GUIDELINE FOR GLOVEBOXES THIRD EDITION AGS-G001 February 2007
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1 GUIDELINE FOR GLOVEBOXES THIRD EDITION AGS-G001 February 2007 AMERICAN GLOVEBOX SOCIETY STANDARDS DEVELOPMENT COMMITTEE All Rights Reserved Copyright 2007 No portion may be duplicated without written consent of the American Glovebox Society. ISBN: Extra copies may be requested as follows: American Glovebox Society P.O. Box 9099 Santa Rosa, CA (800) (707) (Fax) ( ) i
2 DISCLAIMER The American Glovebox Society (AGS) Guideline for Gloveboxes,, has been compiled from established practices and member and contributor experiences. Its intended use is strictly as a guide. Its directions may be altered to suit individual applications. The AGS, its membership, and contributors assume no responsibility for any liability arising out of its use or application. ii
3 Table of Contents 1 SCOPE Limitations Purpose SUPPORTING STANDARDS ORGANIZATIONS TERMS AND DEFINITIONS FOR THE PURPOSES OF THIS DOCUMENT SAFETY Design Fabrication Installation Operations Maintenance Decontamination and Decommissioning DESIGN Shell Basic Design Considerations Materials Finish Weld Studs and Fasteners Shell Joints Appurtenances Glove Materials and Systems Transfer Devices Shell Penetrations Fitting Supports and Stands Safety-Related Supports Industrial Supports...38 Glovebag Supports Radiation Shielding Requirements Design Considerations Shielding Guidelines Types of Shielding Shielding Windows Instrumentation and Electrical Considerations Glovebox Pressure Glovebox Filter Pressure Drop Exhaust Duct Airflow Temperature Oxygen Detector Other Atmospheric Monitoring Options...47 iii
4 5.5.7 Electrical Atmosphere Systems Glovebox Atmosphere Glovebox Filter Systems Purification Systems Windows Materials Window Mounting Fire Protection Systems Glovebox Fire Protection Interior Equipment Conveyors and Dollies Cranes, Monorails, and Hoists Tanks and Vessels Piping, Tubing, and Valves Blenders, Mills, and Moving Equipment Furnaces Viewing Systems Instruments Manipulators Human Factors Anthropometry Biomechanical Considerations Gloveports Gloves Illumination Windows Warning Devices Alarms Controls and Displays Maintainability General Testing Final Assembly General Criteria for Leak Testing a Glovebox Leak-Testing Packaging, Loading, Shipping Decontamination and Decommissioning Design Modular Confinement Liquid Transfer Systems Gaps and Crevices Exhaust Filtration Accumulation of Hazardous Materials Materials Decontamination Equipment Removal Modular Shielding Lifting Pipe Drainiage...80 iv
5 5.14 Mockup and Modeling Drawing Packages FABRICATION Design for Manufacturability Glovebox Flatness Seal Surface Window Opening Flatness Window Sizing Window Installation Methods Bolted Flange Connections O-Ring Connections Access and Service Panels Gasketing Material Dimensional Tolerances Glovebox Shell Measurement Techniques Welding Capacitive Discharge Stud Welding Gas Metal Arc Welding (GMAW) Gas Tungsten Arc Welding (GTAW) Plasma Arc Welding (PAW) Routine Weld Repair Glovebag Seam Heat Sealing Cutting and Forming Shearing Plasma Arc Cutting Saw Cutting Laser Cutting Water Jet Cutting Forming Dies and Cold Forming Operations Punching and Notching...90 Nibbling Abrasive Disc Cutting Assembly Weld Inspection Visual Examination Dye Penetrant Examination Radiography Ultrasonic and Eddy Current Personnel Qualifications Welders Inspectors Finishers Layout Finishing Requirements Cleaning Methods...93 v
