OptiMax Product Catalog

Transcription

1 OptiMax Product Catalog OptiMax 1001 Standard Sets 1000 ml Glass Reactor Sets 500 ml Glass Reactor Sets 250 ml Glass Reactor Sets Accessories & Spares Dosing Unit SP-50 OptiMax Your Synthesis Workstation

2 Glossary of Terms Used Glossary of Terms Used ReactIR ETFE FFKM FPM PA PBT PE PEEK = Mid-IR spectroscopy = Ethylene tetrafluoroethylene = Perfluoro-elastomer = Fluoro-elastomer = Polyamide = Polybutylene terephthalate = Polyethylene = Polyetheretherketone POM PP GF25 PU PVC PVDF SAN VQM = Polyoxymethylene = Polypropylene = Polytetrafluoroethylene, 25% glass = Polyurethane = Polyvinylchloride = Polyvinylidene Fluoride = Styrene acrylonitrile = Silicone rubber 2

3 Contents General Introduction 2 4 OptiMax Starter Kit 5 OptiMax Thermostat System 6 11 OptiMax 1000 ml Two-Piece Glass Reactor Set OptiMax 1000/500 ml Cover Set OptiMax 500 ml Two-Piece Glass Reactor Set OptiMax 250 ml Two-Piece Glass Reactor Set OptiMax 1000 ml One-Piece Glass Reactor Set OptiMax 500 ml One-Piece Glass Reactor Set OptiMax 250 ml One-Piece Glass Reactor Set OptiMax Spare Parts, Adapters, and Stirrers OptiMax Accessories and Probes 41 Dosing Unit SP-50 Set OptiMax HFCal Kit icontrol Software for OptiMax 49 Compatibility List

4 General Introduction OptiMax Your Synthesis Workstation Editorial No oil baths, ice baths, and cryostats required Precise temperature control from 40 C to 180 C Small and mobile Wide range of different reactors and stirrers Simple and intuitive touch screen operation No learning curve Programmable Secure unattended operation Data logging making experiments traceable and reproducible Data export into icontrol and Microsoft Excel Introduction OptiMax is a synthesis workstation that is beyond traditional synthesis equipment. It is geared towards today s workflows in chemical and process development labs. It simplifies organic synthesis by eliminating cumbersome steps and ensures precise and accurate execution of chemical synthesis. It heats and cools efficiently without the need for cryostats, oil or ice baths, offers a large variety of different reactors and stirrers, and is operated by a simple touch screen. Even though its use is simple, experiments are carried out with highest precision, reproducible and traceable increasing productivity in chemical and process development significantly. A Remarkable Thermostat OptiMax is a single self-contained box with a built-in solid state thermostat covering the entire Temperature Range without an additional cryostat. The powerful Peltier-based thermostat provides the necessary performance to control the temperature of the reaction mixture accurately and reproducibly. It grants outstanding heating and cooling rates in the entire Temperature Range from 40 C to 180 C. Even strong chemical reactions are kept at constant temperature, ensuring that the experiment is carried out safely and the reaction kinetics remains unaffected. Operation OptiMax is operated completely effortless using a smart and intuitive touch screen. Changing experiment parameters, such as temperature or stirring speed is a matter of seconds and doesn t require any training. The experiment is either carried out stepby-step or programmed and completely unattended. The safety monitoring system ensures safe execution of the individual tasks without permanent supervision. All data and relevant information are displayed and recorded as the experiment proceeds. For further evaluation the recorded data can be transferred to either icontrol, the sophisticated PC software or Microsoft Excel. 4

5 OptiMax Starter Kit OptiMax Starter Kit The OptiMax starter kit is a ready-to-go setup that simplifies the part evaluation and ordering process. The starter kit combines all the key items for an easy-to-use 1000 ml two-piece reactor setup in just one part number. The OptiMax starter kit includes the following key components: OptiMax thermostat system incl. touchscreen Stirrer motor and adapter Tr temperature probe incl. adapter 1000 ml two-piece glass reactor Cover and reactor holders Pitched blade stirrer, downward, Alloy C-22 Bar type baffle, Alloy C-22 incl. adapter Stoppers and Keck clamps for all open ports Accessories holder The OptiMax starter kit can be combined individually with any additional items in this catalog OptiMax 1001 starter kit consists of the following items OptiMax thermostat system OptiMax 1000 ml two-piece glass reactor set adapter for Tr, ph, and turbidity probe Tr probe, Alloy C Accessories holder set Details regarding these items can be found on the following pages. 5

6 OptiMax Thermostat System OptiMax Thermostat System Power Supply Voltages Back-/Frontlight Heating/Cooling Temperature Mode OptiMax 1001 reactor block available only in a thermostat system set Powder-coated stainless steel with FEP/PFA coated cover plate VAC 12 LEDs Solid state thermostat Jacket control, reaction mixture control, crystallization and distillation (constant or ramp) Temperature Range 40 C to 180 C, jacket temperature (Tj) 388 mm x 414 mm x 539 mm (w, d, h), 388 mm x 414 mm x 780 mm (w, d, h with overhead stirrer) Weight 35 kg, including touchscreen OptiMax thermostat system set consisting of Order Number Product Description Quantity OptiMax 1001 reactor block TFT OptiMax touchscreen Pen for OptiMax touchscreen Overhead stirrer drive complete Lab bar, 600 mm x 14 mm Reactor block plug for bottom drain valve opening PVC tube for coolant, length 2.5 m PVC tube, soft, for reflux condenser, length 5 m PVC tube for gas inlet, length 2 m Flow indicator for coolant Reducing connector for purge gas tubing Quick connect coupling for purge gas inlet Hose clamp for PVC tube 4 USB memory stick for data export Bubble counter Magnetic bubble counter holder Purge gas regulation valve OptiMax touchscreen protective cover Identification clips for adhesive labels to label individual sensors, reactors etc Glass adapter ST19/26-GL Screw cap GL14, with aperture Sealing ring with vulcanized-on washers for GL14 cap Y-piece for gas tubing OptiMax LOGBook, includes Operating Instructions, Guides, and other product-related documents 1 6

