NA-LUBE EP 5000 Series

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1 EP 5000 Series

2 EP 5000 Series EP 5000 Series consists of low odor, light colored sulfurized fatty acid esters, triglycerides and a-olefins. The 5000 Series is produced from hydrogen sulfide and elemental sulfur, offering improved oxidative stability and better solubility in paraffinic base oils Series Product Key Series Sulfurized Backbone 1 - Olefin 2 - Fatty Acid Esters 3 - Fatty Acid Esters /Triglyceride 4 - Olefin / Triglyceride Total Sulfur Content % Total Sulfur Example: EP series 2 - Sulfurized Fatty Acid Ester - % total sulfur EP 5000 Series ADTC % Total Sulfur - 30 % Total Nitrogen EP 50 Sulfurized Olefin EP 5 Sulfurized Fatty Acid Esters EP 5300 Sulfurized Fatty Acid Esters / Triglycerides EP 5400 Sulfurized Olefin / Triglycerides / Fatty Acid Esters EP-5131 % Total Sulfur - 30 % Active Sulfur - 19 EP-52 % Total Sulfur - % Active Sulfur - <1.5 EP-53 % Total Sulfur - % Active Sulfur - <1.0 EP-5415 % Total Sulfur - 15 % Active Sulfur - 4 EP-5216 % Total Sulfur - 16 % Active Sulfur - 5 EP-5316 % Total Sulfur - 16 % Active Sulfur - 5 EP-5420 % Total Sulfur - 20 % Active Sulfur - EP-5218 % Total Sulfur - 18 % Active Sulfur - 6 EP-5425 % Total Sulfur - 26 % Active Sulfur - 19

3 Extreme Pressure / Antiwear Additives King Industries offers a broad range of low color, low odor Extreme Pressure Additives used for metalworking fluids, greases, slideway oils and other industrial lubricants. Product % Total Sulfur % Active Sulfur (cst) EP EP-52 < EP EP EP-53 <1.0 EP EP EP EP EP Powder Product ADTC Ashless Dialkydithiocarbamate % Total Sulfur % Total Nitrogen Description Light colored, low odor sulfurized olefin with excellent extreme pressure properties. Unique low odor, very light colored inactive sulfur carrier based on fatty acid ester chemistry. Compatible with copper and its alloys. Enhances the oxidation stability of Group I & II oils when used with yellow metal deactivators and phenolic/aminic antioxidants. Light colored, low odor sulfurized fatty acid ester with excellent extreme pressure properties. Light colored, low odor sulfurized fatty acid ester with excellent extreme pressure properties. Light colored, low odor inactive sulfurized fatty acid ester/fatty oil with excellent extreme pressure properties. Light colored, low odor sulfurized fatty acid ester/ fatty oil with excellent extreme pressure properties. Provides excellent boundary lubrication. Light colored, low odor sulfurized olefin/fatty oil with excellent extreme pressure properties and outstanding thermal and hydrolytic stability. Compatible with copper and its alloys. Enhances the oxidation stability of Group I & II oils when used with yellow metal deactivators and phenolic/aminic antioxidants. Compatible with zinc dithiophosphates. Light colored, low odor sulfurized olefin/fatty oil with excellent extreme pressure properties. Highly suitable for heavy duty drilling and cutting operations. Light colored, low odor sulfurized olefin/fatty oil with excellent extreme pressure properties. Highly suitable for heavy duty drilling and cutting operations. Bis-dimercaptothiadiazole derivative (yellow powder) with excellent extreme pressure/antiwear and antioxidant properties. Recommended for use in grease where heavy load carrying capability is required. (cst) 370 Description A unique ashless dithiocarbamate offering extreme pressure, antiwear and antioxidant properties. EP 5000 Series - Extreme Pressure Additives 2

