High Surface Area Silica. High Performance Tread. STRUKTOL SCA 98 (Tetrasulfide)

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1 Producers of Specialty Chemicals Struktol Company of America 1 E. Steels Corners Road P. O. Box 19 Stow, Ohio 9 High Surface Area Silica in High Performance Tread with Next Generation Struktol Process Additives (STRUKTOL CY 8 and STRUKTOL KK 9) and STRUKTOL SCA 98 (Tetrasulfide) Struktol Rubber Lab Project 9 Part 3 Paul Danilowicz Benny Bezilla Phone: (33) Fax: (33) 9887 Technical Services: customerservice@struktol.com

2 Next Generation Struktol Process Additives STRUKTOL KK 9 Blend of fatty acid derivatives DP C Zn % STRUKTOL CY 8 Blend of fatty acid derivatives DP 97C Zn ~8% 1 High Surface Area Silica in High Performance Tread with Next Generation Struktol Process Additives SCA98 (Tetrasulfide) Struktol Rubber Lab Project 9 Part 3 Paul Danilowicz Benny Bezilla Struktol Company of America 1

3 Outline Formulations Mix Spec Mix Data Physical Property Data Conclusions 3 Formulations First Pass 1 3 INGREDIENT MASS MASS MASS MASS MASS DURADENE 71B TAKTENE N SCA 98 Tetrasulfide ZN..... ST ACID PPD SUNDEX 79 ZS PMP KK 9 CY 8 TOTAL

4 Formulations Second Pass 1 3 MB 1 3 MB 3 MB 3 3 MB 3 MB 3 TOTAL Formulations Final Pass 1 3 MB 1 3 MB 3 MB 3 3 MB 3 MB 3 DPG..... CBS..... SULFUR TOTAL

5 Mix Spec First Pass mix spec ( rpm, fill factor 7%) SECONDS ADD RUBBER 3 SECONDS ADD 1/3 SILICA SECONDS ADD 1/3 SILICA 9 SECONDS ADD SILANE, OIL, CARBON BLACK, ADDITIVES AND REST OF SILICA 18 SECONDS OR F RAM LIFT 3 SECONDS OR 3F BRUSH AND SWEEP SECONDS OR 3F DISCHARGE ROTOR SPEED RPM AT DISCHARGE 3 PSI nd pass mix spec for batch rotor speed started at 1 rpm, at 3F changed rotor speed to rpm fill factor 7%) SECONDS ADD all MB 3F AUTO RAM LIFT, CHANGE ROTOR SPEED TO RPM DISCHARGE 7 MINUTES AFTER ROTOR SPEED Mix spec final pass for batch ( % fill factor) SECONDS ADD ALL RUBBER 1 SECONDS ADD CURES SECONDS BRUSH AND SWEEP SECONDS OR F DISCHARGE ROTOR SPEED 77 RAM PRESSURE 3 PSI 7 Mixing Observations Temp ( C) Probe Temp(ºC) Energy (WH) First pass comments BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Significant Reduction in mix energy with Struktol Additives 8

6 Mixing Observations KW Part 3 Mix Data #1 KW # KW #1 Temp # Temp Time (Sec.) Temp. ( C) Mixing Time Reduced with Struktol Additives Mixing Peaks Shifted with Struktol Additives 9 Mixing Observations KW Part 3 Mix Data #1 KW #3 KW #1 Temp #3 Temp Time (Sec.) Temp. ( C) Mixing Time Reduced with Struktol Additives Mixing Peaks Shifted with Struktol Additives

7 KW Mixing Observations 9 Part 3 Mix Data #1 KW # KW #1 Temp # Temp Time (Sec.) Temp. ( C) Mixing Time Reduced with Struktol Additives Mixing Peaks Shifted with Struktol Additives 11 KW Mixing Observations 9 Part 3 Mix Data #1 KW # KW #1 Temp # Temp Time (Sec.) Temp. ( C) Mixing Time Reduced with Struktol Additives Mixing Peaks Shifted with Struktol Additives 1

8 Mixing Observations Temp ( C) Probe Temp(ºC) Energy (WH) Second pass comments Final pass comments BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Rheometer Curves Reduced viscosity and increased cure state with KK 9 1 7

9 Rheometer Curves Reduced viscosity and increased cure state with CY 8 1 Rheometer Curves 1 8

10 Rheometer Data 1 C; 3 arc; range; 3 minutes Tech Pro Min Torque Max Torque Ts T T 9 T Reversion BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Increased cure state and reduced minimum torque with KK 9 and CY 8 17 Mooney Viscosity ML C Aged Mooney Initial Viscosity ML (1+) Initial Viscosity 3 day ML (1+) Initial Viscosity 1 day ML (1+) Initial Viscosity 8 day ML (1+) MS 1 7. BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Decreased viscosity for better processability for KK 9 and CY 8 Better viscosity control with time providing more stable stock storage

11 Mooney Scorch 1 C Min Torque T T 3 Cure Index BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Scorch Safety Doubled with KK 9 CY 8 19 Tensile Data Unaged Cure 1 C Shore A Duro Tensile (MPa) Elongation (%) % Mod. (MPa) % Mod. (MPa) 3% Mod. (MPa) BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Increased Tensile, Elong. and Modulus with KK 9 and CY 8

12 Oven Aged Tensile 7 ºC Sample Shore A Pts. Change Tensile (Mpa) Pct. Change Elong. % Pct. Change % Mod. (Mpa) Pct. Change % Mod. Mpa Pct. change BATCH 1 (Control) BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Better retention of aged properties with KK 9 and CY 8 1 Tear Strength ASTM D Die C N/MM BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr 3ºC ºC Tear Strength better with KK 9 CY 8 11

13 Heat Build Up lb. Weight;.3 Throw; minute test Cure time 1C Duro Temp.3 BATCH (KK 9) phr 7. BATCH 3 (KK 9) phr 7 9. BATCH (CY 8) phr 8. BATCH (CY 8) phr 7.8 Heat Build Up is equivalent 3 MER Tension/Compression/Cylindrical / 1 HZ COMPOUND BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Tan delta/ average of 3 / 3c Tan delta/ average of 3 / c

14 Spiral Mold Flow Cured at 1ºC Cure Weight 1 Weight Weight 3 Average Weight BATCH (KK 9) phr BATCH 3 (KK 9) phr BATCH (CY 8) phr BATCH (CY 8) phr Significantly increased flow for better processability with KK 9 and CY 8 Conclusions Struktol Additives KK 9 and CY 8 Reduced mix energy and mix time. Increased cure state. Better scorch resistance. Higher tensile and modulus. Better tear. Reduced viscosity for better processability/ extrudability (less scrap/workaway).

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