[ Delivery date ) Aromatic a mines and carcinogens ace. to EU Resolution ResAP(2008)1: Part 1 a, Part 1 b

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1 \'GO -..,.,., -. Cf ''C,, T inologif L L 0 QRV CTL GmbH 1 Chemical-Technological Laboratory Krackser StraBe Bielefeld Germany [CL -No /1 215 Rt. 17 South Rochelle Park [ Order date ) [ Delivery date ) [Date) [Article) [Article-No ) S T 1001SWO Aromatic a mines and carcinogens ace. to EU Resolution ResAP(2008)1: Part 1 a, Part 1 b Part 1a 64 LFGB ,3,4,9 nvestigation of aromatic a mines with carcinogenic, mutagenic, reprotoxic and GC/MS Analysis sensitising properties according to EU Resolution ResAP(2008)1 Detection limit: 1 ppm; Legal Limit: 30 ppm P..mounl Amine EC-No C?.S No Amount l<nmt:- EC-No Biphenyl-4-ylamine , 3'-Dimethoxybenzidine Benzidine ,3'-Dimethylbenzidine Chloro-o-toluidine ,4'-Methylenedi-o-toluidine Naphthylamine Methoxy-m-toluidine o-aminoazotoluene ,4'-Methylenebis-(2-chloroaniline) Nitro-o-toluidine Methyl-m-phenylenediamine Chloroaniline o-anisidine Methoxy-m-phenylenediamine Aminoazobenzene ,4'-Methylenedianiline Amino-2-ethoxynaphthaline 3,3'-Dichlorobenzidine Amino-3-fiuorophenol CAS-Jc Part 1b 64 LFGB ,3,4,9 nvestigation of carcinogens classified in Categories 1, 2 and 3 by the European GC/MS Analysis Commission and mentioned in the Council Directive 1967/548/EEC of 27 June 1967 according to EU Resolution ResAP(2008) 1 Detection limit 1 ppm Amounl AminE: EC-Nu GAS No '\mount ;: rllhh:; "C-i'>lo 4,4'-0xydianiline Para-phenylenediamine ,4'-Thiodianiline ,4 Xylidine o-toluidine lidine... 2,4,5-Trimethylaniline / - ( - r::as-ilo =below detection l1mit [GB) Tht: denoted re>ults art only valid for the tested sample W1t11cu' o Jr wntten conenl a mgle part c' lhs re orf,, allowed to be 1 orwdrderj o lh rd ' lr: Bank Sparkasse Gutersloh Address Krackser Stral1e 12 ;r:.>r) Account No Bielefeld, Germany [f Bank Code Managing Director Dr. rer nat. Gerald Prior i'.llll info@ctl-bielefeld.de SWFT/BG WELADED 1 GTL Based in Bielefeld /Hr -,f....,"1(. - j c\1-bielefeld.de!ban DE Register of Companies AG Bielefeld, HRB ell-tattoo. net VAT D No DE c\1-pmu.net

2 Cl-ki\1C T NOLOG LAB01ATORY CTL<B> GmbH 1 Chemical-Technological Laboratory Krackser StraBe Bielefeld 1 Germany CTL -No /1 215 Rt. 17 South [ Order date ] Rochelle Park [ Delivery date ] (Date] [Article] ace. to EU Resolution ResAP(2008)1 : Part 2 Part 2 nvestigation of Dyestuffs according to EU Resolution ResAP(2008)1 Detection limit: 5 mg/l DN in the up-to-date legislation GC/MS Analysis TLC Analysis Arnount Colour<H1! r.l-!o C:'l.S-'Jo Amount ;--:,,_,,,,,'1n( C-No. C' 1\S- Jo Acid Green Disperse Orange Acid Red Disperse Red Acid Violet Disperse Red Acid Violet Disperse Yellow Acid Yellow Disperse Yellow Basic Blue Pigment Orange Basic Green Pigment Red Basic Red Pigment Violet : Basic Red Pigment Violet : Basic Violet Solvent Blue Basic Violet Solvent Orange Basic Violet Solvent Red Disperse Blue Solvent Red : Disperse Blue Solvent Violet : Disperse Blue 124 ' Solvent Yellow Disperse Blue Solvent Yellow Disperse Blue solv.e.Qt_Yellow Disperse Orange / --+- ( c: ) - below detection limtl [GB] e denoted results are only valid for the test0d sample. Without our wnllen con.,ent no.tng:e part of trrs report,, ::lowed lv b6 or.varded to tbrrd 'ar Bank Sparkasse Guterstoh Address Krackser Stral1e 12 ifcnl Account No Bielefeld, Germany 11, Bank Code Managing Director Dr. rer. nat. Gerald Prior i"' '" info@ctl-bietefeld.de SWFT/BG WELADED 1 GTL Based in Bielefeld (He C!"'- ctl-bielefetd.de BAN DE Register of Companies AG Bielefeld, HRB ell-tattoo. net VATD No DE ctl-pmu.net

