TEST REPORT NO.SL64257 Date: April 14, 2015 Page 1 of 11
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1 TEST REPORT NO.SL64257 Date: April 4, 205 Page of GROSSI SRL V.A. Gramsci onsummano Terme, Pistoia The following sample was (were) submitted and identified by the client as: Sample No. A Sample Description Square Leather Lace in Our code colour for shoe lace Client s reference No. : Buyer End Use : ECCO : Footwear Order No. : - Lot No. : - Style No. : - Season : - Item No. : - Category : - Age Grade : - Production Stage : - anufacturer : - Supplier : - Country of Origin : - Country of Destination : ECCO s Units Sample Receiving Date : April 06, 205 Test Performing Period : April 06 April 4, 205 Overall : PASS
2 TEST REPORT NO.SL64257 Date: April 4, 205 Page 2 of Test s : Please refer to the next page(s). Test Parameters Azo Dyes AP/APEO DFu Extractable Heavy etal PCP, TeCP, TriCP Formaldehyde ph Value Organotin SCCP Total Lead Content Chromium VI after aging Soluble ineral tanning agents Triclosan -methyl-2-pyrrolidone (NP) A Remarks : = F = Fail * = No specified requirement Notes: s on pass/fail are based on the test result from the actual sampling of the received sample(s). Signed for and on behalf of PT. SGS Indonesia. Ellya Santhy Assistant anager Softlines & Hardgoods
3 TEST REPORT NO.SL64257 Date: April 4, 205 Page 3 of Component List / List of aterials Sample aterial Component aterial Color Fiber Type* Remark No. No. A Natural leather Leather Black N/A * This fiber type identification is for the selection of azo dye testing procedure (i.e. EN 4362-/3:202). Type A = Textile contains natural fibers only and/or regenerated fibers exclude the group of acetate. Type B = Textile contains polyester fibers only Type C = Textile contains man-made fibers and/or man-made blended fibers (except polyester fibers)
4 TEST REPORT NO.SL64257 Date: April 4, 205 Page 4 of Test s: Azo Dyes Test ethod: Leather: According to DIN ISO/TS 7234-:202 Analysis was conducted with GC-S/HPLC-DAD. Client s requirement Amines CAS No. 4-Aminobiphenyl Benzidine Chlor-o-toluidine Naphthylamine o-aminoazotoluene nitro-o-toluidine / 2-Amino-4-nitrotoluene Chloroaniline methoxy-m-phenylenediamine / ,4 Diaminoanisole 4,4'-Diaminodiphenylmethane ,3'-Dichlorobenzidine ,3'-Dimethoxybenzidine ,3'-Dimethybenzidine ,4'-methylenedi-o-toluidine / ,3'-Dimethyl-4,4'-diaminodiphenylmethane p-cresidine ,4'-ethylene-bis-(2-chloroaniline) ,4'-Oxydianiline ,4'-Thiodianiline o-toluidine methyl-m-phenylenediamine / ,4-Toluylendiamine 2,4,5-Trimethylaniline aminoazobenzene O-Anisidine ,6 Xylidine ,4 Xylidine Detection Limit = 5 mg/kg (for individual compound) Whenever 4-aminodiphenyl (CAS number ), 2-naphylamine (CAS number ) and 4-methoxy-m-phenylene-diamine (CAS number ) is found, the use of banned azo colorants cannot be reliably ascertained without additional information, e.g. the chemical structure of the colorants used.
