Tesoro Logistics Northwest Terminalling Company LLC Product Quality Control Guidelines
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1 Tesoro Logistics Northwest Terminalling Company LLC Product Quality Control Guidelines For All Products Bound for NWTC Storage Effective 06/19/2013
2 PRODUCT QUALITY CONTROL Scope It is Tesoro Northwest Terminalling Company s intent to meet or exceed the Product Quality requirements of its customers. To be able to achieve this end, Tesoro Northwest Terminalling Company (NWTC) has implemented a product quality-control procedure for product shipped to NWTC terminals. Complete product specifications that all shippers will be required to meet are shown in Attachment 1. Certificate of Analysis Product Quality Methods Tesoro NWTC shall require a Certificate of Analysis (C of A) for all products received into our Terminals. Tesoro NWTC will receive the C of A via the LGSTC C of A process which requires this document for every batch shipped on the Pipeline. For Denatured Ethanol receipts into NWTC Terminals a C of A must accompany the bill of lading. Tesoro NWTC will obtain the same samples as described in the next section and will test for key properties with field analyzers to confirm the correct product was shipped and delivered. Please note that for all Ultra Low Sulfur Diesel Fuels (ULSD) we will test 100% of all product received for sulfur content. Tesoro NWTC s quality assurance program is composed of three main components, namely: Sampling Procedures Testing Procedures Action Plans Aviation Tank Inspection Each Aviation tank is to be opened and visually inspected every 3 years. If cleaning is needed the tank will be cleaned before returning to service. Sampling Procedures Retention: Tank Sampling All terminal receipt samples will be retained for 30 days unless otherwise notified. Tanks will be sampled after each batch receipt or at least monthly using ASTM D 4057 Standard Practice for Manual Sampling of Petroleum and Petroleum Products to obtain representative samples of the product. As an alternative, composite samples of batches being delivered to the terminal tank may be used to represent product received into the tank. Ethanol Receipts from trucks will be randomly sampled and tested. Tank Composites Samples are to be collected and tested on a bi-weekly basis. ULSD receipts are to be to isolated tanks and a composite sample is to be collected and tested before the tank is to be opened up to the rack. In locations where having isolated tanks is impractical, i.e. tanks on running gauge to the truck rack, the following process is to be used: Incoming product is to be sampled and tested for sulfur within the first 15 minutes of the receipt June 2013 Page 2 Quality Control Guidelines
3 PRODUCT QUALITY CONTROL Pull and Test spot Pipeline delivery samples as practical during normally staffed business hours throughout the delivery. Upon completion of every delivery or sequence of deliveries, a composite sample from each ULSD tank must be obtained and tested individually. Marine Vessels (Barges) Testing Procedures Each barge compartment will be sampled and visually checked, the samples will be composited for each shipped and product grade, prior to discharge, using ASTM D 4057 Standard Practice for Manual Sampling of Petroleum and Petroleum Products. Marine Vessels (Barges) Upon Arrival At Pasco All testing is performed on a blended compartment composite sample for each product grade, before discharging to shore tankage (see Attachment 3 for Process to Evaluate Field Testing Results): ULSD Other Diesels Gasoline Ethanol Jet Visual Visual Visual Visual Clear and Bright API Gravity API Gravity API Gravity API Gravity API Gravity Flash Flash Octane Acidity Color Sulfur RVP Water Content Flash Point (TCC) Microseparometer (MSEP) Terminals This testing is performed on each pipeline / barge batch after it is received into a tank or on a composite sample from the receiving line at NWTC Terminals. ULSD product tank samples and/or spot samples are to be tested for sulfur immediately after they are obtained. The following tests will be performed (see Attachment 3 for Process to