ACE GLASS. Benchtop Reactors. Filter Reactors Pressure Reactors

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1 ACE GLASS Benchtop Reactors Filter Reactors Pressure Reactors

2 2 Table of Contents Item Page Filter Reactors... 3 Benchtop All-in-One Reactor Pressure Reactors Reactor Accessories... 9,20 Temperature Controllers New Bench Stand Welcome to the new Ace Glass bench reactor brochure! We have compiled the bulk of our unique and exclusive bench scale reactors and accessories into this easy-to-use catalog. Many of the systems herein feature our exclusive Ace-Threds safer and easier to use in both filter and pressure reactor applications. Choose either jacketed or non-jacketed flasks to fit your laboratory needs. Ace s unique filter reactor design gives you full flexibility to capture both filtrate and supernatant. Reactions can be carried out in completely closed temperature and pressure systems. Our pressure reactors provide added capability so you can run at higher pressures, or with vacuum vs. standard reaction flasks. We are also pleased to introduce our new J-Kem temperature controllers pg. 47), complete with data-logging capability and precise temperature control, and our brand new bench reactor stand assembly (pg. 46). If you have a more custom need, please contact an Ace Glass Tech Service Engineer through the Tech Support tab on our website at Or call in North America ( worldwide) and ask for Tech Services to discuss your application and needs. See the Ace General Catalog for more information, and for larger systems up to 200 Liters. Whether it s a full system ready to run, individual components, or even a custom system designed specifically for you, Ace Glass can deliver. Disclaimer: Prices and specifications in this brochure are subject to change with and without notice. Please contact ACE customer service to verify specifications and pricing. Ways to Order PHONE FAX CREDIT CARD VISA MasterCard American Express MAIL P.O. Box 688 Vineland, NJ WEB SITE sales@aceglass.com INTERNATIONAL export@aceglass.com ACE Glassware Discounts All ACE-manufactured glassware, identified with a spade ( ), listed in this brochure is subject to the following dollar value discounts. Items marked by a star ( ) or that have no designation whatsoever are not subject to this discount. 10% on purchases of $ and over.12% on purchases of $ and over.15% on purchases of $ and over Terms: Net 30 days (Domestic only) ACE GLASS ACCEPTS

3 Filter Reactors 3 ACE Filter Reactors allow single or multi-step reactions and filtrations in the same vessel. Stirrer Motor Major Design Features 100mL to 6000mL standard Unjacketed or Jacketed All inert materials Reactions at ambient or pressure conditions Filtering by vacuum and/or pressure Removable/changeable filters screen or glass wide choice of porosities Mechanical agitation Chuck 8124 Clamp 6517 Reactor Body 6384 PTFE Agitator 8089 PTFE Adapter Shaft 8075 Bearing 8066 Head 6527/6528/6529 Typical Assembly Support Stand Clamp Holder Chain Clamp Bottom drain valve Easy assembly/disassembly for cleaning Valve 5839 w/5844 Adapter Filter Support 5848 Support Stand 13550

