MATERIAL SPECIFICATION FOR EMULSIFIED ASPHALT

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1 ONTARIO PROVINCIAL STANDARD SPECIFICATION METRIC OPSS 1103 FEBRUARY 1996 MATERIAL SPECIFICATION FOR EMULSIFIED ASPHALT SCOPE REFERENCES Not Used Not Used MATERIALS General.02 Physical Requirements.03 Straw Mulch Adhesive.04 Shipment Not Used Not Used QUALITY ASSURANCE Compliance.02 Inspection.03 Sampling.04 Testing.05 Rejection TABLE OF CONTENTS OWNER PURCHASE OF MATERIAL BY PURCHASE ORDER General.02 Measurement for Payment.03 Basis of Payment DESIGNATED SOURCES REQUIREMENTS Page 1 Rev. Date: 02/1996 OPSS 1103

2 SCOPE This specification covers the requirements for different types and grades of emulsified asphalt suitable for both road construction and as a straw mulch adhesive REFERENCES This specification refers to the following standards, specifications or publications: Ontario Provincial Standard Specification, Construction: OPSS 102 Weighing Materials Ontario Provincial Standard Specification, Material: OPSS 1153 Emulsified Asphalt Patching Material American Society for Testing and Materials, ASTM: ASTM D Sampling Bituminous Materials ASTM D (1990) - Test Methods for Emulsified Bitumens Used As Protective Coating Ministry of Transportation Publications: Laboratory Testing Manual Manual of Designated Sources for Materials MATERIALS General Under no circumstances shall the source of supply or the product be changed, or partial or total supply allocated to another supplier without prior written approval of the Owner Physical Requirements Emulsified asphalts shall consist of suitable paving asphalts dispersed in water and shall meet the requirements specified in Tables I, II, III, VIII, IX and Figure 1. The addition of polymers or other additives after the manufacture of an emulsified asphalt shall not be permitted. Emulsified asphalts and polymer-modified emulsified asphalts shall be homogeneous after mixing and show no signs of separation within 14 days of delivery Straw Mulch Adhesive Emulsified asphalt used as a straw mulch adhesive shall be a specially refined petroleum asphalt emulsified in water, of fluid consistency designed for cold spray applications, containing neither petroleum solvents nor other components toxic to plant life, and shall conform to Table I. Page 2 Rev. Date: 02/1996 OPSS 1103

3 Shipment The material shall be shipped in clean containers. Containers which are being reused shall be inspected, and cleaned if required, prior to loading to ensure there is no contamination. When shipment is by tank truck or railway tank car, the material shall arrive at the destination at a temperature not less than 5 C higher than the minimum spraying temperature and not more than the maximum spraying temperature specified in Table IV QUALITY ASSURANCE Compliance Emulsified asphalts shall conform to Tables I, II, III, VIII, IX and Figure 1 for the particular type and grade when tested in conformance to the test methods designated in the tables Inspection The Owner may, at any time, inspect shipping containers for cleanliness Sampling Representative samples of material being supplied to the Owner may be taken by the Owner in conformance with ASTM D 140 from either the supplier's plant or any shipment Testing Samples may be tested by the Owner conforming to the tests listed in material requirement tables Rejection Failure of any sample to conform to any of the material requirements shall be cause for rejection of thematerial. Rejected materials shall be replaced expeditiously OWNER PURCHASE OF MATERIAL BY PURCHASE ORDER General When the Owner purchases emulsified asphalt with type, grade and destination specified on a purchase order, the Owner Purchase of Material by Purchase Order requirements shall also apply and the emulsified asphalt shall be transported to the contract by the supplier unless otherwise stated on the tender and the purchase order Measurement for Payment The supplier shall measure the emulsified asphalt by weighing the mass in tonnes conforming to OPSS 102, sections , , , and In addition to the requirement of OPSS , the tares of the hauling vehicle shall be determined for each load. Page 3 Rev. Date: 02/1996 OPSS 1103