Evaluate Field Testing Results): ULSD Other Diesels Gasoline Ethanol (By Truck) Jet* Visual Visual Visual Visual Clear and Bright API Gravity API Gravity API Gravity API Gravity API Gravity Flash Flash Octane Acidity Color Sulfur RVP Ethanol content (quarterly GC)* Flash Point (TCC) Water content Distillation + Freeze Point + Microseparometer (MSEP) Note *: Run by outside laboratory at Boise or by Pasco Terminal Laboratory. Note +: Not run on Jet batches continuing on to Spokane. FULL TESTING A Full Test will be performed when a fungible storage tank is off-spec or when it can be reasonably assumed that there are problems with product quality. This testing includes all tests shown on the ASTM specification through a non- NWTC affiliated testing lab. June 2013 Page 3 Quality Control Guidelines
4 PRODUCT QUALITY CONTROL Test Records FULL TESTING CONFIRMATION TESTING Action Plans Situations 1. Product found, as a result of our quality assurance testing, not meeting the NWTC Specifications, in a barge compartment, or a NWTC tank. Results of full testing by an outside laboratory will be filed in a binder by shipper and by product. Records will be kept for five years after testing. The records will be kept at each terminal office. Each time a confirmation test is performed, the results will be recorded. A separate log will be kept at each station. The results will be reviewed periodically to assure that quality control measures are adequate to protect product integrity and provide the desired product oversight. Information obtained by tank testing will be shared upon request, but only with participating shippers. Additionally, any shipper may sample any tank for analysis at any time. Action plans are in place to deal with upsets or other conditions which may occur from time to time that are out of the ordinary. These plans describe the actions that will be taken when such an event occurs. Actions In a barge compartment Pasco Operations will notify the terminal and shipper of the incident and assume the lead role to resolve the problem. In NWTC Tank - NWTC personnel will: Isolate the product and Stop Sales. Notify all affected parties of the problem. Work with responsible Party to: Correct the product or remove it from the facility. Determine the cause of the problem. Review plans to prevent future occurrences Responsible Party will be responsible for all costs associated with the incident. These costs may include, but not be limited to: Trucking Product Down-grading (redesignation) Tank Cleaning Testing Pipeline Down-time Tank Storage Barge Demurrage June 2013 Page 4 Quality Control Guidelines
5 PRODUCT QUALITY CONTROL Oversight Program for Sub-Octane Gasoline This oversight program will have an initial phase for sub-octane entering into the Tesoro Logistics Pipe Line system for the purpose of collecting baseline data on the octane values t for each shipper. After that period there will be an on- going PQ sampling and testing program for Pipeline and NWTC tankage to verify that sub-octane will meet the minimum posted octane requirement for ethanol blended gasoline. Batches Entering Tesoro Logistics Pipeline Beginning on June 19th, 2013 Tesoro Logistics Pipe Line has agreed to draw 3 samples from each shipper for each grade of Sub-Octane product entering the pipeline at the Salt Lake Pump Station. The following tests will be run on these samples: 1.) The octane value (R+M/2) will be determined using ASTM D-2500 on the as-is sample. 2.) The octane value (R+M/2) will be determined after blending with ethanol to a 9:1 gasoline to ethanol ratio, 10% ethanol by volume. If all testing shows that minimum posted octane is reached for the ethanol blended samples, sampling and testing of in-coming sub-octane product for each shipper will convert to quarterly verification testing. Northwest Terminalling Company Tankage Beginning June 19th, 2013 and continuing on a monthly basis thereafter, a one gallon tank sample will be drawn for each sub-octane grade at Pasco, Boise, and Pocatello and tested as follows: 1.) The octane value (R+M/2) will be determined using ASTM D-2500 on the as-is sample. 2.) The octane value (R+M/2) will be determined after blending with ethanol to a 9:1 gasoline to ethanol ratio, 10% ethanol by volume. All test results will be blinded and made available to Position Holders upon request June 2013 Page 5 Quality Control Guidelines