7 OptiMax Thermostat System TFT OptiMax touchscreen including protective cover PA, aluminium 195 mm x 135 mm x 60 mm (w, d, h) PVC tube for coolant PVC Ø 8/12 mm, length 2.5 m Pen for touch screen operation Length 140 mm PVC tube, soft, for reflux condenser PVC Ø 8/12 mm, length 5 m Overhead stirrer drive complete Aluminium anodized, Speed 30 rpm to 1200 rpm PVC tube for purge gas inlet PVC Ø 4/6 mm, length 2 m Lab bar 600 mm x 14 mm Stainless steel, Ø 14 mm x 600 mm Flow indicator for coolant SAN Temperature Max. 30 C For tubes with inner Ø 6 mm to 9 mm available on special request only USB 2.0 memory stick for data export Memory 2 GB 55 mm x 15 mm x 6 mm available on special request only Reducing connector for purge gas tubing PP Temperature Max. 30 C For tubes with inner Ø 7 mm to 11 mm; 4 mm to 7 mm 7

8 OptiMax Thermostat System Reactor block plug for bottom drain valve opening GF25 Ø 56 mm x 35 mm O-ring needed Bubble counter Borosilicate glass Ø 30 mm x 150 mm O-ring for plug FPM Ø mm x 3.53 mm, AS No Magnetic bubble counter holder PET 30 mm x 33 mm x 68 mm Quick connect coupling for purge gas in-/outlet Stainless steel For tubes with inner Ø 4 mm Purge gas regulation valve PA 6.6, NBR Tube Ø 6 mm Hose clamp for PVC tube Stainless steel Ø 14 mm to 9.5 mm available on special request only Identification clips for adhesive labels to label individual sensors, reactors etc. For cables with Ø 2 mm to 4.5 mm 8

9 OptiMax Thermostat System OptiMax touchscreen protective cover Barex resin Glass adapter ST19/26-GL14 Glass Height 50 mm Screw cap GL14, with aperture PBT Aperture Ø 9.5 mm Sealing ring with vulcanized-on washers for GL14 cap Silicone rubber VQM, -coated Ø 12 mm, aperture 6 mm Y-piece for gas tubing Acetal resin For tubes with inner Ø 4 mm OptiMax LOGBook Quantity Includes OptiMax Operating Instructions, Guides, and other product-related documents 1 of each 9

10 OptiMax Thermostat System OptiMax Thermostat System Spare Parts TFT OptiMax touchscreen including protective cover PA, aluminium 195 mm x 135 mm x 60 mm (w, d, h) Overhead stirrer motor standard Aluminium anodized, Speed 30 rpm to 1200 rpm ± 5 rpm Security ring to hold stirrer shaft PEEK Speed Inner Ø 10 mm Stirrer adapter, ST24 (Valfon 117) Inner Ø 10 mm Loosening nut for stirrer adapter PEEK Inner Ø M Bearing sleeve for overhead stirrer PEEK/ Inner Ø 10 mm Compression spring for overhead stirrer PEEK Inner Ø 10 mm 10

11 Accessories for OptiMax System Accessories for OptiMax System Alloy C-22 temp. sensor, incl. chip Alloy C-22 Ø 1/4 (6.35 mm), 300 mm Accessories holder set to be attached to the lab bar of your OptiMax system for stirrer motor (ST24), for Ø 12 mm probes (ST19), for Ø 6 mm probes (ST14) Stainless steel, GF25 Quantity in a set 2 x holders 1 x adapter with ST14 aperture 4 x adapters with ST19 aperture 1 x adapter with ST24 aperture adapter, eccentric for Tr and turbidity probe, including sealing ring Inner Ø 6 mm, ST14 can also be used for Ø 1/ mm inserts Sealing ring for adapter Inner Ø 6 mm can also be used for Ø 1/ mm inserts Purge gas set for overhead stirrer available only as a set Stainless steel, PVC, PP Temperature PP max 30 C Quantity in a set 1 x bulkhead connector 2 x quick connect couplings (for tubes inner Ø 4 mm) 1 x reducing connector (for tubes inner Ø 7 mm to 11 mm and 4 mm to 7 mm) 1 x PVC tube (inner Ø 4 mm) Plastic hose, straight with silicone rubber seal, for GL14 screw cap PP, VQM For tube inner Ø 6 mm to 9 mm Touchscreen cable extension to be ordered with base unit or assembled by a field service engineer Length 3 m 11

12 OptiMax 1000 ml Two-Piece Glass Reactor Set OptiMax 1000 ml Glass Reactor Set Two-Piece ml two-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 1000 ml two-piece glass reactor set consisting of The 1000 ml two-piece glass reactor is equipped with a bottom drain valve and has a working volume of 1000 ml, a nominal volume of 1310 ml and a starting volume of 200 ml. Order Number Product Description Quantity Glass reactor, 1000 ml Reactor holder for 1000 ml reactor Glass cover, for 1000/500 ml reactor, 7 ports Cover holder for 1000/500 ml reactor cover Reactor clamp for 1000/500 ml reactor O-ring for 1000/500 ml reactor Stirrer shaft for 1000/500 ml reactor, Alloy C Pitched stirrer blade, Alloy C-22, downward Bar type baffle for 1000 ml reactor, Alloy C adapter for baffle Drain union, bended Pinch clamp S Glass stopper ST29/ Glass stopper ST19/ Glass stopper ST14/ Keck clamp ST Keck clamp ST Keck clamp ST Keck clamp ST

