VISCOPLEX Pour Point Depressant technologies. High-performance solutions for low-temperature challenges

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1 VISCOPLEX Pour Point Depressant technologies High-performance solutions for low-temperature challenges

2 Solving low-temperature challenges for over 70 years Evonik's Oil Additives business line is the leading developer of high-performance lubricant additives and synthetic base fluids marketed under the brand names VISCOPLEX and VISCOBASE for use in automotive and industrial lubricants. Based on polyalkylmethacrylate (PAMA) chemistry, a comprehensive line of Pour Point Depressant (PPD) products delivers robust low-temperature performance that adapts to a variety of base oils, performance packages and viscosity modifiers. With over 70 years of PPD expertise, the Oil Additives specialists at Evonik partner with formulators to develop custom PPD solutions for the toughest lowtemperature challenges while providing dedicated technical support. The advantages of VISCOPLEX PPDs: Bringing customer-specific solutions through custom-designed PPDs Reliable, proven performance above industry standards Global technical support and supply security Help in achieving optimum performance for your product and application Paraffin crystal formation and relationship to cold flow Temperature Nucleation Crystal growth Agglomeration/gelation Without PPD Significant temperature reduction Improved cold flow With VISCOPLEX PPD Crystal size n-paraffins without VISCOPLEX PPD VISCOPLEX PPD 2

3 Continuing innovation with VISCOPLEX PPDs It s a well-known fact that most oils contain small amounts of waxy material. Less common is the know-how to select the ideal PPD solution to achieve optimal performance, meet used-oil pumpability requirements, and ensure compatibility with other components of the formulation. Evonik's Oil Additives Team has achieved this level of expertise through over 70 years of research, product development, close collaboration with leading industry formulators, and application testing of innovative polymer architectures. Evonik's VISCOPLEX PPDs are based on the versatility of polyalkylmethacrylate (PAMA) chemistry, whose general structure is as follows: CH 3 - (-CH 2 - C -) x CO 2 R Group R is a mixture of alkyl groups from C1 to C22. The Oil Additives specialists at Evonik carefully engineer the waxy alkyl groups in R and the chain-length distribution to match wax molecules in the oil, helping to achieve the best pour point depressant activity. How VISCOPLEX PPDs modify wax crystals at low temperatures Without VISCOPLEX PPD Crystallization of wax molecules below cloud point temperature With VISCOPLEX PPD Mainly lateral growth forms needles or plates Wax crystal structure continues to grow Large, structured 3D crystal network formation, crystal size > 100µm, oil ceases to flow Co-crystallization occurs between wax molecules and VISCOPLEX PPD crystalline units VISCOPLEX PPD modifies wax crystal growth Interlocking of wax crystals is prevented, leading to smaller and more random structure No aggregation of gel-like wax network, oil continues to flow without yield stress Crystalline unit formed by n-paraffins Crystalline unit formed by VISCOPLEX PPD VISCOPLEX Polymer backbone 3

4 Base stock alone does not determine which PPD is right for you There are many factors that affect the proper selection of the right PPD for a formulation. The Oil Additives specialists at Evonik can help identify key factors, evaluate options and fine-tune Pour Point Depressant choice to best meet formulators needs. Factors that affect PPD selection and treat rate: Base stock Other waxy components Detergents and friction modifiers Viscosity modifiers Test methods required by different specifications Low-temperature performance reversion Aged-oil pumpability requirements VISCOPLEX PPD performance in base stock and fully formulated oil ASTM D Yield Stress, Pa <140 <105 <70 <35 fail pass PPD 0.1wt% 150N Oil SAE 10W-40 PPD 0.1wt% VISCOPLEX PPD solutions to meet the most severe lowtemperature test requirements Mini-Rotary Viscometer (MRV TP-1) Yield Stress and Scanning Brookfield Technique (SBT) Gelation Index A significant challenge when selecting a PPD is the sometimes conflicting requirements among low-temperature tests, which have differences in cooling rates, shear rates, and conditioning times. The ideal PPD would provide the appropriate level of wax control to meet all required specifications, such as MRV TP-1 and SBT. Therefore, it is crucial to carefully consider all of the cold-temperature requirements of a lubricant, as a passing result in one test does not guarantee success in other tests. 4

