Extraction News Notes Blog

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1 Extraction News Notes Blog BY: Infinity Supercritical Staff TAGS: Supercritical CO2 Fluid Extraction, Cannabis, Oil Extraction Kiinja System Versus Infinity Supercritical CO2 Extraction System CO2 Extraction System Review Blog Industry Series Overall Comments: They offer 10-20L and 1,000 to 10,000 psi. Company: Relatively new to the Cannabis space, first time I've heard of them. Website: They use WordPress and Yoast SEO plugin. Last Google spider/cache was on November 1st. They use Google Analytics tracking ID: UA Website is not updated on any regular basis, and there is no content related material (for extraction, botanicals, etc.). Infinity maintains a website with additions on a daily basis, and a full publications resource. Infinity 10L System System: Collection: They offer only one collection vessel (2L), unsure of capacity to collect or prevent carryover of oil. Infinity has three at 1.5 L each, and we use electrostatic precipitation and filter to prevent any carry-over. Fractionation can be controlled by Back Pressure Valve(s), chiller temperature, and electrostatic precipitation. Infinity Collection Vessels

2 Kiinja System Versus Infinity Supercritical CO2 Extraction System 2 Extraction Vessel: Appears as though they offer a 5x5 or 10L and a 10x10 or 20L. The patent-pending innovation is the vessel which can be rotated. Looks like they have some type of electromechanical sealing/lid closure (more moving parts = more maintenance and possibility of failure). Infinity System is horizontal, no moving parts, and includes baskets which allow easy loading-unloading. Baskets also allow flash freezing from harvest, which allows extraction of high-value resin. Extraction Time: Infinity 10L Horizontal Extraction Vessel Based on modeling only to 2.2 hours. Actual testing will be done first quarter "Actual performance may vary and is not guaranteed. System projections based on engineering modeling. Actual system performance data expected Q " Modeling based on what - Cannabis trim, flower, hops, etc.? I think they're being very optimistic on the modeling. What we have found is that computer models don't work well in this type application, since the botanicals are never consistent (variety, size, moisture content, trim, flower, pellet type, etc.). Infinity has a 30/30 and 45/45 time. Oil Extract From Infinity Supercritical Machine Loading Quantity: They are basing the quantity of botanicals using a pelletized input material. The only thing I've seen pelletized is hops, and trying to extract oil from a pelletized product is longer, and not complete. In addition, to pelletize a botanical, it involves huge compression pressures, which results in heat. Heat kills the terpenes and flavinoids - which is exactly why a CO2 system is used (to preserve flavors). The Cannabis industry does not pelletize trim or bud. Extract Oil From Infinity Supercritical Machine

3 Kiinja System Versus Infinity Supercritical CO2 Extraction System 3 CO2 Pump: Unclear whether they use a diaphram pump (requires additional air compressor and additional chiller) or a liquid phase-change pump. A pump that can do 10,000 psi is either a very expensive large diaphram pump, or a Waters type needle plunger pump. Unless they have extensive testing with the pump and this application, they are in for a big surprise (pump failure, seal failure, etc.). It has taken us over 1.5 years to finally modify a pump so that it is a stable and has relatively maintenance free operation. That includes pump head modification, fabricating our own high pressure spring seals, etc. Infinity Liquid CO2 Pump With Heat Recovery CO2 Flow Rate and Temperature: Same. Pressures: They claim to go up to 10,000 psi, which is the full extraction range. Anything above 2,000 psi will extract all waxes and chlorophyll. That requires a great deal of post processing. Waters uses a system that goes up to that pressure as well, and for groups that want high pressure, most will purchase a Waters (which dominates the Denver market) that can also fractionize oil extract output into three vessels. Infinity goes up to 2,000 psi and output can be fractionalized into three collection vessels. Inside a Liquid CO2 Pump Mechanism Pressure Maintenance: How do they regulate pressure? Back pressure valve or valveless technology? Infinity uses a Swagelok BPV (Back Pressure Valve) to precisely regulate pressure, and a automated pressure sensor feedback loop, which is controlled by a VFD. The Variable Frequency Drive regulates the pump RPM, to maintain pressure. Set it, and it maintains pressure. The VFD also has ModBus which allow external communications to network with monitoring and control. Pressure Sensor Feedback Loop VFD

4 Kiinja System Versus Infinity Supercritical CO2 Extraction System 4 Automation: ABB full automation, which allows duplication of recipies, similar to Apeks. In the video they use ABB, which is very old-school and expensive, typically used for large industrial systems. Infinity uses standard semiautomated VFD and PID systems. Customer can upgrade to full automation, and can monitor the system via network computer, or via smartphone. Additional datalogging capabilities using Filemaker database software, which includes text alerts, maintenance alerts, etc. Piping: Unclear what diameter tubes they use. If they are using 10,000 psi compliant tubing, then they're probably using 1/16 or 1/8 inch tubing, which will clog (ask any Waters operator). Infinity uses 1/2 to 1/2 inch stainless steel tubing. No clogging. Infinity Semi-Automated System Control Cost: Their system looks very very expensive. While full automation is a nice option, if something doesn't work perfectly, you can't finish the run and lost product and result in costly downtime. The Infinity System is $90,000 for the base unit and $35,000 for 10L expansion modules. Since the system is semi-automated, you have the flexibility of running different recipes, and can change up the schedule on-the-fly. System not prone to any software glitches. Infinity Uses 1/2 and 1/4 Inch SS Tubing

5 Kiinja System Versus Infinity Supercritical CO2 Extraction System 5 Engineer Review: Looks like they have peer review. Infinity has a engineer peer reviewed system. Infinity System is Engineer Reviewed Overall Comments: Kiinja looks like a interesting system. They don't mention Cannabis or Hops on their website, which will not bode well for getting traffic to their website and selling product. Hard to tell if they've actually built a production mature system, since testing isn't scheduled (at least from what they say) to While the high-automation might seem attractive, unless the PLC is operating with good software 100 percent of the time, it will be frustrating to troubleshoot if something goes wrong. While Apeks systems are very popular, the big complaint with Apeks operators is the software. Cannabis Extract from Infinity System Addendum: One added item, which I did not address, since it wasn't clear how the extraction and collection vessels were heated with their system. In general, the vessels need some type of heating system. This can be a enclosed hot water bath (slow heating time and requires a chiller that is actually used for heated water), or solid state electric heat (fast response). Infinity uses the solid state heat on our system. Infinity Supercritical LLC Extraction News Notes Review Blog Copyright 2016

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