6 Tesoro Logistics Northwest Terminalling Company LLC ATTACHMENT 1 PRODUCT SPECIFICATIONS Effective June 19, 2013 Replaces November 1, 2012 Version
7 Tesoro Northwest Terminalling Company Product Codes LGSTC Description Octane Destination Product Code R1 Regular Unleaded Sub-Octane 81.3 Pocatello Gasoline R4 Regular Unleaded Sub-Octane 84.0 Boise / Pasco Gasoline P8 Premium Unleaded Sub-Octane 88.0 Pocatello/Boise Gasoline P0 Premium Unleaded Sub-Octane 90.0 Pasco Gasoline 1D15 #1D 15 ppm sulfur motor All vehicle diesel fuel 2D15 #2D 15 ppm sulfur motor All vehicle diesel fuel B5-#2D 15 ppm sulfur motor vehicle diesel fuel Pasco Terminal Rack Sales Only Denatured Ethanol Boise / Pasco JET Commercial Jet Fuel Boise / Pasco Effective 06/19/2013 Page 2 Product Specifications
8 Tesoro Northwest Terminalling Company Origin Product Specification Denatured Ethanol ETOH Must Meet ASTM D a Product Property ASTM Test Specifications Method Minimum Maximum Note Appearance Bright & Clear - Appearance Visibly free of suspended or precipitated contaminants Ethanol, volume % D Methanol, volume % 0.5 Solvent-washed gum, D mg/100 ml Water content, volume %, E 203 or 1.0 E 1064 Denaturant content, volume %, Inorganic Chloride content, mass Mod. D ppm (mg/l) Method C Copper content, mg/kg Mod. D 1688, 0.1 Test Method A Acidity (as acetic acid D (56) CH3COOH), mass % (mg/l), Sulfur, ppm (wt./wt). D 2622, phe D D 3120 D 5453 D 7039 Sulfate, mass ppm D 7318 D 7319 D Effective 06/19/2013 Page 3 Product Specifications
9 Tesoro Northwest Terminalling Company Origin Product Specification #1D 15 ppm Sulfur Motor Vehicle Diesel Fuel 1 LGSTC Product Code: 1D15 ASTM Test Test Results Product Property Method Minimum Maximum Appearance Gravity-API D 1298 or 35.0 D 4052 Flash Point - F D 93, D56, 105 D3828 Distillation - F D 86, D2887, D % % 550 Color D Viscosity D c (104 F) Cloud Point F D 2500, -30 D57871; D5772; D5773 Corrosion, Cu strip D 130 No c (122 F) Total Sulfur ppm wt./wt. D 2622 or D 5453 D 7039 Cetane Number or D 613, D6890; D7170 Cetane Index D 4737, SLC Origin 11 Pasco Origin D Ash - Mass% Carbon Residue, Rams D 482 D On 10% Bottoms - Mass%` BS&W, Volume % D Thermal Stability 90 min. -% Reflectance Haze F LGSTC Scale Note Bright & Clear D Using Y unit with Green Filter D Notes: 1) Concentration & type of additives permitted only as approved by Northwest Terminalling Company. Effective 06/19/2013 Page 4 Product Specifications
10 Tesoro Northwest Terminalling Company Origin Product Specification Jet A 1 Pasco LGSTC Product Code: JET Product Property ASTM Method Test Minimum Results Maximum Note Acid No. Total (Mg KOH / G) D3242 Alt.-1 Smoke Point, mm D Alt 2 Smoke Point, mm D Naphthalenes, Vol % D Aromatics, Vol. % D Color, Saybolt D Condition, visual Corrosion, Cu Strip, 2 Hr at 100 C D130 Distillation - C D 86, D2887 Bright & Clear 10% % Report 90% Report End Point 300 Loss, Vol % 1.5 Residue, Vol % Required when Alt. 2 Smoke Point of 18.0 mm is used. Test method D6379 can be used with a maximum specification of 26.5 Thermal Stability Measurement, Filter Pressure Drop, mm of Hg D3241 Heater Tube Deposits; Code No. D3241 Flash Point D56, D93, D < 3 Conducted for 2.5 Hr at a control temperature of 260 C. Tube deposits shall always be reported by the visual method: A rating by the Tube Deposit Rating (TDR) optical density method is desirable but not mandatory. No peacock or abnormal color deposits Freezing Point, deg C D2386, D5972, D7153, D7154 Gravity-API D 1298, D Gum Existentmg/100 ml D381, IP540 7 Net Heat of Combustion, net, D4529, D3338, D (MJ/kg) (42.8) Particulate Contamination, mg/l -40 D5452, D Sulfur, Mass % D2622,D1266,D4294,D Sulfur, Mercaptan, Mass % D Viscosity C D Pipeline shipping requirement may be more strict. May be waived if the fuel is considered sweet by the Doctor Test (ASTM D4952)