5 TEST REPORT NO.SL64257 Date: April 4, 205 Page 5 of In case polyurethane materials are used, e.g. PU foams and coatings and in prints, it cannot be ruled out that certain amines, e.g. 4,4 -methylene-dianiline (DA, CAS number ) and 2,4-toluylen-diamine (TDA, CAS number ) are released from the PU component and not from a banned azo colorant. In case of pigment prints care has to be taken that 4,4 -methylene-dianiline (DA, CAS number ) is not released from a source of banned azo colorants but from e.g. a chemical fixing agent. Remark: Test result for 4-aminoazobenzene (CAS no.: ) is considered as not detected (i.e. <5mg/kg) since both aniline and/or,4-phenylenediamine is not found (i.e. <5mg/kg) by mentioned test method Alkylphenols (AP) & Alkylphenol Ethoxylates (APEO) Test ethod: DIN EN ISO 828:202. Analysis was conducted by HPLC-S. Alkylphenols Nonylphenol (NP) 500 Octylphenol (OP) 500 Nonylphenol Ethoxylate (NPEO) 500 Octylphenol Ethoxylate (OPEO) 500 Detection Limit: AP: 0 mg/kg APEO: 30 mg/kg Total Lead content in substrate material Test ethod : CPSC-CH-E Analysis was conducted by ICP-OES Lead (Pb) 00 ppm = mg/kg Detection Limit: 0 mg/kg
6 TEST REPORT NO.SL64257 Date: April 4, 205 Page 6 of Test s: Dimethyl fumarate Test ethod : DIN CEN ISO/TS 686:202. Analysis was conducted by GC/SD Compounds CAS No. Dimethyl fumarate n.d 0. Detection Limit = 0. mg/kg Extractable Heavy etal Test ethod: With reference to ISO05-E04:2008 solution II, extraction with acidic sweat solution followed by analysis with ICP-OES/ICP-S and UV-VIS for Cr VI. Extractable Heavy etal Client s requirement --- Antimony (Sb) 5.0 Arsenic (As) 0.2 Lead (Pb) 0.8 Cadmium (Cd) 0. Cobalt (Co) 4.0 Copper (Cu) 50 Nickel (Ni) 4.0 ercury (Hg) 0.02 Detection Limit:
7 TEST REPORT NO.SL64257 Date: April 4, 205 Page 7 of Test item(s) Detection Limit Antimony,Sb.0 Arsenic, As 0.2 Lead, Pb 0.2 Cadmium, Cd 0. Cobalt, Co.0 Copper, Cu 5.0 Nickel, Ni 0.5 ercury, Hg 0.02 Chlorinated Phenols Test ethod: odified DIN EN ISO 7070: 2007 with alkaline digestion Analysis was conducted by GC-S Pentachlorophenol (PCP) 0.5 Sum of Tetrachlorophenol (TeCP) 0.5 = not detected Detection limit = 0.05 mg/kg Trichlorophenol Content Test ethod : With reference to DIN EN ISO 7070:2007 with alkaline digestion. Analysis was conducted by GC-S. Trichlorophenol (TCP) 2,4,6-TCP / 2,3,6-TCP / 2,3,5-TCP / 2,4,5-TCP / 2,3,4-TCP / 3,4,5-TCP / Total TCP 0.5 = not detected Detection limit = 0.05 mg/kg (for individual compound)
8 TEST REPORT NO.SL64257 Date: April 4, 205 Page 8 of Free Formaldehyde in Leather Test ethod: With reference to ISO Analysis was performed by HPLC. Compounds Adults Formaldehyde 75 Detection limit = 6 mg/kg ph value in Leather Test ethod: According to DIN EN ISO 4045 Recommended ax. Limit (Leather) ph value Organotins Test ethod: With reference to PD CEN/ISO/TS Analysis was conducted by GC-S. Organotin Tributylin compounds (TBT) Dibutyl tin compounds (DBT).0 onobotyl tin compounds (BT).0 Dioctyltin compounds (DOT).0 Triphenyltin compounds (TPhT).0 Bis (tributyl) tin compounds (TBTO).0 Detection limit = 0.02 mg/kg (for individual compound)
9 TEST REPORT NO.SL64257 Date: April 4, 205 Page 9 of Short Chain Chlorinated Paraffin (SCCP) Test ethod : In prdin EN ISO 829:202. Analysis was performed by GC-ECD. Short Chain Chlorinated Paraffin (SCCP) Client s Requirement = Not detected * = exceeds the limit Detection Limit = 50 mg/kg Chromium VI after aging* Test ethod: Chromium (VI) With reference to ISO Analysis was performed by UV/VIS Spectrometry (Aging condition at 80 for 24 hour at <20% relative humidity before Cr(VI) determination). PASS mg/kg = ppm Detection Limit = 3 ppm Client s Limit: < 3 ppm Soluble ineral Tanning Agents* Test ethod: With reference to EN ISO Determination by using ICP-AES. Aluminum (Al) Chromium (Cr) Titanium (Ti) Zirconium (Zr) Sum Al, Cr, Ti, Zr 2.02 ppm 23 ppm ppm PASS Detection Limit : Al, Ti, Zr = ppm; Cr = 0.5 ppm mg/kg = ppm Client s Limit: Sum <50 ppm (Children s product under 36 months) Sum <200 ppm (Adults)
10 TEST REPORT NO.SL64257 Date: April 4, 205 Page 0 of Triclosan* Test ethod : Solvent extraction. Analysis was conducted by GC/S. Triclosan PASS Detection Limit = 2 ppm mg/kg = ppm Client s Limit: <50 ppm -ethyl-2-pyrrolidone (NP)* Test method: Headspace GC/S. NP PASS Detection Limit = 0 ppm mg/kg = ppm Client s Limit: < 500 ppm Remark* = The captioned test is conducted by SGS Taiwan, test report number: KE/205/402, dated at April 08.
11 TEST REPORT NO.SL64257 Date: April 4, 205 Page of Sample Picture **********End of Report**********
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