3 \fjj CHEMCAL- H 1JOLOGCAL LA'JGRATORY CTL GmbH 1 Chemical-Technological Laboratory Krackser Strae Bielefeld Germany 215 Rt. 17 South Rochelle Park CTL''-No /1 [ Order date ) [ Delivery date ] [Date J [Article) [Article-No ) [Test) ace. to EU Resolution ResAP(2008) 1: Part 3 Part 3 DN E29 nvestigation of Heavy Metals according to EU Resolution ResAP(2008)1 A nalys is ace. to EU ResAP(89)1 Detection limit: 0.01 ppm extraction using acidic perspiration Ar,lOunl Lin1it Arrount Lrmit (ppr.l) Elements or compc ll'd!pmn1 \PDil') Elme-Pt, or compol'rd (";i''". Arsenic (As) 2 Nickel (N i) Barium (Ba) 50 Lead (Pb) 2 As low as technically achievable Cadmium (Cd) 0.2 Selenium (Se) 2 Cobalt (Co) 25 Antimony (Sb) 2 Chromium (Cr), V 0.2 Tin (Sn) 50 Copper (Cu), soluble 25 Zinc (Zn) 50 Mercury (Hg) ( ) below detection lun11 [GB) The dbnoted results are only valid for the tested sample Wtlhout our written consent no ;tnqlt part of th1s report 1s allo.vect ) be fornjrdeu.o.l>ild par!ic Bank Sparkasse Gutersloh Address Krackser StraBe 12 [: 't! i Account No Bielefeld, Germany [f., Bank Code Managing Director Dr. rer. nat. Gerald Prior 1"' ' '1 info@ctl-bielefeld.de SWFT/BG WELADED 1 GTL Based in Bielefeld H: m1,.. );>'_. ctl-bielefeld.de BAN DE Register of Companies AG Bielefeld, HRB ell-tattoo. net VATD No DE ctl-pmu.net

4 C E t( T f\10 OG ':Aroq CTL 10 GmbH 1 Chemical-Technological Laboratory Krackser StraBe Bielefeld 1 Germany CTL'"-No /1 215 Rt. 17 South [ Order date ] Rochelle Park [ Delivery date ] [Date] [Article] PAH and SAP ace. to EU Resolution ResAP(2008)1: Part 4 Part 4 EPA, ZEK nvestigation of Polycyclic aromatic hydrocarbons (PAH) and Senzene-a-pyrene (SAP) according to ResAP(2008)1 Detection limit: PAH : 0.05 ppm as total; Senz-a-pyrene: 0.5 ppb Limit: PAH: 0.5 ppm as total; Senz-a-pyrene: 5 ppb Amount EPrne 1ts or compouncl Amorrnt FkcrTr 3,Jt.s or compound Naphthalene Senz(a)anthracene Acenaphthylene Chrysene Acenaphthene Senzo(b)fluoranthene Fluorene Senzo(k)fluoranthene Phenanthrene Dibenzo(a,h)anthracene Anthracene ndo (1,2,3-cd)pyrene Fluoranthene Senzo(g, h, i)perylene Pyrene Senzene-a-pyrene (SaP) Result as total: all below detection limit BELEFELD, 28TH SEPTEMBER 2010 Dr. rer. nat. ( ) below detect onlunr [Ge) TO? denoteo resl.il re only {Jiid for 1.he te.,ed ample Witti0U,)[f\";" ltsn coroopl ll,,rj pr',h;s report ' "liiov.cd b, )1.-JJr,J.:' :o h " 1 Bank Sparkasse Gotersloh Address Krackser Strafle 12 f<ilj Account No Bielefeld, Germany!: Bank Code Managing Director Dr. rer. nat. Gerald Prior [:n.d) info@ctl-bielefeld.de SWFT/BG WELADED 1 GTL Based in Bielefeld [H\.fi C 't''.ll', ctl-bielefeld.de BAN DE Register of Companies AG Bielefeld, HRB ctl-tattoo.net VATD No DE ctl-pmu.net

5 CHEMCAL- TL C4NOLOGCAL LAbORATORY CTL GmbH 1 Chemical-Technological Laboratory Krackser Stra!1e Bielefeld Germany TL'' - N o /1 215 Rt. 17 South [ Order date 1 Rochelle Park [ Delive1y date 1 [Date [Article 1 [Colour 1 Sterility ace. to EU Resolution ResAP(2008)1: Part 5 Part 5 nvestigation of Sterility Detection limit: < 1.0 x 1 oo CFU/g microbiological test: pseudomonads = King A, King B, Oxidase test ace. to ResAP(2008)1 : Rt:SUit. < 1.0 X 10 CFU/g [Gs) The denoted results are only valid for the tested sampls. Wrthout our Nntten consent no srngle part ol tills reportrs 1llowed to be forwarded to lhrd partie Bank Sparkasse Gutersloh Address Krackser Strat:\e 12 tl Oflj Account No Bielefeld, Germany,f:r ) Bank Code Managing Director Dr. rer. nat. Gerald Prior 1 1n dj info@ctl-bielefeld.de SWFT/BG WELADED 1 GTL Based in Bielefeld [Hnn1,;:"'q ctl-bielefeld.de BAN DE Register of Companies AG Bielefeld, HRB ell-tattoo. net VAT D No DE ctl-pmu.net

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