4 4 Filter Reactors 8075 Stirring Shaft 8066 Bearing 6527/6528/6529 Head 6517 Clamp 7855 CAPFE O Ring Reactor Body 8089 Agitator 6384 Unjacketed Filter Reactor «Rugged heavy wall Reactor with 60 (2.4 inch), 100 (4 inch), or 150 (6 inch) Schott flange with O Ring groove at top, for connection to 6527, 6528 or 6529 Jointed Head, with 6517 Quick Release Clamp. Bottom has an Ace-Thred (internal glass thread) for installing (size 50) or (size 80) Bottom Adapter with filter support and drain valve. Head has three 24/40 joints on 60 size; four 24/40 joints on 100 and 150 sizes. Complete item consists of: Reactor Body with CAPFE O Ring, Head with Joints, Clamp, PTFE Bottom Adapter with CAPFE O Ring (with perforated plate #80 Thread only), retainer ring, 350 micron polypropylene screen support and 100 micron polyethylene support, 5844 Adapter, 5839 Shutoff Valve (optional larger valve is available), 8066 Bearing, 8075 Stirring Rod, and 8089 Multipaddle Agitator. For replacement glass fritted support, polyethylene support or polypropylene screen, see 5848 or For condenser and funnel, see 6029 and 7298; stoppers with 24/40 joints, see For stirring motor, see Motor; for Chuck, see Flange I.D., (in.) Bottom Thread Size Body I.D., Approx. Depth*, Replacement CAPFE O Ring Cap., ml (2.4) # (2.4) # (4) # (4) # (6) # (6) # *Depth measurements: Codes -115,-121 and -125 measured from top of flange to seal on bottom thread; Code -129, add 90 for cutdown top and bottom; Codes -133 and -137 add 65 for bottom cutdown. 5838/5857 Bottom Adapter w/filter Support (#50 or #80 3/8" fpt) 5844/12770 Adapter (3/8" mpt 1/4" fpt/ 3/8" mpt 3/8" mpt**) 5839 Bottom Valve (**For #80, also available with 1/2" mpt.) Stand and Clamps not included.

Filter Reactors 5 6384 Unjacketed Filter Reactor, Pressure Version Heavy wall glass reactor available with 60 (2.

Reactor bottom has an Ace-Thred for installing a 5838-83 (size 80) or 5857-86 (size 50) adapter with a filter support and bottom drain valve.

The 150 head has a #15 Ace-Thred center neck, (4) #15 and (1) #7 Ace-Thred side necks. The Ace- Threds allow for vacuum or pressure applications and for easy draining of material out of the reactor.

5 Filter Reactors Unjacketed Filter Reactor, Pressure Version Heavy wall glass reactor available with 60 (2.4-inch), 100 (4-inch), or 150 (6-inch) diameter Schott flange with O-Ring groove at top. Connects to #6433 head with a #6517 Quick Release clamp. Reactor bottom has an Ace-Thred for installing a (size 80) or (size 50) adapter with a filter support and bottom drain valve. The 60 reactor head has a #15 Ace-Thred center neck, (2) #15 and (1) #7 Ace-Thred side necks. The 100 head has a #15 Ace-Thred center neck, (3) #15 and (1) #7 Ace-Thred side necks. The 150 head has a #15 Ace-Thred center neck, (4) #15 and (1) #7 Ace-Thred side necks. The Ace- Threds allow for vacuum or pressure applications and for easy draining of material out of the reactor. The main bearing, funnel and condenser are designed to connect to the threds on the head via compression bushing connections. The #7 Ace-Thred is used for connecting a ¼ inch O.D. tubing fitting to allow for a direct connection to a pressure source or a #6448 pressure manifold. Complete item consists of: reactor body with CAPFE O-Ring, head with Ace Threds, quickclamp, PTFE bottom threaded adapter and valve with CAPFE O-Ring, retainer ring, 350 micron polypropylene screen support, 100 micron polyethylene support, 5844 adapter, 8044 bearing, 8075 stir rod, 8089 paddle agitator, 6024 condenser, 7299 addition funnel and #7 Ace-Thred bushing. Size 80 bottom adapter also comes with a perforated glass plate support. Pressure manifold (page 34), stand and clamps are optional. For replacement glass fritted discs and supports see 5848 or Flange I.D., (in.) Bottom Thread Size Body I.D., Approx. Depth*, Replacement CAPFE O Ring Cap., ml (2.4) # (2.4) # (4) # (4) # (6) # (6) # *Depth measurements: Codes -225,-231 and -235 measured from top of flange to seal on bottom thread; Code -239, add 90 for cutdown top and bottom; Codes -243 and -247 add 65 for bottom cutdown. «35 C 8075 Stirring Shaft 8044 Bearing 6433 Head 6517 Clamp 7855 CAPFE O Ring Reactor Body 8089 Agitator 5838/5857 Bottom Adapter w/filter Support (#50 or #80 3/8" fpt) 5844/12770 Adapter (3/8" mpt 1/4" fpt/ 3/8" mpt 3/8" mpt**) Filter Discs 5839 Bottom Valve Clamps, Stand and Support Shelf not included. (**For #80, also available with 1/2 inch mpt.)

