REBCO (RUSSIAN EXPORT BLEND CRUDE OIL) SPECIFICATION GOST

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1 REBCO (RUSSIAN EXPORT BLEND CRUDE OIL) SPECIFICATION GOST Characteristics Units Result Test Method Density (Specific 20 C g /sm ASTM D5002 Sulphur Content wt.% 1.8 ASTM D4294 Paraffin Content % 1.8 ASTM D5443 Water & Sediment Content vol. % 1.2 ASTM D4007 Distillated recovered % ASTM 200 C 300 C 350 C 50.0 Chlorine Salt Content mg/dm ASTM D3230 Density API API 32.0 ASTM D5002 Salts Content as NaCl mg /l 17.3 ASTM D3230 Ash Content wt.% 0.05 ASTM D482 Mercaptans mg/kg <1 ASTM D3227 Pour Point C 15 ASTM D5863 Kinematic Viscosity 20 C mm 2 /s 4.92 ASTM D455 Hydrogen Sulfide mg/kg <1 ASTM D3227 Asphaltenes % 0.9 ASTM D6560 Nitrogen mg /l 342 ASTM D4629 KOH Number mg/g 0.39 ASTM D

2 BASRA LIGHT CRUDE OIL SPECIFICATION (BASRA OIL COMPANY - IRAQ) Characteristics Units Result Test Method Specific 15.6 C ASTM D5002 API Gravity API ASTM D5002 Kinematic 10 C mm 2 /s 15.0 ASTM D455 Water & Sediment Content vol. % 0.2 ASTM D4007 Pour Point C -35 ASTM D5863 Reid Vapor 37.8 C psi 4.0 ASTM D323 Sulphur Content (Total) wt.% ASTM D4294 Salts as NaCl mg /l <8 ASTM D3230 Carbon Residue wt.% 3.5 ASTM D189 Water Content vol. % 4.0 ASTM D4006 Asphalt Content wt.% 1.0 ASTM D6560 Ash Content wt.% 4.5 ASTM D482 Vanadium Content mg/kg 28.5 ASTM D5863 Nickel Content mg/kg 12.5 ASTM D5863 Iron Content mg/kg 1.0 ASTM D5863 Copper Content mg/kg < 0.1 ASTM D5863 ASTM Distillation I.B.P.C. (deg) 3.7 ASTM C 100 C 200 C 250 C 300 C 45.0 If the specification of the product as per inspection for Iraqi Basra Light Grade fails to conform with the light Crude Oil specification, as agreed to in the contract, the price per barrel shall decrease by USD 0.02 (two US Cents) for each 1/10th (one tenth) of a percent above 0.15% wt., Sulphur for the Сrude Oil. Note: All specifications are as obtained with Basra Crude

3 KIRKUK LIGHT CRUDE OIL SPECIFICATION (NORTH OIL COMPANY - IRAQ) Characteristics Units Result Test Method Specific 15.6 C ASTM D5002 API Gravity API 35.9 ASTM D5002 Kinematic Viscosity, 21.1 C mm 2 /s ASTM D455 Kinematic Viscosity, 38.8 C mm 2 /s ASTM D455 Kinematic Viscosity, 48.9 C mm 2 /s ASTM D455 Kinematic Viscosity, 60.0 C mm 2 /s ASTM D455 Water & Sediment Content vol. % 0.02 ASTM D4007 Pour Point C -27 ASTM D5863 Reid Vapor 37.8 C psi 5.5 ASTM D323 Sulphur Content (Total) wt.% 1.9 ASTM D4294 Salts as NaCl mg /l <5 ASTM D3230 Carbon Residue wt.% 3.2 ASTM D189 Water Content vol. % 0.02 ASTM D4006 Asphalt Content wt.% 1.1 ASTM D6560 Ash Content wt.% ASTM D482 Vanadium Content mg/kg 28.5 ASTM D5863 Nickel Content mg/kg 12.5 ASTM D5863 Iron Content mg/kg 1.0 ASTM D5863 Copper Content mg/kg < 0.1 ASTM D5863 Characterization Factor K(UOP or Watson) 12.0 ASTM D2501 ASTM Distillation 50 C 75 C 100 C 125 C 150 C 175 C 200 C 225 C 250 C 275 C 300 C 53.0 Total Distillate 54.0 Residue Distillation Loss 1.86 ASTM D a