11 Water Reaction, Interface Cond. A Water Separation Rating (MSEP) D1094 D B Notes: 1) Concentration and types of additives permitted only as approved by Northwest Terminalling Company. Metal deactivator 2.0 mg/l max on initial blending with 5.7 mg/l max. 2) For all grades use either Eq 1 or Table 1 in Test Method D4529 or Eq 2 in Test Method D3338. Test Method D4809 may be used as an alternative. In case of dispute, Test Method D4809 shall be used. Effective 06/19/2013 Page 5 Product Specifications
12 Tesoro Northwest Terminalling Company Origin Product Specification #2D 15 ppm Sulfur Motor Vehicle Diesel Fuel 1 Pocatello, Boise and Other Locations within Idaho LGSTC Product Code: 2D15 ASTM Test Method Test Minimum Results Maximum Product Property Note Appearance Bright & Clear Biodiesel (FAME) 30 ppm No Biodiesel is to be intentionally blended into diesel. Contamination must be limited to the standard shown. Gravity-API D 1298 or D 4052 Flash Point - F D 93, D3828, D Aromatics, Vol. % B Distillation - F D 86, D2887, D % End Point 698 Color D Viscosity - D Product is not for No. 2 c (104 F) Fuel Oil Sales Pour Point - F D 97 (2&3) Cloud Point F D 2500, (2&3) D5771, D5772, D5773, Corrosion, Cu strip 3 50 c (122 F) Total Sulfur, ppm (wt./wt.) D 130 No. 3 D 2622 or D 5453 D 7039 Cetane Number or D 613, D6890, D (4) Cetane Index (Procedure B) D 4737, 40 D967 Aromatics, Vol. % D Lubricity, μm D7688 Report Ash - Mass% D Carbon Residue, Rams D On 10% Bottoms - Mass %,Water and Sediment Volume % D Thermal Stability D Using Y unit with Green 90 min. - % Reflactance Filter Haze Rating D F CPC Scale Notes: 1) Concentration and types of additives permitted only as approved by Tesoro Northwest Terminalling Company. Product may contain Drag Reducing Agent (DRA) up to a maximum of 15 ppm cumulative active material. 2) When the cloud point is specified to be less than +10 F or the pour point less than 0 F, the minimum viscosity shall be 1.7 cst and the minimum 90% recovered temperature shall be waived. 3) Seasonal Materials are based on dates received into pipeline. Terminals must meet the requirement the following month. Period Max Cloud F Max Pour F 1-Apr to 31-Aug
13 1-Sep to 30-Sep Oct to 28-Feb Mar to 31-Mar Where cetane number by test method D 613 is not available, test method D 4737 can be used as an approximation. Minimum cetane index specifications must be met regardless of cetane number. Effective 06/19/2013 Page 6 Product Specifications
14 Tesoro Northwest Terminalling Company Origin Product Specification #2D 15 ppm Sulfur Motor Vehicle Diesel Fuel 1 Pasco, WA LGSTC Product Code: 2D15 ASTM Test Method Test Minimum Results Maximum Product Property Note Appearance Bright & Clear Biodiesel (FAME) 30 ppm No Biodiesel is to be intentionally blended into diesel. Contamination must be limited to the standard shown. Gravity-API D 1298 or D 4052 Flash Point - F D 93, D3828, D Aromatics, Vol. % D Distillation - F D 86, D2887, D % End Point 698 Color D Viscosity - D Product is not for No. 2 c (104 F) Fuel Oil Sales Pour Point - F D 97 (2&3) Cloud Point F D 2500, (2&3) D5771, D5772, D5773, Corrosion, Cu strip 3 50 c (122 F) Total Sulfur, ppm (wt./wt.) D 130 No. 3 D 2622 or D 5453 D 7039 Cetane Number or D 613, D6890, D7170 Cetane Index (Procedure B) Aromatics, Vol. % D 4737, D967 D (4) Lubricity, μm D7688 Report Ash - Mass% D Carbon Residue, Rams D On 10% Bottoms - Mass %,Water and Sediment Volume % D Thermal Stability D Using Y unit with Green 90 min. - % Reflactance Filter Haze Rating D F CPC Scale Notes: 1) Concentration and types of additives permitted only as approved by Northwest Terminalling Company. Product may contain Drag Reducing Agent (DRA) up to a maximum of 15 ppm cumulative active material. 2) When the cloud point is specified to be less than +10 F or the pour point less than 0 F, the minimum viscosity shall be 1.7 cst and the minimum 90% recovered temperature shall be waived. 3) Seasonal Materials are based on dates received into pipeline. Terminals must meet the requirement the following month
15 Period Max Cloud F 1-Apr to 31-Aug Sep to 31-Oct Nov to 28-Feb Mar to 31-Mar +24 4) Where cetane number by test method D613 is not available, test method D4737 can be used as an approximation. Minimum cetane index specifications must be met regardless of cetane number.. Effective 06/19/2013 Page 7 Product Specifications