4 Basis of Payment Payment at the contract price for the tender item Emulsified Asphalt shall be full compensation for all labour, equipment and material for the emulsified asphalt, conforming to the requirements specified herein and identified on the Owner's purchase order, including any sample material taken prior to delivery and the replacement of rejected materials DESIGNATED SOURCES REQUIREMENTS In order for a supplier to be considered for addition to the Manual of Designated Sources for Materials for emulsified asphalts, the supplier shall submit a request in writing to the Manager, Bituminous Section, Engineering Materials Office, Ministry of Transportation, Downsview, accompanied by a minimum 8 litre sample for testing for conformance to subsection The sample shall be accompanied by certified test results. If the sample conforms to this specification and the is satisfied that the supplier has the equipment and ability to produce the material in bulk quantities, then the will list the supplier in the Manual of Designated Sources for Materials. Page 4 Rev. Date: 02/1996 OPSS 1103

5 TABLE I ANIONIC EMULSIFIED ASPHALTS REQUIREMENTS TYPE RAPID SETTING MEDIUM SETTING SLOW SETTING Viscosity, Saybolt Furol Seconds Residue by at 50 C GRADE RS-1 RS-2 MS-1 MS-2 SS-1 SS-1H STRAW MULCH ADHESIVE Min. Max. Min. Max. Min. Max. Min. Max. Min. Max. Min. Max. Min. Max Distillation, % by Mass Settlement, %, 5 days Demulsibility, % 7 days 35 ml, 0.02 N CaCl ml, 0.1 N CaCl 2 Oil Portion of Distillate, (Volume/Mass) % 10 Sieve Text, % by Mass Cement Mixing Test, % by Mass TEST METHOD Particle Charge NEGATIVE OR NEUTRAL Coating Test, % Fire Resistance PASS SEE NOTE Tests on Residue (, g, 5 s), 0.1 mm Ductility (, 5 cm/min) cm Solubility in Trichloroethylene, % by Mass NOTE: FIRE RESISTANCE TEST - There shall be no flash or flame when the flame of a bunsen burner is held in contact with the surface of the material, as received, for a period of 10 seconds. 2.0 LS-219 LS-216 LS-221 LS-2 LS-217 LS-223 LS-222 LS-218 LS-224 LS-0 LS-5 LS-4 Page 5 Rev. Date: 02/1996 OPSS 1103

6 TABLE II CATIONIC EMULSIFIED ASPHALTS REQUIREMENTS TYPE RAPID SETTING MEDIUM SETTING SLOW SETTING SLURRY Viscosity, Saybolt Furol Seconds Residue by at 50 C GRADE CRS-1 CRS-2 CMS-2 CMS-2H CSS-1 CSS-1H CSS-H TEST SEAL Min. Max. Min. Max. Min. Max. Min. Max. Min. Max. Min. Max. Min. Max Distillation, % by Mass Settlement, %, 5 days Demulsibility, % 35 ml, Dioctyl Sodium Sulfosuccinate Solution (0.8%) Oil Portion of Distillate, (Volume/Mass) % Sieve Text, % by Mass Cement Mixing Test, % by Mass Particle Charge POSITIVE Coating Test, % Tests on Residue (, g, 5 s), 0.1 mm Ductility (, 5 cm/min) cm Solubility in Trichloroethylene, % by Mass METHOD LS-219 LS-216 LS-221 LS-2 LS-217 LS-223 LS-222 LS-218 LS-224 LS-0 LS-5 LS-4 Page 6 Rev. Date: 02/1996 OPSS 1103

