High Performance Lithium-Ion Hybrid Capacitors Employing
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1 Supporting Information High Performance Lithium-Ion Hybrid Capacitors Employing Fe 3 O 4 -Graphene Composite Anode and Activated Carbon Cathode Shijia Zhang a,b,1, Chen Li a,b,1, Xiong Zhang a,b*, Xianzhong Sun a, Kai Wang a, Yanwei Ma a,b* a Institute of Electrical Engineering, Chinese Academy of Sciences, Beijing , PR China b University of Chinese Academy of Sciences, Beijing , PR China 1 These authors contributed equally to this work. address: zhangxiong@mail.iee.ac.cn; ywma@mail.iee.ac.cn
2 Figure S-1. Schematic structure of soft packaging LIC. Figure S-2. N 2 adsorption desorption isotherm and BJH model pore size distribution of RGO.
3 Figure S-3. (a) Nitrogen adsorption-desorption isotherm and density function theory (DFT) pore size distribution of AC. (b) Galvanostatic charge-discharge curves of AC at different current densities. (c) Rate performance of AC at different current densities in the voltage range of V. (d-f) Prelithiation processes of full cells; (d) first galvanostatic charge-discharge curve of cathode in the voltage range of V at current density of 50 ma g -1 ; (e) first galvanostatic charge-discharge curves of anode
4 in the voltage range of V at current density of 50 ma g -1. (f) intercalation capacity of lithium ion curves. Figure S-4. Charge-discharge curves of electrodes and LIC at 0.1 and 0.2 A g -1.
5 Figure S-5. Cycling life, coulombic efficiency and charge discharge curves of Fe 3 O 4 -G//AC soft packaging hybrid capacitors with a mass ratio of 1:2.
6 Table S-1. Electrochemical performances of recently published Li-ion hybrid capacitors in organic system. Hybrid System (anode//cathode) Energy density (Wh kg 1 ) Power density (kw kg 1 ) Capacity retention //Cycing number Ref. TiC//PHPNC % 1 at 450 W kg 1 at 35.6 Wh kg -1 //5000 cycles Graphene/Li 4 Ti 5 O 12 //Graphene 95 at 45 W kg 1 3 at 32 Wh kg -1 87% //500 cycles 2 CNT/V 2 O 5 //AC % 3 TiO 2 belt //Graphene Graphene/Li 4 Ti 5 O 12 //AC Li 4 Ti 5 O 12 //carbo n cuboids Fe 3 O 4 /G //graphene at 40 W kg 1 82 at 570 W kg 1 at 6.9 Wh kg Wh kg Wh kg at 150 W kg 1 at 21 Wh kg -1 at 15 Wh kg -1 at 9 Wh kg at 86 Wh kg -1 //10000 cycles 73%, 600 cycles 75% 82% //10000 cycles 70% LiTi 2 (PO 4 ) 3 //AC 14 Wh kg kw kg -1 68% H 2 Ti 6 O 13 //CMK- 3 Nb 2 O //250 cycles 90 Wh kg 1 11 kw kg -1 80% % 9 10 //MSP-20 at 70 W kg 1 at 5 Wh kg -1 m-nb 2 O 5 -C //MSP Wh kg at 15 Wh kg -1 90% 11
7 T Nb 2 O 5 /Graph ene paper//ac 47 at 393 W kg 1 18 at 15 Wh kg -1 93% //2000 cycles 12 Graphene-VN % 13 //carbon at 200 W kg 1 nanorods B-Si/SiO 2 /C//AC 128 at 64 Wh kg % 14 at 1200 W kg 1 at 89 Wh kg -1 //6000 cycles H 2 Ti 12-x Nb x O 25 // AC 24.3 at 1800 W kg at 11.3 Wh kg -1 84% //10000 cycles 15 N-GMCS//PLM G 80 at 152 W kg 1 88 at 32.2 Wh kg -1 93% //4000 cycles 16 Graphite//URGO % 17 at 84 W kg 1 at 85 Wh kg -1 //1000 3D-MnO//CNS % 18 at 83 W kg 1 at 90 Wh kg -1 //5000 NbN//NG % 19 at 100 W kg 1 at 98.4 Wh kg -1 //1000 MnO@GNS//H NC 127 at 125 W kg 1 15 at Wh kg -1 76% // G-MoO 2 // G-MoO at 150 W kg 1 3 at 33.2 Wh kg % // Graphene//graph ene at 141 W kg at 71.5 Wh kg -1 68% // CPIMS900//AC % 23 at 348 W kg 1 at 13.1 Wh kg -1 //5000 MCMB//AC % 24 at 114 W kg 1 at 23.3 Wh kg -1 //1000
8 Figure S-6. Ragone plots comparison between Fe 3 O 4 -G//AC LICs (the mass ratio of anode/cathode is 1:3 and 1:2, respectively) and commercial energy storage devices, calculated by ratio of 35%. References 1. Wang, H.; Zhang, Y.; Ang, H.; Zhang, Y.; Tan, H. T.; Zhang, Y.; Guo, Y.; Franklin, J. B.; Wu, X. L.; Srinivasan, M.; Fan, H. J.; Yan, Q. A High-Energy Lithium-Ion Capacitor by Integration of a 3D Interconnected Titanium Carbide Nanoparticle Chain Anode with a Pyridine-Derived Porous Nitrogen-Doped Carbon Cathode. Adv. Funct. Mater. 2016, 26, Leng, K.; Zhang, F.; Zhang, L.; Zhang, T.; Wu, Y.; Lu, Y.; Huang, Y.; Chen, Y. Graphene-Based Li-Ion Hybrid Supercapacitors with Ultrahigh Performance. Nano Res. 2013, 6, Chen, Z.; Augustyn, V.; Wen, J.; Zhang, Y.; Shen, M.; Dunn, B.; Lu, Y. High-Performance Supercapacitors Based on Intertwined CNT/V 2 O 5 Nanowire Nanocomposites. Adv. Mater. 2011, 23,
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