13 OptiMax 1000 ml Two-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST24/29 Overhead stirrer ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/ mm ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/ mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ml glass reactor Borosilicate glass,, PEEK, silicone Working Volume Max ml Nominal Volume 1310 ml Temperature 40 C to 180 C Inner Ø 101 mm, height 172 mm, wall 3 mm Glass cover for 1000/500 ml reactor, seven ports 1 x ST14/23, 3 x ST19/26, 2 x ST29/32, center ST24/29 Borosilicate glass Temperature 40 C to 180 C Inner Ø 98 mm Reactor holder for 1000 ml reactor Stainless steel , PE Cover holder for 1000/500 ml reactor cover Stainless steel , PE Inner Ø 121 mm x 22 mm Reactor clamp for 1000/500 ml reactor Stainless steel , Glastherm HT 220 (Thermalite 220M) O-ring for 1000/500 ml reactor Elastomer Vollkern Silicone VQM, FEP-coated Temperature 60 C to 200 C Ø mm x 3.53 mm, AS No

14 OptiMax 1000 ml Two-Piece Glass Reactor Set Drain union, bended Borosilicate glass Inner Ø 9 mm, spherical joint S Pinch clamp S19 drain union clamp Stainless steel Glass stopper ST29/32 Glass Glass stopper ST19/26 Glass Glass stopper ST14/23 Glass Keck clamp ST29 POM Keck clamp ST24 POM Keck clamp ST19 POM Keck clamp ST14 POM 14

15 OptiMax 1000 ml Two-Piece Glass Reactor Set Stirrer shaft for 1000/500 ml reactor M8 thread Alloy C-22 Ø 10 mm, length 400 mm Pitched stirrer blade for 1000/500 ml reactor downward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm adapter for baffle, eccentric for baffle, including sealing ring Inner Ø 10 mm, ST Bar type baffle for 1000 ml reactor Alloy C-22 Ø 10 mm, width 15 mm, length 249 mm Optional Accessories O-ring for 1000/500 ml reactor FFKM Temperature up to 275 C Ø mm x 3.53 mm, AS No

16 OptiMax Cover Set OptiMax Cover Set For 1000 ml and 500 ml Reactors OptiMax cover set This reactor cover is an extremely robust alternative for the standard glass cover It is the perfect choice if the reactor is equipped with heavy inserts and probes which bears the risk to break the glass version of the cover. The cover comes as full set with all the required adapters to accommodate typical combinations of probes and inserts. OptiMax cover set consisting of The cover can be used in combination with the standard O-rings and reactor clamp as used for the glass cover. COWIE part number Product Description Quantity cover for 1000 ml and 500 ml reactors 1 OptiMax standard stirrer adapter, ST24/32 x 3/4 NPT 1 PC ST19/38 x 3/4 NPT 3 PC ST29/42 x 1 NPT 2 PC ST14/35 x 1/2 NPT 1 PC NPT x 19 mm compression fitting 1 PC NPT x 5/ mm compression fitting 1 PC /4 NPT x 14 mm compression fitting 1 PC /4 NPT x 12 mm compression fitting 1 PC /4 NPT x 8 mm compression fitting 1 PC /4 NPT x 3/ mm compression fitting 1 PC /4 NPT x 1/ mm compression fitting 1 PC /2 NPT x 6 mm compression fitting 1 PC /2 NPT x 1/ mm compression fitting 1 Note: All the contained threaded adapters are standard parts from COWIE. In case replacement or additional adapters are required, please refer to All the COWIE part numbers are indicated with a PC as prefix. 16

17 OptiMax Cover Set The cover is mainly used to run crystallization experiments. Special care needs to be taken when the cover is used for reflux experiments since absolute solvent tightness cannot be guaranteed under all circumstances. 3/4 NPT ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm, calibration heater Ø 8 mm 3/4 NPT Overhead stirrer 3/4 NPT ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm, calibration heater Ø 8 mm 1 NPT ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/ mm, ParticleTrack G400 probe Ø 19 mm 1 NPT ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/ mm, ParticleTrack G400 probe Ø 19 mm 1/2 NPT Tr probe glass Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm, Tr probe Alloy C-22 Ø 1/ mm 3/4 NPT ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm, calibration heater Ø 8 mm cover for 1000 ml and 500 ml reactors, seven ports 2 x 1 NPT, 4 x 3/4 NPT, 1 x 1/2 NPT Temperature 40 C to 180 C OptiMax standard stirrer adapter ST24/32 x 3/4 NPT Inner Ø ST24/32, 3/4 NPT PC ST29/42 x 1 NPT Inner Ø ST29/42, 1 NPT, height 60 mm PC ST19/38 x 3/4 NPT Inner Ø ST19/38, 3/4 NPT, height 57 mm PC ST14/30 x 1/2 NPT Inner Ø ST14/35, 1/2 NPT, height 45 mm PC NPT x 19 mm compression fitting Inner Ø 19 mm, 1 NPT 17

18 OptiMax Cover Set PC NPT x 5/8 compression fitting, PEEK Inner Ø 5/ mm, 1 NPT PC /4 NPT x 14 mm compression fitting, PEEK Inner Ø 14 mm, 3/4 NPT PC /4 NPT x 12 mm compression fitting, PEEK Inner Ø 12 mm, 3/4 NPT PC /4 NPT x 8 mm compression fitting, PEEK Inner Ø 8 mm, 3/4 NPT PC /4 NPT x 3/8 compression fitting, PEEK Inner Ø 3/ mm, 3/4 NPT PC /4 NPT x 1/4 compression fitting, PEEK Inner Ø 1/ mm, 3/4 NPT PC /2 NPT x 1/4 compression fitting, PEEK Inner Ø 1/ mm, 1/2 NPT PC /2 NPT x 6 mm compression fitting, PEEK Inner Ø 6 mm, 1/2 NPT 18