7 TABLE III HIGH FLOAT EMULSIFIED ASPHALTS REQUIREMENTS TYPE HIGH FLOAT Viscosity, Saybolt Furol GRADE HFRS-2 HF-S HF-150S HF-250S HF-150M *HF-0M TEST Min. Max. Min. Max. Min. Max. Min. Max. Min. Max. Min. Max. Seconds at 50 C Residue by Distillation, % by Mass Demulsibility, % 50 ml 0.1 N CaCl 2 35 ml 0.02 N CaCI 2 60 Oil Portion of Distillate, (Volume/Mass) % Sieve Text, % by Mass Coating Test, (See Note) Pass Pass Pass Note1 Note 1 Storage Stability Test, 24 h, % by Mass Tests on Residue (, g, 5 s), 0.1 mm Ductility (, cm/min) cm 40 Solubility in Trichloroethylene, % by Mass METHOD LS-219 LS-226 LS-216 LS-2 LS-217 LS-223 LS-224 LS-225 LS-226 LS-0 LS Float Test at 60 C, s Viscosity (at 60 C), Pa.s NOTE: Requirements outlined on attached Chart, Figure 1 LS-4 LS-226 LS ** 2 8** 1. Follow LS-224, except that the mixture of aggregate and emulsified asphalt shall be mixed vigorously for 5 min. then allowed to stand for 3 h after which the mixture shall be capable of being mixed an additional 1 min. The mixture shall then be rinsed twice with approximately its own volume of tap water, without showing appreciable loss of bituminous film. After the second mixing the aggregate shall be at least 90% coated. * Stripping and Workability - refer to OPSS 1153, Material Specification for Emulsified Asphalt Patching Materials, Section Quality Assurance. ** Viscosity limits (at 60 C at 1.0s -1 ) shown for mixing grades are tentative. Supplier to advise purchaser before delivery if limits cannot be met. LS-226 Page 7 Rev. Date: 02/1996 OPSS 1103

8 TABLE IV TEMPERATURE FOR SPRAYING AND MIXING EMULSIFIED ASPHALTS C G R A D E S P R A Y I N G M I X I N G Maximum Maximum RS-1, RS-1(P) 30(a) 70 (b) 70 RS-2, RS-2(P) 60(a) 80 MS MS SS SS-1H HFRS HF-S, HF-S(P) HF-150S, HF-150S(P) HF-250S HF-150M, HF-150M(P) HF-0M 40 CRS CRS-2, CRS-2(P) CMS CMS-2H CSS CSS-1H CSS-H (Slurry) 35 Emulsified Asphalt Primer Manufacturer's Requirements (a) For surface treatment. (b) For other uses. Page 8 Rev. Date: 02/1996 OPSS 1103

9 Figure 1 VISCOSITY REQUIREMENTS FOR DISTILLATION RESIDUES FROM HIGH FLOAT EMULSIFIED ASPHALT APPARENT VISCOSITY AT 60 C, Pa-s PENETRATION AT 25 C, g and 5s Page 9 Rev. Date: 02/1996 OPSS 1103

10 Grade of High Float Emulsified Asphalt HF-S HF-150S HF-250S A,B C, D E, F Viscosity shall be above the extrapolated line * designated by specified letters and between penetration limits contained in vertical lines extending upwards from these points. (* See Tables V, VI and VII for acceptable values). Viscosity value shall be reported at the shear rate: 0.5 s -1 for grades HF-S and HF-150S 1.0 s -1 for grade HF-250S Page 10 Rev. Date: 02/1996 OPSS 1103

11 TABLE V MINIMUM APPARENT VISCOSITY, HF-S Pa.s at 0.5 s -1 Pa.s at 0.5 s -1 Pa.s at 0.5 s Note: 1. This table is based on the apparent viscosity of 0 Pa.s at 0.5 s -1 at penetration, and 500 Pa.s at 0.5 s -1 at 1 penetration. Page 11 Rev. Date: 02/1996 OPSS 1103

12 TABLE VI MINIMUM APPARENT VISCOSITY, HF-150S Pa.s at 0.5 s -1 Pa.s at 0.5 s -1 Pa.s at 0.5 s Note: 1. This table is based on the apparent viscosity of 140 Pa.s at 0.5 s -1 at 150 penetration, and 90 Pa.s at 0.5 s -1 at 250 penetration. Page 12 Rev. Date: 02/1996 OPSS 1103