4 UPPER ZAKUM CRUDE OIL SPECIFICATION (ANDOC UAE) Description of Tests Method Unit Result Density at 15 o C ASTM D5002 g/cm Specific Gravity at 60/60 o F Calculation API Gravity at 60 o F Calculation o API Sulphur ASTM D4294 Wt % 1.95 Mercaptan Sulphur UOP 163 wppm 31 Hydrogen Sulphide UOP 163 wppm <1 Total Acid Number ASTM D664 mgkoh/g 0.02 Salt Content as NaCl ASTM D3230 lbs/1000 Bbl 5 Water & Sediment (BS&W) ASTM D4007 Vol % <0.05 Water Content by Distillation IP 74 Vol % <0.05 Sediment by Extraction ASTM D473 Vol % 0.02 Reid Vapor 100 o F ASTM D323 psi 8.3 Kinematic o F ASTM D445 cst 9.87 Kinematic 100 o F ASTM D445 cst 6.32 Pour Point ASTM D97 o C -18 Wax Content UOP 46 wt% 3.8 Asphalthenes IP 143 Wt % 1.46 Total Nitrogen ASTM D3228 wppm 890 Carbon Residue - Micro ASTM D4530 wt% 5.07 Ash ASTM D482 Wt % Nickel ASTM D5863 wppm 12 Vanadium ASTM D5863 wppm 13 Lead ASTM D5863 wppm <1 Iron ASTM D5863 wppm 1 Mercury Cold Vapor wppb <1 Arsenic UOP 387 wppb <5

5

6 SPECIFICATIONS FOR DIESEL FUEL EN PPM PROPERTY UNIT VALUE Test Method Cetane Index Calc. 46 Min EN ISO 4264 Cetane Number CN 51 Min EN ISO 5165 EN Density 15 C Kg/M Min/Max EN ISO 3765 EN ISO Polycyclic Aromatics %m/m 8.0 Max EN Sulphur Content mg/kg 10.0 Max EN ISO EN ISO Flash Point deg. C >55 Min EN ISO 2719 Carbon Residue % Mass 0.30 Max EN ISO Ash Content % Mass Max EN ISO 6245 Water Content mg/kg 200 Max EN ISO Total Contaation- mg/kg 24 Max EN Particulate Matter Copper Strip Corrosion Class 1 Max EN ISO 2160 (3hrs@50 deq. C Oxidation Stability g/m3 25 Max EN ISO Lubricity Microns 460 Max EN ISO C cst Min/Max EN ISO 3104 Distillation: EN ISO 3405 % Recovered 250 deg. C % Vol 65.0 Max EN ISO 3405 % Recovered 350 deg. C % Vol 85.0 Min EN ISO % deg. C Max EN ISO 3405 Fatty Acid Methyl Ester % Vol 7.0 Max EN (FAME) Content Cloud Point deg. C Winter -5 Max EN 23015

7 SPECIFICATION OF RUSSIAN AVIATION KEROSENE COLONIAL GRADE 54 JET FUEL (TS-1) GOST PROPERTY UNIT RESULT TEST-IP METHOD ASTM ADDITIVES Antioxidant in hydro processed fuel Antioxidant non hydro processed fuel Static dissipater first doping ASA-3 Stadis 450 COMBUSTION PROPERTIES Specific energy, net Smoke point Luomitter number Naphthalene s COMPOSITION Total Acidity Aromatics Sulphur, Total Sulphur, Mercaptan Doctor, test VOLATILITY Initial Boiling Point 10% vol at C 20% vol at C 50% vol at C 80% vol at C End point Recovered residuals Loss Flash Point mg/i mg/i mg/i mg/i mj/kg mm % vol mg KOH/g % vol %mass %mass Centigrade Centigrade % vol % vol Centigrade kg/m 2 / / 17/ Report 240 Report Report Report / / /385 D4808 D1322 D1740 D1840 D3242 D1318 D1266/2 D3227 D4952 D96 D56/382 D1298 Density at 15 C LOW TEMPERATURE Freezing Point Centigrade D2256 CORROSION Corrosion, copper (2hrs at 100C) Corrosion, silver (4hrs at 50C) STABILITY Thermal stability control, Temp. 280C Filter pressure, differential Tube deposit rating (visual) CONTAMINATIONS Existent Gum Water reaction, interface rating Fuel with static dissipater additives Fuel without static dissipater additive mm/hg mg/100ml CONDUCTIVITY Electrical conductivity p3/m Report < D130 D361 D1084 D3648