19 OptiMax 500 ml Two-Piece Glass Reactor Set OptiMax 500 ml Glass Reactor Set Two-Piece ml two-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 500 ml two-piece glass reactor set consisting of The 500 ml two-piece glass reactor is equipped with a bottom drain valve and has a working volume of 500 ml, a nominal volume of 830 ml and a starting volume of 70 ml. Order Number Product Description Quantity Glass reactor, 500 ml Reactor holder for 500 ml reactor Glass cover, for 1000/500 ml reactor, 7 ports Cover holder for 1000/500 ml reactor cover Receptacle for 500 ml reactor Reactor clamp for 1000/500 ml reactor O-ring for 1000/500 ml reactor Stirrer shaft for 1000/500 ml reactor, Alloy C Pitched stirrer blade, Alloy C-22, downward Bar type baffle for 500 ml reactor, Alloy C adapter for baffle Drain union, bended Pinch clamp S Glass stopper ST29/ Glass stopper ST19/ Glass stopper ST14/ Keck clamp ST Keck clamp ST Keck clamp ST Keck clamp ST

20 OptiMax 500 ml Two-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST24/29 Overhead stirrer ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/ mm ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/ mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ml glass reactor Borosilicate glass,, PEEK, silicone Working Volume Max. 500 ml Nominal Volume 830 ml Temperature 40 C to 180 C Inner Ø 77 mm, height 172 mm, wall 2.5 mm Glass cover for 1000/500 ml reactor, seven ports 1 x ST14/23, 3 x ST19/26, 2 x ST29/32, center ST24/29 Borosilicate glass Temperature 40 C to 180 C Inner Ø 98 mm Reactor holder for 500 ml reactor Stainless steel , PE Cover holder for 1000/500 ml reactor cover Stainless steel , PE Inner Ø 121 mm x 22 mm Receptacle for 500 ml reactor Thermostat sleeve Aluminium anodized 20

21 OptiMax 500 ml Two-Piece Glass Reactor Set Reactor clamp for 1000/500 ml reactor Stainless steel , Glastherm HT 220 (Thermalite 220M) O-ring for 1000/500 ml reactor Elastomer Vollkern Silicone VQM, FEP-coated Temperature 60 C to 200 C Ø mm x 3.53 mm, AS No Drain union, bended Borosilicate glass Inner Ø 9 mm, spherical joint S Pinch clamp S19 drain union clamp Stainless steel Glass stopper ST29/32 Glass Glass stopper ST19/26 Glass Glass stopper ST14/23 Glass Keck clamp ST29 POM Keck clamp ST24 POM 21

22 OptiMax 500 ml Two-Piece Glass Reactor Set Keck clamp ST19 POM Keck clamp ST14 POM Stirrer shaft for 1000/500 ml reactor M8 thread Alloy C-22 Ø 10 mm, length 400 mm Pitched stirrer blade for 1000/500 ml reactor downward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm adapter for baffle, eccentric for baffle, including sealing ring Inner Ø 10 mm, ST Bar type baffle for 500 ml reactor Alloy C-22 Ø 10 mm, width 15 mm, length 237 mm Optional Accessories O-ring for 1000/500 ml reactor FFKM Temperature up to 275 C Ø mm x 3.53 mm, AS No

23 OptiMax 250 ml Two-Piece Glass Reactor Set OptiMax 250 ml Glass Reactor Set Two-Piece ml two-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 250 ml two-piece glass reactor set consisting of The 250 ml two-piece glass reactor has no bottom drain valve and has a working volume of 250 ml, a nominal volume of 370 ml and a starting volume of 50 ml. Order Number Product Description Quantity Glass reactor, 250 ml Reactor stand for 250 ml reactor Glass cover for 250 ml reactor, 7 ports Cover holder for 250 ml reactor cover Receptacle for 250 ml reactor Reactor clamp for 250 ml reactor O-ring for 250 ml reactor Stirrer shaft for 250 ml reactor, Alloy C Pitched stirrer blade, Alloy C-22, downward Glass stopper ST19/ Glass stopper ST14/ Keck clamp ST Keck clamp ST Keck clamp ST

24 OptiMax 250 ml Two-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm ST24/29 Overhead stirrer ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm Glass reactor, 250 ml Borosilicate glass Working Volume Max. 250 ml Nominal Volume 370 ml Temperature 40 C to 180 C Inner Ø 62 mm, height 127 mm, wall 2.2 mm Glass cover for 250 ml reactor, seven ports 2 x ST14/23, 4 x ST19/26, center ST24/29 Borosilicate glass Temperature 40 C to 180 C Inner Ø 68 mm Reactor stand for 250 ml reactor PE Ø 108 mm x 105 mm Cover holder for 250 ml reactor cover Stainless steel , PE Inner Ø 88 mm x 22 mm Receptacle for 250 ml reactor Thermostat sleeve Aluminium anodized Reactor clamp for 250 ml reactor Stainless steel , Glastherm HT 220 (Thermalite 220M) 24

