MATERIAL TEST REPORT/ Q.C. DOCUMENTATION MADE IN CANADA

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1 PRODUCT DESCRIPTION: PUP JOINT 3" 1502 X 3FT NACE NK DATE: MAY C: Mn: Si: Cr: Ni: Mo: Cu: P: S: Sn: V: Al: Yield: 84,000 PSI HB Hardness: 210 BHN Tensile: 105,000 PSI Charpy Temp: -50 ⁰F Elongation: 29.0% Charpy 1: 105 FT.LBS. Reduction: 67.0% Charpy 2: 109 FT.LBS. Charpy 3: 127 FT.LBS. SHELL TEST PRESSURE: 15000PSI DURATION: 3 MIN HEAT# 00A HEAT CODE: M909 MATERIAL: AISI Manufactured in accordance with requirements of API 6A & NACE MR0175 NK PRODUCT DESCRIPTION: PUP JOINT 3" 1502 X 3FT NACE HEAT# 00A HEAT CODE:

2 INTEGRAL PUP JOINT 3'' X 3FT FIG 1502 NACE Date: 2011 June 03-7:07:49 AM Part Number: sqz Part Description: INTEGRAL PUP JOINT 3'' X 3FT FIG 1502 NACE Serial Number: NK-01 TO 05, Job Number: 8423 Test Pressure: 15000PSI Operator: RDI-138 Comments: SHELL TEST Pressure (psi) Minutes

3 PRODUCT DESCRIPTION: WING NUT 3" FIG 1502 DATE: JAN C: Mn: Si: Cr: Ni: Mo: Cu: P: S: Sn: V: Al: Yield: 86,200 PSI HB Hardness: 215 BHN Tensile: 101,700 PSI Charpy Temp: -46 ⁰C Elongation: 25.0% Charpy 1: 36 FT.LBS. Reduction: 73.0% Charpy 2: 72 FT.LBS. Charpy 3: 42 FT.LBS. HEAT# A " ZK " MATERIAL: AISI CONFORMS TO API 6A & NACE MR0175 SHELL TEST PRESSURE: N/A DURATION: N/A PRODUCT DESCRIPTION: WING NUT 3" FIG 1502 HEAT# A " ZK "

4 PRODUCT DESCRIPTION: SEGMENT 3" 1502 DATE: MARCH C: Mn: Si: Cr: Ni: Mo: Cu: P: S: Sn: V: Al: Yield: 92,700 PSI HB Hardness: 19 HRC Tensile: 105,500 PSI Charpy Temp: -50 ⁰F Elongation: 30.0% Charpy 1: 60 FT.LBS. Reduction: 67.0% Charpy 2: 51 FT.LBS. Charpy 3: 54 FT.LBS. SHELL TEST PRESSURE: N/A DURATION: N/A HEAT# A 'GI' MATERIAL: AISI 4140 PRODUCT DESCRIPTION: SEGMENT 3" 1502 HEAT# A 'GI'

5 PRODUCT DESCRIPTION: PUP JOINT 3" 1502 X 3FT NACE NK DATE: MAY C: Mn: Si: Cr: Ni: Mo: Cu: P: S: Sn: V: Al: Yield: 84,000 PSI HB Hardness: 210 BHN Tensile: 105,000 PSI Charpy Temp: -50 ⁰F Elongation: 29.0% Charpy 1: 105 FT.LBS. Reduction: 67.0% Charpy 2: 109 FT.LBS. Charpy 3: 127 FT.LBS. SHELL TEST PRESSURE: 15000PSI DURATION: 3 MIN HEAT# 00A HEAT CODE: M909 MATERIAL: AISI Manufactured in accordance with requirements of API 6A & NACE MR0175 NK PRODUCT DESCRIPTION: PUP JOINT 3" 1502 X 3FT NACE HEAT# 00A HEAT CODE:

6 INTEGRAL PUP JOINT 3'' X 3FT FIG 1502 NACE Date: 2011 June 03-7:07:49 AM Part Number: sqz Part Description: INTEGRAL PUP JOINT 3'' X 3FT FIG 1502 NACE Serial Number: NK-01 TO 05, Job Number: 8423 Test Pressure: 15000PSI Operator: RDI-138 Comments: SHELL TEST Pressure (psi) Minutes

7 PRODUCT DESCRIPTION: WING NUT 3" FIG 1502 DATE: JAN C: Mn: Si: Cr: Ni: Mo: Cu: P: S: Sn: V: Al: Yield: 86,200 PSI HB Hardness: 215 BHN Tensile: 101,700 PSI Charpy Temp: -46 ⁰C Elongation: 25.0% Charpy 1: 36 FT.LBS. Reduction: 73.0% Charpy 2: 72 FT.LBS. Charpy 3: 42 FT.LBS. HEAT# A " ZK " MATERIAL: AISI CONFORMS TO API 6A & NACE MR0175 SHELL TEST PRESSURE: N/A DURATION: N/A PRODUCT DESCRIPTION: WING NUT 3" FIG 1502 HEAT# A " ZK "

8 PRODUCT DESCRIPTION: SEGMENT 3" 1502 DATE: MARCH C: Mn: Si: Cr: Ni: Mo: Cu: P: S: Sn: V: Al: Yield: 92,700 PSI HB Hardness: 19 HRC Tensile: 105,500 PSI Charpy Temp: -50 ⁰F Elongation: 30.0% Charpy 1: 60 FT.LBS. Reduction: 67.0% Charpy 2: 51 FT.LBS. Charpy 3: 54 FT.LBS. SHELL TEST PRESSURE: N/A DURATION: N/A HEAT# A 'GI' MATERIAL: AISI 4140 PRODUCT DESCRIPTION: SEGMENT 3" 1502 HEAT# A 'GI'

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