Ballot Summary and Comments on Revision of API 1509 BOI/VGRA

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1 Ballot Summary and Comments on Revision of API 1509 BOI/VGRA Issued: 10-Jun-11 Closed: 11-Jul-11 Ballot Item 01: Revision of API 1509, APPENDIX K - Pysical and Cemical Ranges for Auditing Company Member Vote Ballot Item 01 1 Afton Dan Pridemore APPROVE 2 BP Castrol Barbara Dennis APPROVE 3 Cevron Mattew Ansari APPROVE 4 ConocoPillips Steve Tarbox N.R. 5 Evonik-RoMax Steve Herzog APPROVE 6 ExxonMobil Tom Olszewski APPROVE W/Comments 7 Infineum Joan Evans APPROVE 8 Lubrizol Gail Evans APPROVE 9 Motiva Greg Raley APPROVE 10 Suncor (Petro-Canada) Luc Girard DISAPPROVE 11 Pinnacle Oil Harji Gill N.R 12 RT Vanderbilt Glenn Mazzamaro APPROVE 13 Safety-Kleen Rodney Walker APPROVE 14 Sell Scott Lindolm APPROVE 15 SK Mike Brown APPROVE 16 Total Lubricants Jim Linden APPROVE 17 Valvoline Tom Smit APPROVE Ballot Item Comments Ballot Item 1: Revision of API 1509, APPENDIX K - Pysical and Cemical Ranges for Auditing Petro-Canada Our disapproval is around HTHS viscosity being tied to ASTM D4683. Disapprove Te HTHS measure tat correlates wit Seq. VID (for resourceconserving) is D6616 wic is run at 100 C. HTHS150 for RC oils sould be. HTHS100 could be added as a separate audit measure for RC oils. We also ave a comment on Foam testing: We would like to see te 1-minute settling requirement explicitly stated, peraps in footnote (b). ExxonMobil Approve w/comments Finally, we point out a simple typo: Te first note under table K-1 as te word measurers, and probably sould read measures Recommend tat te correlation of L38 SS and KO be Re-investigated for newer generation S category oils. Page 1 of 1 1/11/2012

2 API Lubricants Committee Ballot Proposed Revisions to API 1509, 16t Edition, April 2007 PLEASE RETURN BY FACSIMILE ( ) OR TO DENNIS L BACHELDER AT BacelderD@API.org, BY CLOSE OF BUSINESS JULY 11, 2011 Name: Company: Telepone/Fax: Address: A DISAPPROVE VOTE MUST INCLUDE THE (A) SPECIFIC PARAGRAPH, SECTION, OR PART THE NEGATIVE BALLOT PERTAINS TO; (B) SPECIFIC SUBSTANTIVE REASONS FOR THE NEGATIVE; AND (C) PROPOSED WORDING OR ACTION TO RESOLVE THE NEGATIVE. PLEASE ATTACH YOUR COMMENTS ON A SEPARATE SHEET OF PAPER. IF THE API LUBRICANTS COMMITTEE APPROVES ANY OF THE CHANGES, THEY WILL BE EFFECTIVE MAY 5, 2011 OR THE DATE NOTED IN THE BALLOT ITEM, WHICHEVER COMES FIRST. Ballot Item 1: Revision of API 1509, APPENDIX K - Pysical and Cemical Ranges for Auditing Lubricants Group as approved additions and canges in te testing and auditing of oil samples. Te update of Appendix K - Pysical and Cemical Ranges for Auditing formalizes tese canges in API A copy of te updated APPENDIX K- Pysical and Cemical Ranges for Auditing is attaced to tis ballot. Approve Approve wit Comments Disapprove Abstain Comments:

3 APPENDIX K - Pysical and Cemical Ranges for Auditing Table K-1 API After-Market Audit Ranges - Standard Audit Viscosity at 100 C (ASTM D445) Cranking viscosity (ASTM D5293) All oils +10% b Pumping viscosity (ASTM D4684) Pumping yield stress (ASTM D4684) HTHS viscosity (ASTM D4683) API S 1 st / ILSAC Oils c Resource Conserving/ -15%, +10% d API CI-4, CI-4 PLUS & CJ-4 Oils NOACK volatility (ASTM D5800) API S 1 st / ILSAC Oils c As defined in API % e API CH-4, CI-4, CI-4 PLUS & CJ-4 Oils Elements wit publised specification (ICP-D4951) Posporus Sulfur Elements wit no publised specification (ICP (D D5762) f Values 100 parts per million 10%, +15% Values <100 parts per million 15%, +20% Total Base Number (D2896) 10%, +15% Note: HTHS = ig temperature/ig sear, ICP = inductively coupled plasma, D5762 measurers Nitrogen. a ASTM analytical test metod precision will be accounted for wen applying te acceptance range. b Maximum = Part B reported value x 1.10 (+10% tolerance) x (7.3% Reproducibility) or J300 adjusted for Reproducibility, if lower. c Applies to specifications for API SJ, API SL, API SM, API SN, ILSAC GF-4, or ILSAC GF-5, as. d Maximum = Part B reported value x 1.10 (+10% tolerance) x (3.6% Reproducibility) / Minimum = Part B reported value x 0.85 (-15% tolerance) x (-3.6% Reproducibility) or J300 minimum adjusted for reproducibility, if iger. e Maximum = Part B reported value x 1.10 (+10% tolerance) ( Reproducibility) or API 1509 Max Reproducibility, if lower. f Te elements to be reported and audited are tose sown in PART B PRODUCT DATA SHEET provided wit te license application..