4 Applications for the EP 5000 Series The EP 5000 Series consists of a variety of novel sulfur-containing additives with total sulfur content ranging from approximately % to 65% and the active sulfur content ranging from <1.5% to 18%. Because these unique products provide both extreme pressure and antiwear properties and also perform as friction modifiers, they are used in a wide variety of lubricant applications, including: Industrial Gear Oils Automotive Gear Oils Automatic Transmission Fluids Slideway Oils EP-52 and EP-5415 are well suited for formulating slideway oils. Hydraulic Fluids Rust and Oxidation Oils Greases EP-52, EP-5415 and EP-5665 are highly recommended for grease applications including non-antimony/lead containing EP greases. Neat Oil Metalworking Fluids EP-5131, EP-52, EP-5216, EP-5218, EP-53, EP-5316, EP-5415 and EP-5425 are outstanding alternatives to chlorinated paraffins in metalworking fluids, when used in combination with ash-producing or ashless phosphorus-type antiwear and boundary lubrication additives. EP-5131, EP-5216, EP-5218, EP-53, EP-5316, EP-5415 and EP-5425 are highly suitable for heavy-duty drilling and cutting operations. Water Miscible Metalworking Fluid Concentrates Environmentally Friendly Lubricants and Greases The EP 5000 sulfur carriers, when combined with AW, AO, NA-SUL and K-CORR products, are highly suitable for formulating high quality/high performance industrial and automotive lubricants and greases. Solubility EP-5121, EP-5131, EP-52, EP-5216, and EP-5218 have excellent solubility in hydrotreated mineral oils, synthetic diesters, and fatty oils. EP-5316 has solubility in napththenic and solvent refined Group I base oils. EP-5415 extends solubility to Group II base oils as well. EP-53 s unique chemistry gives it outstanding solubility characteristics in naphthenic and solvent refined Group I base oils. Due to its novel chemistry, EP-53 provides improved lubricity over similar inactive sulfur fatty acid ester type extreme pressure additives.

5 Performance for the EP 5000 Series Series Performance in a ISO VG 32 Group I Base Oil The following table highlights the performance of the products in various bench tests for lubrication properties. EP-52 EP-5216 EP-5218 Base Oil ISO VG 32 (Group I) Treat Level, % 5.0 Four Ball Weld (ASTM D 2783) seconds, 25 C, 1800 rpm OK Load, kgf Weld Load, kgf EP-5316 EP-5415 Four Ball Wear (ASTM D 4172) 1 hour, 75 C, 40 kgf, 1 rpm Scar Diameter, mm Copper Corrosion (ASTM D 130) 3 hours, 0ºC 24 hours, 0ºC EP-52 - Concentration Effect On Properties 1a 2a As shown below, with increasing concentrations of EP-52, the wear and extreme pressure properties improve with no negative effects on demulsibility or copper corrosion protection. 2.0% EP-52 3a 4a 7.5% EP-52 3a 4a.0% EP-52 Base Oil ISO VG 32 (Group I) Four Ball Weld (ASTM D 2783) seconds, 25 C, 1800 rpm OK Load, kgf Weld Load, kgf 120 1b 3b 220 1b 3b.0% EP % AW-60 Four Ball Wear (ASTM D 4172) 1 hour, 75 C, 40 kgf, 1 rpm Scar Diameter, mm Falex PIN & VEE (ASTM D 3233) Lbs Copper Corrosion (ASTM D130) 3 hours, 0ºC 24 hours, 0ºC Demulsibility (ASTM D 1401,DIN Oil-Water-Emulsion, ml Time, Minutes 1a 3a a 2a a 2a b 2a EP 5000 Series - Extreme Pressure Additives

6 EP-5415 Metalworking Performance Data EP-5415 imparts good extreme pressure performance for metalworking fluids and can be used to replace chlorinated paraffins as shown in the chart below. % Mid-chain Chlorinated Paraffin (C >50% Cl) % EP-5415 Base Oil ISO VG 32 (Group I) Four Ball Weld (ASTM D 2783) seconds, 25 C, 1800 rpm OK Load, kgf Weld Load, kgf Four Ball Wear (ASTM D 4172) 1 hour, 75 C, 40 kgf, 1 rpm Scar Diameter (mm) As shown below, tapping torque tests were conducted to compare the performance of EP-5415 versus the performance of a commonly used chlorinated paraffin. The tests were conducted using 4340-alloy steel under varying machining speeds Copper Corrosion (ASTM D 130) 3 hours, 0ºC 1a 1b Alloy Steel Base Oil: Paraffinic ISO VG 32 % Chlorinated Paraffin Average Peak Torque (inch - pounds) % EP-5415 Average Peak Torque (inch - pounds) % Efficiency 40 sfm* (407rpm) sfm (488rpm) sfm (586rpm) sfm (703rpm) sfm (844rpm) *sfm = surface feet per minute Additionally, EP-5415 can be used to formulate premium quality machine tool slideway lubricants. Various treat levels of EP-5415 in combination with 0.5% tackifier in an ISO VG 68 oil meet the requirements of the Cincinnati Lamb P-47 Heavy-Medium Way Oil specification. 1.5% EP % Tackifier 5.0% EP % Tackifier Cincinnati Lamb P-47 Specification Base Oil ISO VG 68 ISO VG 68 40ºC: ºF: Flash Point (ASTM D 92) COC, ºF >380 > Minimum Fire Point (ASTM D 92) COC ºF >380 > Minimum Acid Number (ASTM D 974) mg KOH/g Maximum Cincinnati Lamb Stick-Slip (μs/μk)* 0.07 / = / 0.09 = Maximum Thermal Stability Test Procedure B: 24 hours, 1ºC CM Color Class Rod Weight of Deposit, mg Rod Metal Loss, mg Acid Number Change, mg KOH/g Precipitate * Ratio of static to kinetic friction Steel Copper None Steel Copper None Maximum Limits Steel Copper