8 SPECIFICATION OF RUSSIAN AVIATION KEROSENE TYPE JET A1 GOST COMPONENT UNIT Min/Max Test Methods ASTM / IP / GOST COMPOSITION Appearance C&B (1) Visual Colour, Saybolt Report (2) D156, D6045 Acidity, Total mg KOH/g Max D3242, IP 354 Aromatics vol % Max D1319, IP 156, GOST R Sulphur, Total wt % Max. 0.25, D1266 Sulphur, Mercaptan wt % Max (3) D3227, IP 342, GOST R OR Doctor Test Negative (3) D4952, IP 30 VOLATILITY Distillation Temperature: D86, IP % Recovery C Max % Recovery C Report 90% Recovery C Report Final BP C Max Distillation Residue vol % Max. 1.5 Distillation Loss vol % Max. 1.5 Flash Point C Min D56 (4), D3828, IP C kg/m D1298, D4052, IP 160, IP 365, GOST R FLUIDITY Freezing Point 20 C (cst) COMBUSTION C Max (5) Max. 8 D2386, D5972, D 7153, IP 16 Net Heat of Combustion MJ/kg Min (6) D3338, D4529, D4809 Smoke Point mm Min. 25 D1322, IP 57 OR Smoke Point mm Min. 19 D1322, IP57 AND Naphthalenes vol % Max. 3 D1840 CORROSION Copper Strip 100 C) THERMAL STABILITY Max. No.1 D130, IP 154

9 JFTOT 260ºC (mm Hg) Tube Rating (Visual) CONTAMINANTS Max. 25 Max. <3 (7) D3241, IP 123 Existent Gum Max. 7 (8) D381, IP 131 Water Reaction Interface Rating Max. 1b D1094 MSEP Rating Fuel without SDA Min. 85 Fuel with SDA Min. 70 Particulates mg/dm 3 Max. 1.0 (2) D5452, IP423 OTHER Conductivity ps/m D2624, IP 274, GOST Without SDA Max. 10 BOCLE Wear Scar Diameter (mm) ADDITIVES Max (9) Antioxidant Optional (24 mg/l ) Static Dissipator Optional (10) Lubricity Improver Optional (11) D5001

10 SPECIFICATIONS OF MAZUT ORIGIN: RUSSIA M-100 GOST COMPONENT UNIT RESULT Ash content, not more % 0.14 Mass fraction of sulphur, not more (low sulphur residual oil) % 0.5 Temperature of the flash, not less (in the closed crucible) 65 (in the open crucible) 110 The temperature of solidification, not higher 25 Kinematics Viscosity 118 Water Content % 0.5 Mechanical Impurities % Lower than 0.1 Acidity mg KOH/ 100ml Lower than 5 Alkalinity nil Gross Calorific Value Kcal/kg / KJ/kg 9200 / Density at 15.0 deg. C Kg/l Hydrogen Sulfide Content (H2S) ppm 0.5 Carbon Residual % Lower than 7 Vanadium ppm 23 Aluium ppm 5 Silikon ppm 12 Nickel ppm 29 Asphaltenes m/m 3.6% mm Hg Extracted to 760 mm Hg Initial Boiling Point deg. C 216 5% recovered % recovered % recovered % recovered % recovered % recovered % recovered % recovered 545 Final Boiling point deg. C 550 Percent Recovered vol % 78 Residua vol % 22 Total Nitrogen m/m % Sodium (Na) ppm 15

11 M-100 GOST COMPONENT UNIT RESULT The temperature of solidification, not higher 42.0 Kinematics 80 C not higher, Conditional 16.0 Kinematics 80 C not higher, Kinematical mm 2 /c 118 Kinematics 100 C not higher, Conditional 6.8 Kinematics 100 C not higher, Kinematical mm 2 /c 50 Ash Content, not more Low Ash Mazut % 0.05 Normal Ash Mazut % 0.14 Mechanical Impurities, lower then % 1.0 Water Content, not higher than % 1.0 Water Dissoluble Acids (Alkalinity) Absent Mass fraction of Sulphur, not more % Grade I % 0.5 Grade II % 1.0 Grade III % 1.5 Grade IV % 2.0 Grade V % 2.5 Grade VI % 3.0 Grade VII % 3.5 Temperature of flash in the open crucible, not less than C 110 Gross Calorific Value not less than KJ/Kg Temperature of sodification, not higher than C 25; 42 (for mazut from high paraffin oil) Heat of combustion (the lowest) recalculated for solid fuel, not less than KJ/Kg Grade I, II, III and IV Grade V, VI, VII C kg/m 3 Not standardized, Must be defined

12 SPECIFICATION OF VISCOUS ROAD BITUMEN GRADE OF BND GOST (ORIGIN RUSSIA) Parameter BND 200/300 BND 130/200 BND 90/130 BND 60/90 BND 40/60 The depth of penetration of the needle into the bitumen, C C Softening point ring and ball, C, not less: Extensibility, not less 25 C C ,2 3,5 - Brittleness temperature, C, : Flash Point, C, not less: Adhesion to the marble or sand Change of softening temperature after heating, C, not more: Satisfied according to the control sample Penetration index: Content of water-soluble compounds,%, not more: 0,2 0,2 0,3 0,3 0,3 Packaging Details: Packed in New Steel Drums

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