6 Filter Reactors 6386 jacketed Filter Reactor «6527/6528/ 6529 Head 6517 Clamp 7855 CAPFE O Ring 6386-16 Jacketed Reactor Body 8089 Agitator 8075 Stirring Shaft 8066 Bearing Rugged heavy wall

6 6 Filter Reactors 6386 jacketed Filter Reactor «6527/6528/ 6529 Head 6517 Clamp 7855 CAPFE O Ring Jacketed Reactor Body 8089 Agitator 8075 Stirring Shaft 8066 Bearing Rugged heavy wall Reactor, jacketed for cooling and/or heating of reaction material. With 60 (2.4 inch), 100 (4 inch), or 150 (6 inch) Schott flange with O Ring groove at top, for connection to 6533 Head, with 6517 Quick Release Clamp. Bottom has an Ace-Thred (internal glass thread) for installing (size 50) or (size 80) Bottom Adapter with filter support and drain valve. Body is jacketed with size 28/15 O Ring ball joints on inlet/outlet, sealed tangentially for more efficient circulation. Head has three 24/40 joints on 60 size; four 24/40 joints on 100 and 150 sizes. Complete item consists of: Reactor Body with CAPFE O Ring, Head with joints, Clamp, PTFE Bottom Adapter with CAPFE O Ring (with perforated plate #80 Thread only), retainer ring, 350 micron polypropylene screen support and 100 micron polyethylene support, 5844 Adapter, 5839 Shutoff Valve (optional larger valve is available), Non-Flaking 8066 Bearing, 8075 Stirring Rod, 8089 Multipaddle Agitator. For replacement glass fritted support, polyethylene support or polypropylene screen, see 5848 or For condenser and funnel, see 6029 and 7298; stoppers with 24/40 joints, see For stirring motor, see Motor; for Chuck, see O Ring Ball Joint Connectors Flange I.D., (in.) Bottom Thread Size Body I.D., Approx. Depth*, Top CAPFE O Ring Cap., ml (2.4) # (2.4) # (4) # (4) # (6) # (6) # *Depth measurements: Codes -40,-45 and -50 measured from top of flange to seal on bottom thread; Code -55, add 90 for cutdown top and bottom; Codes -60 and -65 add 65 for bottom cutdown. For a complete listing of recirculating chillers, please see the Ace General Catalog, 5838/5857 Bottom Adapter w/filter Support (#50 or #80 3/8" fpt) 5844/12770 Adapter (3/8" mpt 1/4" fpt/ 3/8" mpt 3/8" mpt**) 5839 Bottom Valve (**For #80, also available with 1/2 inch mpt.) Stand and Support Shelf not included.

Filter Reactors 7 6386 jacketed Filter Reactor, Pressure Version Heavy wall glass reactor, jacketed version for cooling or heating of reactor. Available with 60 (2.

Reactor bottom has an Ace-Thred for installing a 5838-83 (size 50) or 5857-86 (size 80) adapter with a filter support and bottom drain valve.