16 Tesoro Northwest Terminalling Company Origin Product Specification B5-#2D 15 ppm Sulfur Motor Vehicle Diesel Fuel 1 Pasco, WA ASTM Test Method Test Minimum Results Maximum Product Property Note Appearance Bright & Clear Biodiesel (FAME) 30 ppm No Biodiesel is to be intentionally blended into diesel. Contamination must be limited to the standard shown. Gravity-API D 1298 or D 4052 Flash Point - F D 93, D3828, D Distillation - F D 86, D2887, D % End Point 698 Color D Viscosity - D Product is not for No. 2 c (104 F) Fuel Oil Sales Pour Point - F D 97 (2&3) Cloud Point F D 2500, (2&3) D5771, D5772, D5773, Corrosion, Cu strip 3 50 c (122 F) Total Sulfur, ppm (wt./wt.) D 130 No. 3 D 2622 or D 5453 D 7039 Cetane Number or D 613, D6890, D7170 Cetane Index (Procedure B) Aromatics, Vol. % D 4737, D967 D (3) Lubricity, μm D7688 Report Ash - Mass% D Carbon Residue, Rams D On 10% Bottoms - Mass %,Water and Sediment Volume % D Thermal Stability D Using Y unit with Green 90 min. - % Reflactance Filter Haze Rating D F CPC Scale Notes: 1) Concentration and types of additives permitted only as approved by Tesoro Northwest Terminalling Company. Product contains up to 5% FAME (biodiesel) and may contain Drag Reducing Agent (DRA) up to a maximum of 15 ppm cumulative active material. 3) Seasonal Materials are based on dates received into pipeline. Terminals must meet the requirement the following month. Period Max Cloud F 1-Apr to 31-Aug Sep to 31-Oct Nov to 28-Feb Mar to 31-Mar
17 3) Where cetane number by test method D613 is not available, test method D4737 can be used as an approximation. Minimum cetane index specifications must be met regardless of cetane number. Effective 06/19/2013 Page 8 Product Specifications
18 Tesoro Northwest Terminalling Company Origin Product Specification Regular Unleaded Sub-Octane Gasoline LGSTC Product Code: R1 Product Property ASTM Test Method Test Minimum Results Maximum Appearance Bright & Clear Gravity- 60 F D 1298 or Report D 4052 Color (2) Corrosion, Cu strip D F (50 C) Solvent-washed Gum Content D mg/100ml Lead Content - gm/gal at D None intentionally origin added. Mg Content - gm/gal at origin None None intentionally (MMT) added. Doctor test or: D 235 or Negative Mercaptan sulfur, mass % D (6) Sulfur, ppm (wt./wt.) D 2622 D1266, 80 ppm National D3120, D5453, D6929, D7039, D7220 Phosphorus, gms/gal D (1) Oxidation stability - minutes D Octane RON D 2699 Report MON D 2700 Report 80.0* R+M * 2 Benzene, volume. % D 3606 or 4.9 D 4053 Oxygen, wt.% None (3) Port Fuel Injector and Intake (4) Valve detergent additives Reid Vapor Pressure (5) Distillation (5) Driveability Index (5) Vapor/Liquid Ratio (5) * Shipper certifies that the batch will meet the minimum posted octane requirements at retail after the addition of 10 volume % ethanol Notes: 1) No additives or corrosion inhibitors containing phosphorus may be used in this gasoline. Phosphorus tests are not required on every batch. Product may contain Drag Reducing Agent (DRA) up to a maximum of 15 ppm cumulative active material. 2) This product will be undyed. 3) Oxygenates are not allowed in this fuel for shipments on pipeline. 4) The use of the Port Fuel Injector (PFI) and Intake Valve detergent additives is prohibited for pipeline shipments. DCA will be added as product is loaded into trucks at the terminal. 5) Refer to latest revision of Northwest Terminalling Company Gasoline RVP/Volatility Schedule and Gasoline RVP / Volatility Requirements 6) The Mercaptan Sulfur determination may be waived if the result of the doctor test (ASTM D 235) is negative. Effective 06/19/2013 Page 9 Product Specifications Note
