcyclohexane ,5-dimethylheptane FED Chim Sao Crude Assay Report.xls Page 25
26 Boiling Range C Yield mass % vol % Component mass % vol % 2,6-dimethylheptane ,1,3-trimethylcyclohexane N ethylbenzene c,2t,4t-trimethylcyclohexane I I ,3-dimethylbenzene ,4-dimethylbenzene ,3-dimethylheptane ,4-dimethylheptane I ethylheptane methyloctane c,2t,3-trimethylcyclohexane ethylheptane methyloctane c,2t,4c-trimethylcyclohexane ,2-dimethylbenzene I N N N I I i-butylcyclopentane N N I n-nonane N i-propylbenzene N i-propylcyclohexane I ,2-dimethyloctane ,4-dimethyloctane N N ,6-dimethyloctane ,5-dimethyloctane FED Chim Sao Crude Assay Report.xls Page 26
27 Boiling Range C Yield mass % vol % Component mass % vol % n-butylcyclopentane N I ,3-dimethyloctane N n-propylbenzene ,6-dimethyloctane methyl-5-ethylheptane N ,3-methylethylbenzene ,4-methylethylbenzene N ,3,5-trimethylbenzene I I methylnonane methylnonane ,2-methylethylbenzene methylnonane ethyloctane methylnonane I ,2,4-trimethylbenzene I i-butylcyclohexane I I22 & I N t-methyl-2-n-propylcyclohexane I i-butylbenzene sec-butylbenzene n-decane ,2,3-trimethylbenzene ,3-methyl-i-propylbenzene ,4-methyl-i-propylbenzene dihydroindene sec-butylcyclohexane ,2-methyl-i-propylbenzene ethylnonane I FED Chim Sao Crude Assay Report.xls Page 27
28 Boiling Range Yield C mass % vol % Component mass % vol % 1,3-methyl-n-propylbenzene ,2-methyl-n-propylbenzene Class Summary n-paraffins Iso-Paraffins Naphthenes Aromatics Olefins Unidentified Average Molecular Weight : Relative Density : Vapor Pressure, 0.01 calc. RVP (EPA method) 100F Octane Number (calculated) : Percent Carbon : Percent Hydrogen : FED Chim Sao Crude Assay Report.xls Page 28
29 Totals by Group Type & Carbon Number (in Mass Percent) Paraffins: I-paraffins: Olefins: Naphthenes: Aromatics: Total: C1: C2: C3: C4: C5: C6: C7: C8: C9: C10: C11: C12: C13: Total : Oxygenates : Total C14+ : Unknowns : Grand Total : Totals by Group Type & Carbon Number (in Volume Percent) Paraffins: I-paraffins: Olefins: Naphthenes: Aromatics: Total: C1: C2: C3: C4: C5: C6: C7: C8: C9: C10: C11: C12: C13: Total : Oxygenates : Total C14+ : Unknowns : Grand Total : FED Chim Sao Crude Assay Report.xls Page 29
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