7 Filter Reactors jacketed Filter Reactor, Pressure Version Heavy wall glass reactor, jacketed version for cooling or heating of reactor. Available with 60 (2.4-inch), 100 (4-inch), or 150 (6-inch) diameter Schott flange with O-Ring grove at top. Connects to #6433 head with a #6517 Quick Release clamp. Reactor bottom has an Ace-Thred for installing a (size 50) or (size 80) adapter with a filter support and bottom drain valve. Jacket inlet/outlet are size 28/15 O-Ring ball joint connections, sealed tangentially for more efficient circulation. The 60 reactor head has a #15 Ace-Thred center neck, (2) #15 and (1) #7 Ace-Thred side necks. The 100 head has a #15 Ace-Thred center neck, (3) #15 and (1) #7 Ace-Thred side necks. The 150 head has a #15 Ace-Thred center neck, (4) #15 and (1) #7 Ace-Thred side necks. The Ace-Threds allow for vacuum or pressure applications and for draining material out of the reactor. The main bearing, funnel and condenser are designed to connect to the threds on the head via compression bushing connections. The #7 Ace-Thred is used for connecting a ¼ inch O.D. tubing fitting to allow for a direct connection to a pressure source or a #6448 pressure manifold. Complete item consists of: reactor body with CAPFE O-Ring, head with Ace Threds, quickclamp, PTFE bottom threaded adapter and valve with CAPFE O-Ring, retainer ring, 350 micron polypropylene screen support, 100 micron polyethylene support, 5844 adapter, 8044 bearing, 8075 stir rod, 8089 paddle agitator, 6024 condenser, 7299 addition funnel and #7 Ace-Thred bushing. Size 80 bottom adapter also comes with a perforated glass plate support. Pressure manifold (page 34), stand and clamps are optional. For replacement glass fritted discs and supports see 5848 or Flange I.D., (in.) Bottom Thread Size Body I.D., Approx. Depth*, Top CAPFE O Ring Cap., ml (2.4) # (2.4) # (4) # (4) # (6) # (6) # *Depth measurements: Codes -107, -110 and -115 measured from top of flange to seal on bottom thread; Code -120, add 90 for cutdown top and bottom; Codes -124 and -128 add 65 for bottom cutdown. «35 C 8075 Stirring Shaft 8044 Bearing 6433 Head 6517 Clamp 7855 CAPFE O Ring Jacketed Reactor Body O Ring Ball Joint Connectors 8089 Agitator 5844/12770 Adapter (3/8" mpt 1/4" fpt/ 3/8" mpt 3/8" mpt**) Stand and Support Shelf not included Bottom Valve (**For #80, also available with 1/2 inch mpt.)

8 Filter Reactors Small Volume 9534 Stirring Shaft 8066 Bearing 6381 Small-volume filter Reactor with 45/50 joint at top and #50 Ace-Thred (internal glass thread) at bottom that accepts a 5838-83

8 8 Filter Reactors Small Volume 9534 Stirring Shaft 8066 Bearing 6381 Small-volume filter Reactor with 45/50 joint at top and #50 Ace-Thred (internal glass thread) at bottom that accepts a (size 50) Bottom Adapter with filter support and drain valve. Head has a 19/38 center neck and three 14/20 side necks. Complete item consists of: Reactor Body, Head with Joints, Clamp, PTFE Bottom Adapter with CAPFE O Ring, 350 micron polypropylene screen support, 100 micron polyethylene support, 5844 Adapter, Shutoff Valve, Non-Flaking Bearing, Stirring Rod, Blade. For glass fritted support replacements for polypropylene screen and polyethylene support, see 5848 or 5814; for condensers see 6024; for addition funnel see For stirring motor, see 13507; for Chuck, see Cap., ml Top Joint Bottom Thread Size Body I.D., Approx. Depth, Use Joint Clamp /50 # /50 # Head, only Body, only Complete Cap., ml Head 6381 Body Description Adapter, PTFE, 3 8" mpt ¼" FPT, only Bottom Adapter, #50 3 8" FPT, only Bottom Shutoff Valve, ¼" mpt ¼" Tube, PTFE Clamp, Plastic, 45/ Bearing, 19/22, Stopper, 14/ Description Stirring Shaft, 6 x 318 long, with button Stirring Blade, PTFE Optional Accessories PTFE Sleeves 14/20/Pk PTFE Sleeves 19/38/Pk PTFE Sleeves 45/50/Pk Thermometer Adpt., 14/ Blade 5838 Bottom Adapter w/filter Support (#50 3/8" fpt) Adapter (3/8" mpt 1/4" fpt 5839 Valve Stand and Clamp not included.