25 OptiMax 250 ml Two-Piece Glass Reactor Set O-ring for 250 ml reactor Elastomer Vollkern Silicone VQM, FEP-coated Temperature 60 C to 200 C Ø mm x 3.53 mm, AS No Stirrer shaft for 250 ml reactor M3 thread Alloy C-22 Ø 10/8 mm, length 400 mm Pitched stirrer blade for 250 ml reactor downward, four impellers, 45, M3 thread Alloy C-22 Outer Ø 38 mm Glass stopper ST19/26 Glass Glass stopper ST14/23 Glass Keck clamp ST24 POM Keck clamp ST19 POM Keck clamp ST14 POM Optional Accessories O-ring for 250 ml reactor FFKM Temperature up to 275 C Ø mm x 3.53 mm, AS No

26 OptiMax 1000 ml One-Piece Glass Reactor Set OptiMax 1000 ml Glass Reactor Set One-Piece ml one-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 1000 ml one-piece glass reactor set consisting of The 1000 ml one-piece glass reactor has a working volume of 1000 ml, a nominal volume of 1150 ml and a starting volume of 200 ml. Order Number Product Description Quantity One-piece glass reactor, 1000 ml Reactor stand for 1000 ml reactor Glass stirrer shaft for 1000/500/250 ml one-piece reactor Half-moon stirrer blade, 71 mm Bar type baffle for 1000 ml reactor, Alloy C adapter for baffle Glass stopper ST29/ Glass stopper ST19/ Glass stopper ST14/ Keck clamp ST Keck clamp ST Keck clamp ST Keck clamp ST

27 OptiMax 1000 ml One-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST24/29 Overhead stirrer ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/ mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm ml one-piece glass reactor, seven ports 1 x ST14/23, 4 x ST19/26, 1 x ST29/32, center ST24/29 Borosilicate glass Working Volume Max ml Nominal Volume 1150 ml Temperature 40 C to 180 C Inner Ø 101 mm, height 230 mm, wall 3 mm Reactor stand for 1000 ml one-piece reactor PE Ø 148 mm x 120 mm Glass stirrer shaft for 1000/500/250 ml reactor Borosilicate glass Ø 10 mm, length 380 mm Bar type baffle for 1000 ml reactor Alloy C-22 Ø 10 mm, width 15 mm, length 249 mm Half-moon stirrer blade for 1000 ml reactor 19 mm x 71 mm adapter for baffle, eccentric for baffle, including sealing ring Inner Ø 10 mm, ST19 27

28 OptiMax 1000 ml One-Piece Glass Reactor Set Glass stopper ST29/32 Glass Glass stopper ST19/26 Glass Glass stopper ST14/23 Glass Keck clamp ST29 POM Keck clamp ST24 POM Keck clamp ST19 POM Keck clamp ST14 POM 28

29 OptiMax 500 ml One-Piece Glass Reactor Set OptiMax 500 ml Glass Reactor Set One-Piece ml one-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 500 ml one-piece glass reactor set consisting of The 500 ml one-piece glass reactor has a working volume of 500 ml, a nominal volume of 700 ml and a starting volume of 70 ml. Order Number Product Description Quantity One-piece glass reactor, 500 ml Receptacle for 500 ml reactor Glass stirrer shaft for 1000/500/250 ml one-piece reactor Half-moon stirrer blade, 54 mm Reactor stand for 500 ml reactor Bar type baffle for 500 ml reactor, Alloy C adapter for baffle Glass stopper ST19/ Glass stopper ST14/ Keck clamp ST Keck clamp ST Keck clamp ST Keck clamp ST

30 OptiMax 500 ml One-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST24/29 Overhead stirrer ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm ml one-piece glass reactor, seven ports 2 x ST14/23, 4 x ST19/26, center ST24/29 Borosilicate glass Working Volume Max. 500 ml Nominal Volume 700 ml Temperature 40 C to 180 C Inner Ø 77 mm, height 225 mm, wall 2.5 mm Receptacle for 500 ml one-piece reactor Thermostat sleeve Aluminium anodized Glass stirrer shaft for 1000/500/250 ml reactor Borosilicate glass Ø 10 mm, length 380 mm Reactor stand for 500 ml one-piece reactor PE Ø 123 mm x 120 mm Half-moon stirrer blade for 500 ml reactor 19 mm x 54 mm 30

31 OptiMax 500 ml One-Piece Glass Reactor Set adapter for baffle, eccentric for baffle, including sealing ring Inner Ø 10 mm, ST Bar type baffle for 500 ml reactor Alloy C-22 Ø 10 mm, width 15 mm, length 237 mm Glass stopper ST19/26 Glass Glass stopper ST14/23 Glass Keck clamp ST29 POM Keck clamp ST24 POM Keck clamp ST19 POM Keck clamp ST14 POM 31

32 OptiMax 250 ml One-Piece Glass Reactor Set OptiMax 250 ml Glass Reactor Set One-Piece ml one-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 250 ml one-piece glass reactor set consisting of The 250 ml one-piece glass reactor has a working volume of 250 ml, a nominal volume of 400 ml and a starting volume of 50 ml. Order Number Product Description Quantity One-piece glass reactor, 250 ml Reactor stand for 250 ml reactor Receptacle for 250 ml reactor Glass stirrer shaft for 1000/500/250 ml one-piece reactor Half-moon stirrer blade, 43 mm Glass stopper ST19/ Glass stopper ST14/ Keck clamp ST Keck clamp ST Keck clamp ST

33 OptiMax 250 ml One-Piece Glass Reactor Set ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST24/29 Overhead stirrer ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/ mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/ mm ml one-piece glass reactor, seven ports 2 x ST14/23, 4 x ST19/26, center ST24/29 Borosilicate glass Working Volume Max. 250 ml Nominal Volume 400 ml Temperature 40 C to 180 C Inner Ø 62 mm, height 205 mm, wall 2.5 mm Receptacle for 250 ml one-piece reactor Thermostat sleeve Aluminium anodized Glass stirrer shaft for 1000/500/250 ml reactor Borosilicate glass Ø 10 mm, length 380 mm Reactor stand for 250 ml one-piece reactor PE Ø 108 mm x 105 mm Half-moon stirrer blade, 43 mm 19 mm x 43 mm 33