4 APPENDIX K - Pysical and Cemical Ranges for Auditing Table K-2 API After-Market Audit Ranges - Expanded Audit Foaming (ASTM D892, all sequences) b Hig temperature foaming (ASTM D6082) Sear stability (D6278) SL, SM & SN oils CH-4 & CI-4 oils Sear stability (D7109) CI-4 PLUS & CJ-4 Oils Ball rust test (D6557) HTCBT (D6594) ROBO (D7528) MRV Only d, e f g i j Note: HTCBT = Hig Temperature Corrosion Benc Test, ROBO MRV Only = ROBO Benc Oxidation Test measuring used oil MRV per D7528 a ASTM analytical test metod precision will be accounted for wen applying te tolerance limits. b Use Option A for API SJ, API SL, API SM, API SN, ILSAC GF-4, and ILSAC GF-5. No Option A for API CH-4, CI-4 & CI-4 PLUS. Option A may be used for API CJ-4. c Added to API SJ, API SL, API SM API SN, ILSAC GF-4, or ILSAC GF-5 specification limits, as d Apply limits outlined in API 1509, Appendix F, Table F-2, Footnote 6. e Non-conformance to limits outlined in API 1509, Appendix F, Table F-2 Footnote 6 leads to a request for licensee to confirm Sequence VIII Stay-in-Grade support. f Refer to API CH-4 or CI-4, as. g Refer to API CI-4 PLUS or CJ-4, as. Refer to API SJ, API SL, API SM, API SN, ILSAC GF-4 or ILSAC GF-5 specifications, as i Refer to API CH-4, CI-4,CI-4 PLUS or CJ-4, as j Refer to API SM, API SN, ILSAC GF-4 or ILSAC GF-5 specifications, as

5 APPENDIX K BALLOT RESOLUTION AMAP Work Group met to develop recommendation for resolving ballot negative related to use of HTHS150 to ceck for VID wit RC oils Factors Considered: Use of HTHS carried forward on principle approved for EC oils Limited to HTHS for RC oils HTHS150 cosen as tis test is normal AMAP test Recognize HTHS100 a stronger correlation wit VID HTHS100 not prevalent in Quality Control operation RECOMMENDATION: Remove HTHS for RC oils from Appendix K Table issue for furter study

6 APPENDIX K - Pysical and Cemical Ranges for Auditing Table K-1 API After-Market Audit Ranges - Standard Audit Viscosity at 100 C (ASTM D445) Cranking viscosity (ASTM D5293) All oils +10% b Pumping viscosity (ASTM D4684) Pumping yield stress (ASTM D4684) HTHS viscosity (ASTM D4683) API S 1 st / ILSAC Oils c Resource Conserving/ Only API CI-4, CI-4 PLUS & CJ-4 Oils -15%, +10% d NOACK volatility (ASTM D5800) API S 1 st / ILSAC Oils c As defined in API % e API CH-4, CI-4, CI-4 PLUS & CJ-4 Oils Elements wit publised specification (ICP-D4951) Posporus Sulfur Elements wit no publised specification (ICP (D D5762) f Values 100 parts per million 10%, +15% Values <100 parts per million 15%, +20% Total Base Number (D2896) 10%, +15% Note: HTHS = ig temperature/ig sear, ICP = inductively coupled plasma, D5762 measurers Nitrogen. a ASTM analytical test metod precision will be accounted for wen applying te acceptance range. b Maximum = Part B reported value x 1.10 (+10% tolerance) x (7.3% Reproducibility) or J300 adjusted for Reproducibility, if lower. c Applies to specifications for API SJ, API SL, API SM, API SN, ILSAC GF-4, or ILSAC GF-5, as. d Maximum = Part B reported value x 1.10 (+10% tolerance) x (3.6% Reproducibility) / Minimum = Part B reported value x 0.85 (-15% tolerance) x (-3.6% Reproducibility) or J300 minimum adjusted for reproducibility, if iger. e Maximum = Part B reported value x 1.10 (+10% tolerance) ( Reproducibility) or API 1509 Max Reproducibility, if lower. f Te elements to be reported and audited are tose sown in PART B PRODUCT DATA SHEET provided wit te license application..

7 APPENDIX K - Pysical and Cemical Ranges for Auditing Table K-2 API After-Market Audit Ranges - Expanded Audit Foaming (ASTM D892, all sequences) b Hig temperature foaming (ASTM D6082) Sear stability (D6278) SL, SM & SN oils CH-4 & CI-4 oils Sear stability (D7109) CI-4 PLUS & CJ-4 Oils Ball rust test (D6557) HTCBT (D6594) ROBO (D7528) MRV Only d, e f g i j Note: HTCBT = Hig Temperature Corrosion Benc Test, ROBO MRV Only = ROBO Benc Oxidation Test measuring used oil MRV per D7528 a ASTM analytical test metod precision will be accounted for wen applying te tolerance limits. b Use Option A for API SJ, API SL, API SM, API SN, ILSAC GF-4, and ILSAC GF-5. No Option A for API CH-4, CI-4 & CI-4 PLUS. Option A may be used for API CJ-4. c Added to API SJ, API SL, API SM API SN, ILSAC GF-4, or ILSAC GF-5 specification limits, as d Apply limits outlined in API 1509, Appendix F, Table F-2, Footnote 6. e Non-conformance to limits outlined in API 1509, Appendix F, Table F-2 Footnote 6 leads to a request for licensee to confirm Sequence VIII Stay-in-Grade support. f Refer to API CH-4 or CI-4, as. g Refer to API CI-4 PLUS or CJ-4, as. Refer to API SJ, API SL, API SM, API SN, ILSAC GF-4 or ILSAC GF-5 specifications, as i Refer to API CH-4, CI-4,CI-4 PLUS or CJ-4, as j Refer to API SM, API SN, ILSAC GF-4 or ILSAC GF-5 specifications, as

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