9 Filter Reactors 9 Instatherm Heated Filter Reactor Use with either regular or pressure version head and accessories Filter Reactor, Unjacketed Instatherm, Body only Same rugged, heavy-wall Reactor as 6384, except Instatherm coated for safer, rapid heating. Instatherm is an integral noble metal alloy fused permanently to the glass and covered with a tough silicone rubber-treated glass cloth insulation which serves as a thermal barrier as well as protection against physical shock. Heat response is rapid and thermal lag low typical heating rates are approximately 5 per minute. Instatherm can be operated at 115v with ACE Proportional Temperature Controllers, such as: 12324, Flange at top is 60 (2.4 inch), 100 (4 inch), or 150 (6 inch) with shallow O Ring groove, for connection to 6527, 6528, 6529 or 6533 Head, with 6517 Quick Release Clamp. Bottom has a #50 or #80 Ace-Thred (internal glass thread) for installing or Bottom Adapter with filter support and drain valve. For Head, Bottom Adapter, and other accessory items, order separately. Supplied with cord Flange I.D., (in.) Bottom Thread Size Body I.D., Approx. Depth, Replacement CAPFE O Ring Volts Amps Watts Cap., ml Order Code (2.4") # (2.4") # (4") # (4") # (6") # (6") # Filter Reactor Unjacketed, Body only Reactor body, only, with Schott-style flange with O Ring groove at top and ACE #50 or #80 internal thread at bottom. Pressure rating is 35 psi. Supplied with CAPFE O Ring. Flange I.D., (in.) Bottom Thread Size Body I.D., Approx. Depth*, Repl. CAPFE O Ring Cap., ml Order Code (2.4) # (2.4) # (4) # (4) # (6) # (6) #

10 Filter Reactor Accessories 5838-80 5844-120 5839-42 5839-47, -55 Reactor Bottom Combinations 5857-85 12770-54 5857-68 12770-59 5839-55 5857-85 5844-120 5838-80 5839-42 12770-54 6386 5839-42 12770

Inlet/outlet of jacket are 28/15 O Ring ball joints, sealed tangentially, for more efficient circulation. Pressure rating is 35 psi. Supplied with CAPFE O Ring. Flange I.D., (in.

10 10 Filter Reactor Accessories , -55 Reactor Bottom Combinations Filter Reactor Jacketed, Body only Reactor body, only, with Schott-style flange with O Ring groove at top and ACE #50 or #80 internal thread at bottom. Body is jacketed for heating/cooling. Inlet/outlet of jacket are 28/15 O Ring ball joints, sealed tangentially, for more efficient circulation. Pressure rating is 35 psi. Supplied with CAPFE O Ring. Flange I.D., (in.) Bottom Thread Size Body I.D., Approx. Depth*, Repl. CAPFE O Ring Cap., ml Order Code (2.4) # (2.4) # (4) # (4) # (6) # (6) # Valve Bottom Shut Off PTFE valve for bottom of 5838 or 5857 Bottom Adapter to control flow from Reactor.Code -42 has an MPT thread at one end for attaching to 5844 Adapter, other end is a ¼ inch O.D. tubing compression fitting; codes -47 and -55 have FPT threads on both ends, for connecting to 5844 Adapter using Nipple. Must use Adapter ( 3 8 inch mpt ¼ inch fpt) when connecting ; ( 3 8 inch mpt 3 8 inch mpt) when connecting For Bottom Adapter Size NPT Size 50 1/4" MPT 1/4" Tube /8" FPT 3/8" FPT /2" FPT 1/2" FPT Barb (for use with ) 3/8" MPT 3/8" I.D. Tube Adapter PTFE PTFE Adapter used to connect or -55 Valve to 5838 or 5857 Bottom Adapter. NPT Size NPT Size 3/8" MPT 3/8" MPT /2" MPT 1/2" MPT Adapter PTFE Used to connect 5839 Valve to 5838 or 5857 Bottom Adapter NPT Size NPT Size 3/8" MPT 1/4" FPT /2" MPT 1/2" FPT Perforated Glass Plate For #80 Thread Size Adapter (only)