19 Tesoro Northwest Terminalling Company Origin Product Specification Regular Unleaded Sub-Octane Gasoline LGSTC Product Code: R4 Product Property ASTM Test Method Test Minimum Results Maximum Appearance Bright & Clear Gravity- 60 F D 1298 or Report D 4052 Color (2) Corrosion, Cu strip D F (50 C) Solvent-washed Gum Content D mg/100ml Lead Content - gm/gal at D None intentionally origin added. Mg Content - gm/gal at origin None None intentionally (MMT) added. Doctor test or: D 235 or Negative Mercaptan sulfur, mass % D (6) Sulfur, ppm (wt./wt.) D 2622 D1266, 80 ppm National D3120, D5453, D6929, D7039, D7220 Phosphorus, gms/gal D (1) Oxidation stability - minutes D Octane RON D 2699 Report MON D * R+M * 2 Benzene, volume. % D 3606 or 4.9 D 4053 Oxygen, wt.% None (3) Port Fuel Injector and Intake (4) Valve detergent additives Reid Vapor Pressure (5) Distillation (5) Driveability Index (5) Vapor/Liquid Ratio (5) * Shipper certifies that the batch will meet the minimum posted octane requirements at retail after the addition of 10 volume % ethanol Notes: 1) No additives or corrosion inhibitors containing phosphorus may be used in this gasoline. Phosphorus tests are not required on every batch. Product may contain Drag Reducing Agent (DRA) up to a maximum of 15 ppm cumulative active material. 2) This product will be undyed. 3) Oxygenates are not allowed in this fuel for shipments on pipeline. 4) The use of the Port Fuel Injector (PFI) and Intake Valve detergent additives is prohibited for pipeline shipments. DCA will be added as product is loaded into trucks at the terminal. 5) Refer to latest revision of Northwest Terminalling Company Gasoline RVP/Volatility Schedule and Gasoline RVP / Volatility Requirements 6) The Mercaptan Sulfur determination may be waived if the result of the doctor test (ASTM D 235) is negative Effective 06/19/2013 Page 10 Product Specifications Note
20 Tesoro Northwest Terminalling Company Origin Product Specification Premium Unleaded Sub-Octane Gasoline LGSTC Product Code: P8 Product Property ASTM Test Method Test Minimum Results Maximum Appearance Bright & Clear Gravity- 60 F D 1298 or Report D 4052 Color (2) Corrosion, Cu strip D F (50 C) Solvent-washed Gum Content D mg/100ml Lead Content - gm/gal at D None intentionally origin added. Mg Content - gm/gal at origin None None intentionally (MMT) added. Doctor test or: D 235 or Negative Mercaptan sulfur, mass % D (6) Sulfur, ppm (wt./wt.) D 2622 D1266, 80 ppm National D3120, D5453, D6929, D7039, D7220 Phosphorus, gms/gal D (1) Oxidation stability - minutes D Octane RON D 2699 Report MON D 2700 Report 91.0* R+M Benzene, volume. % D 3606 or 4.9 D 4053 Oxygen, wt.% None (3) Port Fuel Injector and Intake (4) Valve detergent additives Reid Vapor Pressure (5) Distillation (5) Driveability Index (5) Vapor/Liquid Ratio (5) * Shipper certifies that the batch will meet the minimum posted octane requirements at retail after the addition of 10 volume % ethanol Notes: 1) No additives or corrosion inhibitors containing phosphorus may be used in this gasoline. Phosphorus tests are not required on every batch. Product may contain Drag Reducing Agent (DRA) up to a maximum of 15 ppm cumulative active material. 2) This product will be undyed. 3) Oxygenates are not allowed in this fuel for shipments on pipeline. 4) The use of the Port Fuel Injector (PFI) and Intake Valve detergent additives is prohibited for pipeline shipments. DCA will be added as product is loaded into trucks at the terminal. 5) Refer to latest revision of Northwest Terminalling Company Gasoline RVP/Volatility Schedule and Gasoline RVP / Volatility Requirements 6) The Mercaptan Sulfur determination may be waived if the result of the doctor test (ASTM D 235) is negative. Note Effective 06/19/2013 Page 11 Product Specifications
21 Tesoro Northwest Terminalling Company Origin Product Specification Premium Unleaded Sub-Octane Gasoline LGSTC Product Code: P0 Product Property ASTM Test Method Test Minimum Results Maximum Appearance Bright & Clear Gravity- 60 F D 1298 or Report D 4052 Color (2) Corrosion, Cu strip D F (50 C) Solvent-washed Gum Content D mg/100ml Lead Content - gm/gal at D None intentionally origin added. Mg Content - gm/gal at origin None None intentionally (MMT) added. Doctor test or: D 235 or Negative Mercaptan sulfur, mass % D (6) Sulfur, ppm (wt./wt.) D 2622 D1266, 80 ppm National D3120, D5453, D6929, D7039, D7220 Phosphorus, gms/gal D (1) Oxidation stability - minutes D Octane RON D 2699 Report MON D 2700 Report 92.0* R+M Benzene, volume. % D 3606 or 4.9 D 4053 Oxygen, wt.