34 OptiMax 250 ml One-Piece Glass Reactor Glass stopper ST19/26 Glass Glass stopper ST14/23 Glass Keck clamp ST24 POM Keck clamp ST19 POM Keck clamp ST14 POM 34

35 OptiMax Spare Parts, Adapters, and Stirrers OptiMax Reactor Spare Parts and Adapters Glass vessel for two-piece 1000 ml reactor without parts for bottom drain valve Borosilicate glass Working Volume Nominal Volume Max ml 1300 ml Temperature 40 C to 180 C Inner Ø 101 mm, height 172 mm, wall 3 mm Glass vessel for two-piece 500 ml reactor without parts for bottom drain valve Borosilicate glass Working Volume Nominal Volume Max. 500 ml 700 ml Temperature 40 C to 180 C Inner Ø 77 mm, height 172 mm, wall 2.5 mm Bottom drain connect set for bottom drain valve PEEK, Ø 52 mm Sealing ring for bottom drain FEP Inner Ø 22 mm, 14 mm Spindle, bottom drain valve 115 mm, with spring Ø 14 mm x 115 mm adapter, eccentric for PVM/D600 probe, including sealing ring Inner Ø 19 mm, ST Sealing ring for adapter cord Inner Ø 19 mm Quantity 5 pcs in a set 35

36 OptiMax Spare Parts, Adapters, and Stirrers adapter for baffle, eccentric for baffle, including sealing ring Inner Ø 10 mm, ST Sealing ring for adapter cord Inner Ø 10 mm Quantity 5 pcs in a set adapter for G400, including sealing ring Inner Ø 14 mm, ST Sealing ring for adapter Inner Ø 14 mm adapter, eccentric for ph and turbidity probe, including sealing ring Inner Ø 12 mm, ST Sealing ring for adapter Inner Ø 12 mm adapter, eccentric for turbidity probe, including sealing ring Inner Ø 6 mm, ST19 Can also be used for Ø 1/ mm inserts Sealing ring for and adapters Inner Ø 6 mm Can also be used for Ø 1/ mm inserts adapter, eccentric for Tr and turbidity probe, including sealing ring Inner Ø 6 mm, ST14 Can also be used for Ø 1/ mm inserts

37 OptiMax Spare Parts, Adapters, and Stirrers OptiMax Mixing Device Available Stirrers For 1000 ml two-piece reactor Stirrer shaft for 1000/500 ml reactor M8 thread Alloy C-22 Ø 10 mm, length 400 mm Anchor blade for 1000 ml reactor M8 thread Alloy C-22 Outer Ø 90 mm, height 100 mm Pitched stirrer blade for 1000/500 ml reactor upward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm Pitched stirrer blade for 1000/500 ml reactor downward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm Pitched-blade glass stirrer for 1000/500 ml reactor upward, four impellers, 45 Borosilicate glass Outer Ø 45 mm, length 400 mm Pitched-blade glass stirrer for 1000/500 ml reactors downward, four impellers, 45 Borosilicate glass Outer Ø 45 mm, length 400 mm 37

38 OptiMax Spare Parts, Adapters, and Stirrers For 500 ml two-piece reactor Stirrer shaft for 1000/500 ml reactor M8 thread Alloy C-22 Ø 10 mm, length 400 mm Anchor blade for 500 ml reactor M8 thread Alloy C-22 Outer Ø 69 mm, height 100 mm Pitched stirrer blade for 1000/500 ml reactor upward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm Pitched stirrer blade for 1000/500 ml reactor downward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm Pitched-blade glass stirrer for 1000/500 ml reactor upward, four impellers, 45 Borosilicate glass Outer Ø 45 mm, length 400 mm Pitched-blade glass stirrer for 1000/500 ml reactor downward, four impellers, 45 Borosilicate glass Outer Ø 45 mm, length 400 mm 38

39 OptiMax Spare Parts, Adapters, and Stirrers For 250 ml two-piece reactor Stirrer shaft for 250 ml reactor M3 thread Alloy C-22 Ø 10/8 mm, length 400 mm Anchor stirrer for 250 ml reactor M3 thread Alloy C-22 Outer Ø 55 mm, height 80 mm Pitched stirrer blade for 250 ml reactor upward, four impellers, 45, M3 thread Alloy C-22 Outer Ø 38 mm Pitched stirrer blade for 250 ml reactor downward, four impellers, 45, M3 thread Alloy C-22 Outer Ø 38 mm Pitched-blade glass stirrer for 250 ml reactor upward, four impellers, 45 Borosilicate glass Outer Ø 38 mm, length 400 mm Pitched-blade glass stirrer for 250 ml reactor downward, four impellers, 45 Borosilicate glass Outer Ø 38 mm, length 400 mm 39

40 OptiMax Spare Parts, Adapters, and Stirrers For 1000 ml one-piece reactor Glass stirrer shaft for 1000/500/250 ml one-piece reactor Borosilicate glass Ø 10 mm, length 380 mm Half-moon stirrer blade for 1000 ml one-piece reactor 19 mm x 71 mm For 500 ml one-piece reactor Glass stirrer shaft for 1000/500/250 ml one-piece reactor Borosilicate glass Ø 10 mm, length 380 mm Half-moon stirrer blade for 500 ml one-piece reactor 19 mm x 54 mm For 250 ml one-piece reactor Glass stirrer shaft for 1000/500/250 ml one-piece reactor Borosilicate glass Ø 10 mm, length 380 mm Half-moon stirrer blade for 250 ml one-piece reactor 19 mm x 43 mm 40