6 6.8.1 General Mechanical Chemical Shipping Shipping Approval Final Cleaning Packing Package Labeling Lifting Shipping Glovebag Packaging Glovebox Permanent Identification Labeling LININGS INSTALLATION Isolation from Surrounding Activities Site Preparation Receiving and Unpackaging Penetrations Connection of Existing Building Services and Appurtenances Ventilation Installation Installation of Interim Equipment General Preparation and Installation of Glovebags Fire Protection Systems Inspections to Ensure Integrity and Quality Installation Qualification Damage Repair Leak Tests Introduction Glovebox Preparation System Test Differential Pressure Leak Test Method Mass Spectrometer Leak Detector Testing Containment Integrity Testing and Ventilation Flow Characterization Introduction Preparation Material Transfer Integrity Test Glove Changeout Integrity Test Ventilation Flow Characterization Test Post-Test Cleanup OPERATIONS Gloveports Gloves Glove Changes vi
7 9.4 Glovebox Monitoring Airflow Monitoring Differential Pressure Glovebox Flow Rate Oxygen Concentration Operator Awareness Cleaning Periodic Inspections or Certifications Glove Inspection Leak Detection Surveillance Documentation Control of Test Equipment Training for Operator Qualification Training Program Structure Qualifications Review and Audit MAINTENANCE AND RECORDS Procedures General Equipment Removals Replacement of Windows and Window Gaskets Glove Change-out Non-window Gasket Change-out Filter Replacement Glove Change Program Statistical Methodology Environmental Factors Labeling and Documentation Component Labeling Documentation Training for Maintenance Personnel DECONTAMINATION AND DECOMMISSIONING GLOVEBOX FACILITIES Safety Work Environment Planning and Procedures Temporary Contamination Control Gloves, Coveralls, Pads Dosimetry Prejob Survey Glovebox Preparation General Equipment Removal Isolation Waste Categorization Disposal Containers vii
8 Ongoing Work Additional Containment Removable Panels Piping Final Removal Decontamination Glovebox Removal General Contamination Enclosure Monitoring Coatings Internal Openings Packaging Internal Fixtures and Equipment Glovebox Removal Clean The Work Area Dispose of Waste Remove Contamination Enclosure QUALITY ASSURANCE Management Responsibility Quality System Contract Review Design Control Document and Data Control Purchasing General Suspect/Counterfeit Products Control of Customer-Supplied Material Product Identification and Traceability Process Control and Continual Improvement Inspection and Testing Control of Inspection, Measuring, and Test Equipment Inspection and Test Status Control of Nonconforming Product Corrective and Preventative Action and Product Improvement Handling, Storage, Packaging, Preservation, and Delivery Control of Quality Records Quality Audits Training Servicing Statistical Techniques Applicable Standards viii
9 13 REFERENCES APPENDIX A DRAWINGS APPENDIX B EXAMPLE OF A VENDOR EVALUATION PROGRAM B.1 Purpose B.2 Scope B.3 References B.4 Definitions (specific to Appendix B) B.5 Responsibilities B.6 Suggested Procedure B.7 Evaluator Qualifications APPENDIX C AGS-G GLOVEBOX DESIGN CHECKLIST...C-1 APPENDIX D AGS-G GLOVEBOX COMMISSIONING CHECKLIST... D-1 INDEX ix
10 List of Figures FIGURE 5.1. Standing seam joint FIGURE 5.2. Glovebox Glove Dimensions FIGURE 5.3. Glovesleeve installation FIGURE 5.4. Glovebag operation FIGURE 5.5. Bagport ring assembly FIGURE 5.6. Inner bagport ring assembly FIGURE 5.7 Bagport cover assembly FIGURE 5.8. Transfer sleeve configuration FIGURE 5.9. Bagport ring assembly FIFURE 5.11 Removal materials from a continuous flow airlock FIGURE 5.12 Sphincter seal assembly FIGURE Principle of double-door transfer system FIGURE Double-door waste drum system FIGURE Typical bulkhead union with swaged ferrules FIGURE CGB bulkhead feedthrough FIGURE High-integrity push-through. connector FIGURE Service fitting with an O-ring seal FIGURE Typical shielding sandwich FIGURE Typical shielding window FIGURE Inert atmosphere Control System FIGURE Govebox air purification system FIGURE Zipper window assembly FIGURE Clamped window assembly FIGURE Window bolt torquing sequence FIGURE 6.1 Sample nameplate FIGURE 9.1 Data sheet for leak rate test FIGURE 9.2 Glovebox - leak rate calculations FIGURE 10.1 Sample glovebox component labels x
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