% None (3) Port Fuel Injector and Intake (4) Valve detergent additives Reid Vapor Pressure (5) Distillation (5) Driveability Index (5) Vapor/Liquid Ratio (5) * Shipper certifies that the batch will meet the minimum posted octane requirements at retail after the addition of 10 volume % ethanol Notes: 1) No additives or corrosion inhibitors containing phosphorus may be used in this gasoline. Phosphorus tests are not required on every batch. Product may contain Drag Reducing Agent (DRA) up to a maximum of 15 ppm cumulative active material. 2) This product will be undyed. 3) Oxygenates are not allowed in this fuel for shipments on pipeline. 4) The use of the Port Fuel Injector (PFI) and Intake Valve detergent additives is prohibited for pipeline shipments. DCA will be added as product is loaded into trucks at the terminal. 5) Refer to latest revision of Northwest Terminalling Company Gasoline RVP/Volatility Schedule and Gasoline RVP / Volatility Requirements 6) The Mercaptan Sulfur determination may be waived if the result of the doctor test (ASTM D 235) is negative Effective 06/19/2013 Page 12 Product Specifications Note
22 TESORO NORTHWEST TERMINALLING COMPANY Product Specification Gasoline RVP/Volatility Schedule Boise & Pocatello Terminals Pasco Terminal Ship Dates Class at P/L origin Class at Terminal Class at P/L origin Class at Terminal Jan 1 15 E-5 E-5 E 5 E 5 Jan E-5 E-5 E 5 E 5 Feb 1 15 E-5 E-5 E 5 E 5 Feb D-4 E-5 D 4 E-5 Mar 1 15 C-3 D-4 A-4 D-4 Mar A-4 D-4 A 4 A 4 Apr 1 15 A-3 D-4 A 4 A 4 Apr A-3 A-3 A 4 A 4 May 1 15 A-3 A-3 A 4 A 4 May A-2 A-3 A-3 A 4 June 1 15 A-2 A-2 A-3 A-3 June A-2 A-2 A 2 A 3 July 1 15 A-2 A-2 A 2 A 2 July A-2 A-2 A 2 A 2 Aug 1 15 A-2 A-2 A 2 A 2 Aug A-2 A-2 A 2 A 2 Sept 1 15 A-2 A-2 A 2 A 2 Sept B-2 B-2 C-3 C 3 * Oct 1 15 C-3 C-3 D-4 D 4 * Oct C-3 C-3 D-4 D 4 * Nov 1 15 D-4 D-4 D 4 D-4 Nov D-4 D-4 D 4 D-4 Dec 1 15 E-5 E-5 E 5 E 5 Dec E-5 E-5 E 5 E 5 LGSTC maintains the right to specify the RVP of any gasoline it receives into its systems in order to meet RVP requirements at NWTC terminals. Refers to Class designation as specified in ASTM D 4814 * Pasco Gasolines not to be delivered into Southern Idaho during these periods. Class RVP Max. psi 10% Dist. Pt. F Max Gasoline RVP / Volatility Requirements Vapor Pressure and Distillation Class Requirements 50% Dist. Pt. F Min 50% Dist. Pt. F Max 90% Dist. Pt. F Max Dist. End Pt. F Max Dist. Resid ue Vol. % DI Max * Class Vapor Lock Class T V/L F Min AA A B C D E Note *: Driveability Index is calculated as follows: Driveability Index (DI) = 1.5 T T T F (1.33 C) X Ethanol Volume % (ethanol factor is zero for products delivered without ethanol). Note: Product received at NWTC Terminals must not contain MTBE. Effective 06/19/2013 Page 13 Product Specifications
23 Tesoro Northwest Terminalling Company ATTACHMENT 3 PROCESS TO EVALUATE FIELD TESTING RESULTS
24 Tesoro Northwest Terminalling Company Process To Evaluate Field Testing Results Compare Sample Result to Tesoro NWTC Spec. Is result within NWTC Spec + Tolerance? No Retest and average Both sets of results Yes Is Average Result within NWTC Spec + Tolerance? No Isolate Product and work with Shipper's to resolve Problem Document Result and Accept Product Yes June 2013 Page 2 PROCESS TO EVALUATE FIELD TESTING RESULTS
25 Tesoro Northwest Terminalling Company Field Test Tolerances For Products Max or Min Tolerance Action Gasolines RVP Max 0.3 psi See Flowchart. Octane (R+M)/2 Min 0.6 for >= 88 See Flowchart. and 0.7 for < 88 Appearance Bright & Clear If product appears hazy or contains visible particulate mater, isolate product in a tank to allow it to settle. Contact shipper and CSC. API - Gravity Min 50.0 deg API If below 50 deg API, have sample tested for distillation. Notify Shipper and CSC of possible contamination. Diesel Flash Min 7.0 Deg F See Flowchart. Sulfur Max Acceptance See Flowchart Limit Visual Bright & Clear, No Dye API Gravity Min 0.5 deg API See Flowchart. Ethanol (ASTM D4806) Water Content, Vol % Max 1.0 See Flowchart. Acidity, mass % Max See Flowchart If product appears hazy or contains visible particulate mater, isolate product in a tank to allow it to settle. If product appears to have dye in it, contact shipper and CSC. Test product for dye. If it has dye, keep product isolated. Visual API Gravity Bright & Clear If product appears hazy or contains visible particulate mater, isolate product in a tank to allow it to settle. 