41 OptiMax Accessories and Probes OptiMax Accessories Reflux Condenser, Tr and ph Probes Reflux condenser glass, ST19 Borosilicate glass 250 mm x 40 mm Glass temp. sensor, including chip Glass Ø 6 mm, 300 mm Alloy C-22 temp. sensor, including chip Alloy C-22 Ø 1/ mm, 300 mm ph sensor OptiMax, incl. chip without cable Lead-free glass (shaft), high alkaline glass (membrane) Ø 12 mm, 325 mm (glass body only) Cable for ph sensor Length 100 cm 41

42 OptiMax Accessories and Probes Dosing Unit SP-50 Set Dosing unit SP-50 set This unit will allow you to dose one reagent in two reactors completely independent and in parallel via touchscreen or PC software. Only available in the set. Dosing unit SP-50 set consisting of Order Number Product Description Quantity Dosing Unit SP-50, only available in the set CAN cable 100 cm dosing tube Ø 3.2 mm dosing tube Ø 1.6 mm Nut for UNF 1/4 28 threads, outer Ø max. 3.2 mm, 4 pcs in a set Ferrule for tubing and sensors of outer Ø 3.2 mm, 4 pcs in a set Plug for UNF 1/4 28 threads, 4 pcs in a set Nut for UNF 1/4 28 threads, outer Ø max. 1.6 mm, 4 pcs in a set Ferrule for tubing and sensors of outer Ø 1.6 mm, 4 pcs in a set Glass adapter ST14/23-GL Screw cap GL14, closed Silicone rubber seal (septum), 10 pcs in a set Distributor cap GL45 2 x GL Bottle GL ml with cap Adapter GL14-UNF Screw cap GL14, with aperture Silicone rubber sealing ring, outer Ø 12 mm, aperture 6 mm Assorted heat-shrink tubings, 8 pcs in a set 1 42

43 OptiMax Accessories and Probes Nut for UNF 1/4 28 threads ETFE Outer Ø max. 3.2 mm Quantity 4 pcs in a set only available in the set Dosing unit SP Ferrule for tubing and sensors of outer Ø 3.2 mm Quantity ETFE Outer Ø max. 3.2 mm 4 pcs in a set CAN cable 100 cm Length 100 cm Plug for UNF 1/4 28 threads ETFE Outer Ø max. 1.6 mm Quantity 4 pcs in a set dosing tube Ø 3.2 mm Ø 3.2 mm, length 2.5 m Nut for UNF 1/4 28 threads ETFE Outer Ø max. 1.6 mm Quantity 4 pcs in a set dosing tube Ø 1.6 mm Ø 1.6 mm, length 2.5 m Ferrule for tubing and sensors of outer Ø 1.6 mm Quantity ETFE Outer Ø max. 1.6 mm 4 pcs in a set 43

44 OptiMax Accessories and Probes Glass adapter ST14/23-GL14 Glass Height 54 mm Adapter GL14-UNF GF mm x 2.62 mm Screw cap GL14, closed with sealing PBT Temperature Max. 200 C Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm Silicone rubber seal (septum) for screw cap GL14 Quantity Silicone rubber VQM Ø 12 mm, thickness 2 mm 10 pcs in a set Sealing ring with vulcanized-on washers for GL14 cap Silicone rubber VQM, -coated Ø 12 mm, aperture 6 mm Distributor cap GL45 2x GL14 PP Assorted heat-shrink tubings 8 pcs in a set Polyolefin Bottle GL ml with cap Glass, PP 44

45 OptiMax Accessories and Probes Dosing Unit SP-50 Syringes Flexible volumes from 1 ml, 10 ml, 25 ml, and 50 ml syringes Automatic refill of syringes possible with Dosing Unit SP-50 Interchangeable at all times during an experiment Syringe 1 ml Glass,, metal Volume 1 ml Syringe 25 ml Glass,, metal Volume 25 ml Syringe 10 ml Glass,, metal Volume 10 ml Syringe 50 ml Glass,, metal Volume 50 ml 45

46 OptiMax Accessories and Probes OptiMax HFCal Kit OptiMax HFCal Kit A calorimetry Upgrade Kit for OptiMax. It is Plug&Play and contains all necessary parts to convert the workstation into a fully functional calorimeter. icontrol software is not included. No service call is required for installation. OptiMax HFCal kit consisting of Order Number Product Description Quantity OptiMax HFCal box Calibration heater, 300 mm Adapter ST19,, with sealing ring CAN cable 100 cm icontrol HeatFlow License 1 46

47 OptiMax Accessories and Probes CAN cable 100 cm Length 100 cm OptiMax HFCal box can be attached on the left or right side of the OptiMax 120 mm x 40 mm x 170 mm (w, d, h) Calibration heater Alloy C-22 Ø 8 mm, 300 mm adapter, eccentric for calibration heater, including sealing ring Inner Ø 8 mm, ST Sealing ring for adapter Inner Ø 8 mm OptiMax Calorimetry Starter Kit OptiMax Calorimetry Starter Kit The OptiMax HFCal Starter Kit is a heat flow based, ready-to-use system to quickly obtain heat data of any chemical or physical reaction in a 1 L scale. The kit includes all parts required in just one single part number. The icontrol software and the HFCal license are included too. OptiMax Calorimetry Starter kit consisting of Order Number Product Description Quantity OptiMax Startet Kit for details see page OptiMax HFCal Kit icontrol Single Instrument License for details see page