5 VISCOPLEX PPD solutions for modern lubricant specifications Due to oxidation, aged-oil low-temperature rheology is an important specification in ILSAC GF-5. The ASTM D7528 ROBO bench test is an effective alternative to the costly Sequence IIIGA engine test. Developed by Evonik's Oil Additives Team, the ROBO test provides significant cost and time savings. Evonik offers ROBO technology to help customers screen PPDs and develop formulations meeting the GF-5 used oil specifications and the future GF-6 specifications. Not all PPDs that work in fresh oils work in aged oils Different PPD low-temperature performance in fresh 5W oil (at -35 C) versus aged oil (at -30 C) MRV TP-1 Viscosity, P PPD-1 PPD-2 PPD-3 fail pass 100 Fresh Used oil oxidized by ROBO 5

6 The ROBO test is an alternative to the Sequence IIIGA. TMC-certified ROBO units are utilized in both the Evonik Oil Additives Americas and Asia Pacific technology centers. VISCOPLEX PPDs a vital part of any formulation Regulations and industry standards are evolving rapidly. In such an environment of constant change, the value of a PPD comes from its ability to not only exceed these standards but also perform equally well with nearly any additive, DI package, viscosity modifier, or base stock. Formulators gain added product flexibility and the peace of mind that comes from knowing that, unlike some lubricant components, VISCOPLEX PPDs will continue to reliably provide excellent lowtemperature performance enhancement. VISCOPLEX PPD solutions for commercial viscosity modifiers SAE viscosity grade SAE 5W-30, meeting SAE J300 and ILSAC GF-5 low-temperature requirement VII chemistry Styrene- HE-OCP, HE-OCP, LE-OCP, Isoprene, 50 SSI 35 SSI 50 SSI 50 SSI VISCOPLEX PPD A A B B PPD treat rate, % MRV -35ºC, ASTM D4684 Viscosity, cp 17,600 17,500 22,900 20,700 Yield Stress, Pa <35 <35 <35 <35 6

7 VISCOPLEX PPD technology keeps pace with today s Group III and Group III+ base stocks Today s array of different refining technologies and global sourcing of crude oils results in a wide range of molecular structures within the wax present in oils. In addition, Group III and Group III+ base stocks, which are quite different from traditional base stocks, are highly saturated with long-chain hydrocarbons, necessitating new PPD technologies like those incorporated in VISCOPLEX PPDs. Performance of VISCOPLEX PPDs in Group III (4 cst) base 0.6wt.% /-30/-30-53/-52 /-57-51/-56/-59-53/-57/-60 Pour Point, ºC (ASTM D97) VISCOPLEX VISCOPLEX VISCOPLEX

8 Committed to ongoing support As industry trends and specifications shift, formulators may need to modify formulations to continue providing state-of-the-art fluids. With its broad PPD portfolio, Evonik's ability to custom-tailor one PPD to satisfy multiple formulations simplifies logistics for its customers. Evonik's Oil Additives Team is committed to providing ongoing support not just during your initial PPD selection, but also throughout fluid formulation, production and future development. VISCOPLEX versatility one PPD for multiple formulations Applications 5W-30 75W-140 ISO 46 THF (1) ATF (2) PPD treat rate, % ASTM D97, Pour Point, C ASTM D2983, Brookfield -40 C, cp N/A 143,000 (3) 42,000 12,800 (1) 9,400 (2) ASTM D4684, MRV -35 C Viscosity, cp 17,300 N/A N/A N/A N/A Yield stress, Pa <35 (1) Tractor hydraulic fluid: meeting John Deere J20D maximum viscosity specification of 20,000 cp at -40 C (2) Automatic transmission fluid: meeting DEXRON VI maximum viscosity specification of 15,000 cp at -40 C (3) Meeting J306 specification of 150,000 cp at -40 C Guide to VISCOPLEX PPD series selection VISCOPLEX series 1-1 series 1-2 series 1-3 series 1-4 series 1-6 series 1-7 series 1-8 series 10 series Robust PPDs for conventional formulations Tailored wax-interaction strength for maximum performance in modern lube formulations General purpose with VI lift For biodegradable lubricants 8