0.5 deg API See Flowchart. Jet (Run by Outside Laboratory, except at PASCO) Condition None No Tolerance allowed. Must meet specification when all tests are averaged. If results do not meet specification, isolate product, and API Gravity notify shipper and CSC. 0.5 deg API Must be within test tolerance of the gravity as shipped by Shipper when all tests are averaged. Wtd Average may be used in tanks with a heel of previous product. If results don't meet this requirement, isolate product, and notify shipper and CSC. Color None No Tolerance allowed. Must meet specification when all tests are averaged. If results do not meet specification, isolate product, and notify shipper and CSC. Flash Point (TCC) None No Tolerance allowed. Must meet specification when all tests are averaged. If results do not meet specification, isolate product, and notify shipper and CSC. Distillation None No Tolerance allowed. Must meet specification when all tests are averaged. If results do not meet specification, isolate product, and notify shipper and CSC. Freeze Point None No Tolerance allowed. Must meet specification when all tests are averaged. If results do not meet specification, isolate product, and notify shipper and CSC. MSEP None No Tolerance allowed. Must meet specification when all tests are averaged. If results do not meet specification, isolate product, and notify shipper and CSC. June 2013 Page 3 PROCESS TO EVALUATE FIELD TESTING RESULTS
26 Tesoro NWTC Response Procedure Potential DRA Over Injection LGSTC notifies NWTC CSR that a refined product batch with a DRA concentration potentially higher than 15 ppm has been or may be delivered to a NWTC terminal. Discuss the potential need to temporarily discontinue DRA injection into the suspect product being delivered to the terminal Estimate DRA ppm in the suspect product batch and/or in the affected tank(s)* Yes Isolate suspect product to the extent possible and maintain rack operation with remaining tankage. Capture the following samples, as appropriate*: An all-level (composite) sample and various tank level samples (as appropriate) from the affected tank(s) A composite receipt sample from the pipeline (if available) The composite pipeline sample from LGSTC's Salt Lake Station (if appropriate) Retain additional samples for future testing Is the suspect product believed to exceed 15 ppm DRA?* Yes Can suspect product be isolated in the terminal? No CQMPC Document Ship appropriate* product samples via overnight courier to: CSPG: Elvira Spesikova 1000 So. Pine Ponca City, OK Notify the CSPG at that: The sampled are in route, An expedited turnaround of the lab analysis is necessary, and They are to contact the NWTC CSR (and/or others if necessary*) with the lab results CSPG communicates lab results to the NWTC CSR No (and/or others as requested) Notify all affected customers of the potential over injection, including estimated DRA concentration levels and timing to receive lab analysis. Give each customer the option to lock out their rack liftings of the suspect product. Lock out rack liftings of the suspect product at customer's request (if any), pending customer notification and concurrence to continue lifting Yes Is suspect product believed to exceed 15 ppm DRA?* No Notify affected customers of lab results and give each of them the option to lock out their rack liftings of the suspect product. Yes Were customers notified of potential over injection? No Any customers elect to lock out the suspect product? Yes Work with subject customer(s) to develop and implement an action plan to get them unlocked on the suspect product* Release isolated product for rack lifting No Perform LI or NLI * With appropriate support and council from LGSTC Commodity Quality and Measurement Process Consultant (CQMPC) Perform NLI June 2013 Page 4 PROCESS TO EVALUATE FIELD TESTING RESULTS
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