48 48 Notes

49 icontrol Software for OptiMax icontrol Software for OptiMax Optional Accessories The software for experiment preparation, instrument control and data evaluation icontrol for single or multiple instruments icontrol for Office icare software maintenance icontrol provides the maximum amount of information from a single experiment. It uses a simple-tooperate user interface enabling EasyMax to be operated by either the PC software or in combination with the touchscreen. icontrol enables scientists to gain a comprehensive understanding of the chemical reaction under study. The combination of reactor data with information from METTLER TOLEDO analytical tools helps chemists in research and development reach appropriate con-clusions from each experiment, enabling them to make better decisions and complete projects faster. icontrol Software for OptiMax Order Number License type Description icontrol Single Instrument License Software license for experiment preparation, control and data evaluation for one instrument icontrol Multiple Instrument License Software license for experiment preparation, control and data evaluation for up to three instruments icontrol Office License Software license for experiment preparation and experiment evaluation icare for icontrol Instrument Software maintenance for instrument license icare for icontrol Office Software maintenance for office license 49

50 Compatibility List 1000 ml glass reactor and cover 1000 ml glass reactor and cover 500 ml glass reactor and cover 500 ml glass reactor and cover Pitched stirrer blade, upward, four impellers, Ø 45 mm, Alloy C Pitched stirrer blade, downward four impellers, Ø 45 mm, Alloy C Anchor blade, Ø 90 mm, Alloy C Anchor blade, Ø 69 mm, Alloy C Pitched-blade stirrer, upward four impellers, Ø 45 mm, glass Pitched-blade stirrer, downward four impellers, Ø 45 mm, glass Pitched stirrer blade, upward four impellers, Ø 38 mm, Alloy C Pitched stirrer blade, downward four impellers, Ø 38 mm, Alloy C Anchor blade, Ø 55 mm, Alloy C Pitched-blade stirrer, upward four impellers, Ø 38 mm, glass Pitched-blade stirrer, downward four impellers, Ø 38 mm, glass Bar type baffle, 15 mm x 249 mm, Alloy C Bar type baffle, 15 mm x 237 mm, Alloy C Temp. sensor, Alloy C-22, 1/ mm x 300 mm, incl. chip Temp. sensor, glass, 6 mm x 300 mm, incl. chip ph sensor OptiMax, incl. chip Reflux condenser glass, ST19, 250 mm x 40 mm Needed items 1) Stirrer shaft 2) Stirrer shaft 3) adapter for baffle 4) adapter, ST14 5) Stirrer shaft ml glass reactor Glass cover ml glass reactor cover ml glass reactor Glass cover ml glass reactor cover 50

51 Compatibility List 250 ml glass reactor and cover 1000 ml one-piece glass reactor 500 ml one-piece glass reactor 250 ml one-piece glass reactor Pitched stirrer blade, upward four impellers, Ø 38 mm, Alloy C Pitched stirrer blade, downward four impellers, Ø 38 mm, Alloy C Anchor blade, Ø 55 mm, Alloy C Pitched-blade stirrer, upward four impellers, Ø 38 mm, glass Pitched-blade stirrer, downward four impellers, Ø 38 mm, glass Half-moon stirrer blade, 19 mm x 71 mm, Half-moon stirrer blade, 19 mm x 54 mm, Half-moon stirrer blade, 19 mm x 43 mm, Bar type baffle, 15 mm x 249 mm, Alloy C Bar type baffle, 15 mm x 237 mm, Alloy C Temp. sensor, Alloy C-22, 1/ mm x 300 mm, incl. chip Temp. sensor, glass, 6 mm x 300 mm, incl. chip ph sensor OptiMax, incl. chip Reflux condenser glass, ST19, 250 mm x 40 mm Needed items 1) Stirrer shaft 2) Stirrer shaft 3) adapter for baffle 4) adapter, ST14 5) Stirrer shaft ml glass reactor Glass cover ml one-piece glass reactor ml one-piece glass reactor ml one-piece glass reactor 51

52 Characterize the Process While Optimizing the Chemistry In chemical and process development, experiment quality is key. METTLER TOLEDO s OptiMax is designed to help make better decisions faster. It executes experiments with great accuracy, providing critical and information-rich data. Often, chemistry can be understood only when additional information, such as the reaction mechanism or the kinetics, is available. Key reaction species including intermediates and by-products are easily monitored in real-time with ReactIR, an FTIR-based in-situ reaction analysis tool. The analysis is conducted in the reaction mixture itself, eliminating errors associated by taking samples, and allowing organic chemists to quickly understand if the correct reaction occurred and to observe its start- and endpoint. The precise temperature control and the high reproducibility of an experiment makes the OptiMax the ideal workstation to optimize crystallization processes when combined with the particle characterization system ParticleTrack. It provides immediate insight into the particle system, enabling chemists and chemical engineers to quickly screen experimental parameters and develop a scalable process in early process development. The ic software suite allows scientists and engineers within the pharmaceutical, chemical and specialty chemical industries to convert the data collected in their experiments into important process knowledge. It provides a unique perspective when it comes to integration of data sets from other equipment, and shares a common design, so users learn the software once and use many instruments. The seamless integration of complementary data sets contributes to the faster understanding of the process under investigation. For more information Mettler-Toledo AG, AutoChem Sonnenbergstrasse 74 CH-8603 Schwerzenbach, Switzerland Phone Fax autochem@mt.com Internet Subject to technical changes 11/2013 Mettler-Toledo AG, AutoChem Printed in Switzerland, B Quality certificate. Development, production and testing according to ISO Environmental man agement system according to ISO European conformity. The CE conformity mark provides you with the assurance that our products comply with the EU directives.