13 TABLE VII MINIMUM APPARENT VISCOSITY, HF-250S Pa.s at 1.0 s -1 Pa.s at 1.0 s Note: 1. This table is based on the apparent viscosity of 50 Pa.s at 1.0 s -1 at 250 penetration, and Pa.s at 1.0 s -1 at 500 penetration. Page 13 Rev. Date: 02/1996 OPSS 1103

14 TABLE VIII POLYMER-MODIFIED EMULSIFIED ASPHALTS REQUIREMENTS TYPE Anionic Cationic High Float Viscosity, Saybolt Furol Seconds at 50 C GRADE RS-1(P) RS-2(P) CRS-2(P) HF-S(P) HF-150S(P) HF-150M(P) TEST METHOD Min. Max. Min. Max. Min. Max. Min. Max. Min. Max. Min. Max LS-219 Residue by Distillation to 4.4 C, % by Mass LS-216 LS-226 Settlement, 24 h, % by Mass LS-221 Demulsibility, % - 35 ml, 0.02 N CaCl 2-35 ml, 0.8% Dioctyl Sodium Sulfo-Succinate Solution - 50 ml 0.1 N CaCl LS-2 Oil Portion of Distillate, (Volume/Mass) % LS-217 Sieve Text, % by Mass LS-223 Particle Charge Negative or Neutral Positive LS-218 Coating Test Pass Pass Note 1 LS-224 Storage Stability, 24 h, % by Mass LS-225 Tests on Residue (, g, 5 s), 0.1 mm LS-0 LS-226 Solubility in Trichloroethylene, % by Mass, Note LS-4 Float Test at 60 C, s LS-226 LS-227 Ash Content, % by Mass of Residue, Note ASTM D 2939 Elastic Recovery, at 10 C, % Force Ductility at 800% Elongation, 5 cm/min. Pull Rate at 4 C, kg 0.5 Notes: LS Note 3 1. Follow LS-224, except that the mixture of aggregate and emulsified asphalt shall be mixed vigorously for 5 min. then allowed to stand for 3 hrs. after which the mixture shall be capable of being mixed an additional 1 min. The mixture shall then be rinsed twice with approximately its own volume of tap water, without showing appreciable loss of bituminous film. After the second mixing the aggregate shall be at least 90% coated. 2. The ash content shall be determined when the manufacturer indicates that the polymer additive is not soluble in trichloroethylene. 3. Current Ministry test method. Page 14 Rev. Date: 02/1996 OPSS 1103

15 TABLE IX EMULSIFIED ASPHALT PRIMER REQUIREMENTS Min. Max. Test Method Viscosity, Saybolt Furol Seconds at 50 C LS-219 Residue by Distillation to 260 C, % by Mass 40 - LS-216 Oil Portion of Distillate, (Volume/Mass) % - Note LS-217 Particle Charge - Note 2 Neutral LS-218 Flash Point, Tag Open Cup, C 45 - ASTM D-1310 Storage Stability, 24 h - Note 3 No visible separation LS-221 Tests on Residue (, g, 5 s), 0.1 mm 300 LS-0 Ductility ( - Note 4, 5 cm/min), cm - LS-5 Solubility in Trichloroethylene, % by Mass LS-4 Notes: 1. Since the total distillate will exceed ml, follow LS-217 with the following modification: Prior to reaching ml of distillate, carefully replace the first ml graduated cylinder with a second one. After the distillation is complete, determine the volume of oil distillate in both cylinders and record the sum. Calculate the oil portion of the distillate as a percentage of the original weight of primer: % Oil = Total Volume of oil distillate, ml x 0 g primer 2. Follow LS-218 with the modification that the asphalt will not deposit due to an electrical charge on either the anode (positive electrode) or the cathode (negative electrode). Equal adherence to both electrodes due to the viscous nature of the material will not be considered deposition. 3. Follow LS-221 except fill only one 500 ml graduated cylinder and examine for visible separation after 24 hours. 4. If the ductility is less than cm, the material will be acceptable if its ductility at 15 C is more than cm. Page 15 Rev. Date: 02/1996 OPSS 1103

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