y y Manual GPC: Main Characteristics Benefits for the User Flexible Configuration System Control Technical Data / System Components Order Details
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1 Gel Permeation Chromatograh GPC-Sstem for Samle Prearation - Te BASIX Overview of Contents: Manual GPC: Main Characteristics Benefits for the User Flexible Configuration Sstem Control Technical Data / Sstem Comonents Order Details age 1 of 7
2 Manual GPC-Sstem, Te BASIX Main characteristics Benefits for the user The rocessing sequences for samle rearation in esticide analsis are described o.a. within the AOAC method No , USEPA SW-846 method 3640A, EN 12393, EN 1528 and within the L method in accordance with 35 LMBG. After extraction, these methods usuall require the clean-u of the extract via a gel ermeation chromatograh (GPC) sstem. LCTech have develoed a suitable GPC-sstem for this rocessing ste. This sstem, however, can also be utilised in man different areas, for examle in universities or in R&D of industr. This has been realised through the remarkable flexibilit of hardware and the low urchase costs. Flexible... The GPC-sstem BASIX allows for variable set-us, for examle with regard to the column size used, the injection volume, flow rate, overressure or underressure cut-off of the GPC-um, comressibilit of solvents, forerun, main run and tailings and other arameters. Eas to oerate... Great effort has been ut into the design to make it uncomlicated and eas to understand and oerate. Via simle terminal inut on the GPC-um and the LOGO control unit, all imortant arameters can be defined. Once the sstem is switched on, it is immediatel read for oeration. Robust for dail routine oeration... To warrant smooth oeration, all comonents have been designed to be ver robust. All arts wetted b solvents are solvent resistant; materials used are glass, PTFE, stainless steel and PPS-E2. All solvent-carring ies are visible and therefore easil insected and likewise easil exchanged. As a benefit of the robust design, no dail or weekl service needs to be carried out. Summar... The GPC-sstem, Te BASIX, is designed to be eseciall robust for dail routine oeration in the laborator. It is user friendl, versatile and quiet. age 2 of 7
3 Flexible Configuration Flexibilit through intelligent construction B careful combination of units alread included in the basic equiment and comonents secified b the user, an extraordinar flexibilit of the sstem can be ensured. Should ou have further requirements, lease don't hesitate to discuss these with us. The GPC-sstem contains the following comonents: High-qualit LC-dulex um, analtical or rearative Manual injection valve Time-controlled fraction on/off valve LOGO control unit Column stand All necessar tubing Column (diameter of 0 40 mm ossible) and samle loo are to be ordered searatel. We normall recommend a column with 25 mm inner diameter and a bed length of 320 mm and a 5.0 ml samle loo. age 3 of 7
4 Sstem Control Sstem arameterisation Parameterisation is conducted via terminal inut on the sstem and settings on the disla of the GPC-um. The following set-u otions on the GPC-sstem, Te BASIX, are ossible: GPC-um Flow - analtical: ml/min Flow - rearative: ml/min Under/overressure cut-off: variable, adjusted to column Comressibilit: variable, for org. solvents usuall Forerun, main run and tailings from 0 to 100 min Start is automatic via oeration of the manual injection valve Injection b sringe with needle gauge 22 age 4 of 7
5 Technical Data / Sstem Comonents Measurements and weight, electrical connection 380 x 480 x 650 mm (W x D x H), ca kg Connection 1x three-in lug 230 V AC; 50 Hz; CE-certified GPC-um The sstem contains a robust dulex um, which has alread roved itself man times to be excellentl suited for continuous running. This is either a rearative (to be set anwhere between 0.40 and ml/min) or an analtical (from ml/min) um. The um flow rate can be adjusted; ulsation lies below < 1 %. Automatic cut-off on reaching certain thresholds for overressure or underressure as well as comressibilit are art of the sstem standard equiment. The um is solvent resistant and low in maintenance. Pressure range This sstem is ermitted for an oerational ressure of u to 17.5 bar (250 si). A higher ressure range should be discussed first with the manufacturer. Recommended chromatograh column Refillable, DIN-comliant secial column; materials subjected to wetting with solvents are glass and PTFE, 1/8 -PTFE-tube at inlet and outlet site, rigid PTFE-base and adjustable lunger, stable construction, high overressure stabilit, wearing arts are individuall available. If required, an other column ma be built in, which is ermitted for use in the low and intermediate ressure range. The column is not filled. Filling with 50.0 g Bio- Beads, Te S-X3, mesh size is recommended. Samle Loo The sulied standard samle loos are made from PTFE and are set to either 5.0 ml or 1.0 ml. A measuring rotocol is attached. Other volumes are available uon request. The samle loos can be exchanged without an effort. age 5 of 7
6 Order Details Sstems: Gel Permeation Chromatograh (GPC) Sstem, Te BASIX, usable u to 17.5 bar, with rearative HPLC-um (flow rate 0,40 to 40,0 ml/min); with time rogrammed valve for fraction collection; 240 VAC, 50 Hz Order Number GPC-BASIX Gel Permeation Chromatograh (GPC) Sstem, Te BASIX, usable u to 200 bar, with rearative HPLC-um (flow rate 0,40 to 40,0 ml/min); with time rogrammed valve for fraction collection; 240 VAC, 50 Hz Order Number GPC-BASIX-HP Gel Permeation Chromatograh (GPC) Sstem, Te BASIX, usable u to 17.5 bar, with analtical HPLC-um (flow rate 0,10 to 9,95 ml/min); with time rogrammed valve for fraction collection; 240 VAC, 50 Hz Order Number GPC-BASIX-A Gel Permeation Chromatograh (GPC) Sstem, Te BASIX, usable u to 400 bar, with analtical HPLC-um (flow rate 0,10 to 9,95 ml/min); with time rogrammed valve for fraction collection; 240 VAC, 50 Hz Order Number GPC-BASIX-AHP Accessories: Column D25, unfilled, column ID 25 mm, OD 40 mm, filling length between 305 and 365 mm Order Number GPC10010 Column D25, filled with 50 g Bio-Beads (Column GPC10010 / GPC10011) Order Number GPC10011 Column filling kit (onl for LCTech-Column GPC10010 / GPC10011) Order Number GPC10012 Refill (Column GPC10010) with 50 g Bio-Beads Order Number GPC10013 age 6 of 7
7 Column D10, unfilled, column ID 10 mm, OD25 mm, filling length between 300 and 365 mm Order Number GPC20010 Column D10, filled with 10 g Bio-Beads (Column GPC20010 / GPC20011) Order Number GPC20011 Column filling kit (onl for LCTech-Column GPC20010 / GPC20011) Order Number GPC20012 Refill (Column GPC20010) with 10 g Bio-Beads Order Number GPC20013 Bio-Beads, SX-3, mesh size, VE = 100 Order Number GPC10001 Samle loo 5.0 ml, Samle loo with fitting, adjusted to 5 ml, measuring rotocol included Order Number INJ-5 Samle loo 1.0 ml, Samle loo with fitting, adjusted to 1 ml, measuring rotocol included Order Number INJ-1 Samle loo 5.0 ml, Samle loo with fitting, adjusted to 5 ml, material stainless steel Order Numboer INJ-5-HP Samle loo 1.0 ml Samle loo with fitting, adjusted to 1 ml, material stainless steel Order Number INJ-1-HP Laborator bottle made of glass, ml, screw thread GL 45 for solvent sul; with secial sealing ca with searate otions for the GPC um and the sringe um; 1/8 "-connection Order Number F10000-DV Laborator bottle made of glass, ml, screw thread GL 45 with secial sealing ca; connectable to waste-line Order Number F10000-D age 7 of 7
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