7 ADTC Multifunctional Ashless Dialkyldithiocarbamate ADTC is a unique, ashless dialkyldithiocarbamate additive that offers excellent extreme pressure, antiwear, and antioxidant properties. ADTC has well-defined chemistry with sulfur and nitrogen present in the same molecule. Performance of ADTC - Ashless Hydraulic Fluid Package The table below shows the performance capabilities of ADTC in an ashless hydraulic fluid package containing K-CORR 31, an amino acid derived rust inhibitor. Product ADTC Composition Methylene-bisdibutyldithiocarbamate ADTC exhibits the following properties: C 4 H 9 C 4 H 9 Excellent extreme pressure and antiwear Excellent oxidation inhibition Outstanding demulsification Good thermal stability Excellent solubility in highly paraffinic base stocks ASHLESS PACKAGE: ADTC, AO-130, AW-6220, K-CORR 31 Treat Level of Additive Package, % Base Oil ISO VG 32 (Group I) Demulsibility (ASTM D 1401, DIN ) Oil-Water-Emulsion, ml Separation Time, Minutes N S C S Sulfur Approx. (%) CH Nitrogen Approx. (%) Steel Corrosion (ASTM D 665B, DIN ) Pass Pass Copper Corrosion (ASTM D 130, DIN ) 3 hours, 135 C 1a 1a RPVOT* (ASTM D 2272) Lifetime, Minutes Four Ball Wear (ASTM D 4172) 1 hour, 75 C, 40 kgf, 1 rpm, Scar Diameter, mm AFNOR Wet Filtration (E 68691) Filterability Index FZG A/8.3/90 (ASTM D 5182, DIN Part 2) Damage Load Stage Not Determined >12 0 C (ASTM D 445) Approx. mm 2 /s (cst) S C S Due to its multifunctionality, ADTC is used in: N ADTC PROPERTIES & USES C 4 H 9 C 4 H 9 Heavy Metal-free Greases Rust and Oxidation Oils Automotive and Industrial Gear Oils Extreme Pressure Turbine Oils Hydraulic Oils Engine Oils Metalworking Fluids EP 5000 Series & ADTC * Rotating Pressure Vessel Oxidation Test

8 King Industries, Inc - USA Lubricant Additives Division Science Rd. Norwalk, CT Phone (203) info@kingindustries.com King Industries - Europe Mr. Marcel Groenewoud Noordake EZ Waddinxveen The Netherlands Phone: mg@kingintl.nl King Industries - Asia Dr. Zhiqiang Alex He 42 Ju Lin Ya Yuan Rich Mond Hill (Juhaoyuan) Bo Ai 7th Road Zhongshan, Guangdong, China Phone: alex.he@kingindustries.com The conditions of your use and application of our products, technical assistance and information (whether verbal, written or by way of product evaluations), including any suggested formulations and recommendations, are beyond our control. Therefore, it is imperative that you test our products, technical assistance and information to determine to your own satisfaction whether they are suitable for your intended uses and applications. Such testing has not necessarily been done by King Industries, Inc. ("King"). The facts, recommendations and suggestions herein stated are believed to be reliable; however, no guaranty or warranty of their accuracy is made. EXCEPT AS STATED, THERE ARE NO WARRANTIES, EXPRESS OR IMPLIED, OF MERCHANTABILITY, FITNESS OR OTHERWISE. KING SHALL NOT BE HELD LIABLE FOR SPECIAL, INCIDENTAL, CONSEQUENTIAL OR EXEMPLARY DAMAGES. Any statement inconsistent herewith is not authorized and shall not bind King. Nothing herein shall be construed as a recommendation to use any product(s) in conflict with patents covering any material or its use. No license is implied or granted under the claims of any patent. Sales or use of all products are pursuant to Standard Terms and Conditions stated in King sales documents.

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