9 VISCOPLEX food grade PPD is kosher approved and halal certified. New VISCOPLEX PPD technology for food-grade applications VISCOPLEX is specially designed for use in Group III and white oil-based lubricants with incidental food contact. VISCOPLEX 1-135, which is NSF HX-1 approved, in combination with white oils can be a cost-effective alternative to synthetic base stocks when formulating high-performance food-grade lubricants used at very low temperatures. Temp / C Commercial white oil/kv40 C = 23cSt, PP = -12 C Treat rate / wt.% VISCOPLEX Up to 33 C Pour Point reduction VISCOPLEX PPD for environmentally friendly lubricants Demand for environmentally friendly lubricants is growing, and Evonik's PPDs help to address the unique low temperature challenges of these specialty fluids. VISCOPLEX series 10 PPDs are manufactured and delivered in biodegradable diluent oils and maintain the environmental characteristics of the finished lubricants. VISCOPLEX series 10 PPDs are designed to improve cold flow properties in vegetable oils, polyglycols and synthetic esters, and to stabilize oil fluidity during extended storage. 9

10 Evonik's Oil Additives Team a partner providing the leading PPD technologies A history of innovative PPD solutions Evonik offers its partners over 70 years of experience developing base stocks and additive technologies that exceed market and industry specifications. Evonik's Oil Additives Team: Developed the first modern PPD formulation based on API Group II stocks when the first API Group II oil was released Created the first PPD to meet test requirements after the introduction of the MRV TP-1 test method Helped solve low-temperature challenges when high-ethylene OCP VM entered the market Invented the innovative ROBO bench test and reduced the time and cost of identifying PPD solutions for agedoil low-temperature performance requirements Prepared for the future, the Oil Additives specialists at Evonik actively develop new PPDs for highly hydrogenated base stocks and other new requirements in the years ahead. 10

11 Canada France Germany United States China Japan Singapore Headquarters Regional offices Technology centers Manufacturing facilities Sales offices & representatives Experts wherever you need them As a part of Evonik Industries, the global market leader in specialty chemicals, Evonik's Oil Additives Team draws upon a robust and secure supply chain. The global scale of Evonik's oil additives operations helps ensure uninterrupted supply, rapid and localized production and efficient delivery. Contact Evonik's Oil Additives specialists today for low-temperature formulation and testing guidance. To request a copy of the Evonik's VISCOPLEX PPD treatise, scan the QR code, or visit evonik.com/oil-additives. 11

12 This information and all further technical advice is based on our present knowledge and experience. However, it implies no liability or other legal responsibility on our part, including with regard to existing third party intellectual property rights, especially patent rights. In particular, no warranty, whether express or implied, or guarantee of product properties in the legal sense is intended or implied. We reserve the right to make any changes according to technological progress or further developments. The customer is not released from the obligation to conduct careful inspection and testing of incoming goods. Performance of the product described herein should be verified by testing, which should be carried out only by qualified experts and is the sole responsibility of the customer. Reference to trade names used by other companies is neither a recommendation, nor does it imply that similar products could not be used. VISCOPLEX, VISCOBASE, DRIVON, DYNAVIS and NUFLUX are registered trademarks of Evonik Resource Efficiency GmbH. 05/2017 EVONIK INDUSTRIES AG v1 EUROPE, AFRICA, MIDEAST Evonik Resource Efficiency GmbH Kirschenallee Darmstadt Germany PHONE FAX oil-additives@evonik.com AMERICAS Evonik Oil Additives USA, Inc. 723 Electronic Drive Horsham, PA USA PHONE FAX Toll-free ASIA PACIFIC Evonik Oil Additives Asia Pacific Pte. Ltd. 3 International Business Park Nordic European Centre Singapore PHONE FAX

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