11 Filter Reactor Accessories /5857 Adapter Bottom, only Bottom adapter for use with 6384, 8386 or 6388 Reactor Bodies. Fabricated from PTFE, #50 and #80 have a 3 8 inch fpt for connecting bottom valve. Both have a CAPFE O Ring to seal adapter in Ace-Thred. #50 size supplied with 100 micron PE support disc (see 5848, above, for replacement or glass substitute). Can also be replaced with screen support using retainer ring. #80 size supplied with dual filter supports; a 100 micron PE filter (see 5848, above) and/ or perforated support plate with retainer ring for use with 350 micron PP screen (for other screen sizes, see 5814). For Thread Size Bottom Opening 50 3/8" fpt /8" fpt (Optional) 80 1/2" fpt CAPFE O Ring, repl. for #50, Pkg./ CAPFE O Ring, repl. for #80, Pkg./ Retainer Ring For Size #50 & #80 Adapters Adapter Size # # Screen Support Polypropylene For use with 5838 or 5857 Bottom Adapters. It is necessary to use a retainer ring to hold support in adapter. Thread Size Micron Pkg. Quantity Bench Reactor Stand New stand assembly for bench reactors from 1L to 6L sizes. Fits both pressure and filter versions as well as a standard round bottom flasks. It will accept flasks with or without a bottom valve. Motor mount raises and lowers, as does vessel clamping system which aids in easy alignment of overhead stir motors. Motor mount accepts popular models of stir motors. Base also raises and lowers to accoodate bottom valves or large size flasks. Flask are supported bottom and top, with quick clamp for easy access to remove heads for cleaning. All primary stand components are either powder-coated or anodized aluminum. The flasks sit on a rubber base plate attached to the stand base , -89 (Size 80) New (Size 50) 12840

12 Benchtop Reactors All-in-One Benchtop Reactor 1 or 2 liter Cylindrical Large 4" diameter flange on flask and head with CAPFE (PTFE encapsulated silicone rubber) O Ring and Quick Release clamp

12 12 Benchtop Reactors All-in-One Benchtop Reactor 1 or 2 liter Cylindrical Large 4" diameter flange on flask and head with CAPFE (PTFE encapsulated silicone rubber) O Ring and Quick Release clamp facilitate assembly/disassembly and removal of contents. All glass and PTFE wetted components. PTFE joint sleeves and valves and FETFE O Rings for high-purity, grease-free system with high chemical resistance. Suitable for high-vacuum situations. Overhead mechanical stirring with 10 diameter glass stirring shaft, PTFE multi-paddle agitator, flexible shaft and variable speed motor with controller. 1 LITER FLASK, 1-liter, Cylindrical, 4" (100) Grooved Flange with CAPFE O Ring HEAD, 4" (100) 24/40 Center Neck, (3) 24/40 Side Necks CLAMP, Quick Release, 4" CONDENSER, 24/40, 300 Jacket Length with Ace-Safe Connectors FUNNEL, Addition, 125mL, Pressure Equalizing, 24/40 Joints STIRRING SHAFT, 10, Polished with Ring, 44cm AGITATOR, PTFE, 4-Blade Multipaddle, 64 dia BEARING, 10, PTFE, 24/40, Complete CHUCK, Flex-Grip, for 10 Rod, 5/16" Motor Shaft STIRRING MOTOR & CONTROLLER, Reversible, Variable Speed, Complete FLEXIBLE SHAFT, 91.4cm (36") HEATING MANTLE, Aluminum Housed, 335 watts, 115v TEMPERATURE CONTROLLER, Digital, Type J, 120 volts THERMOPROBE, Type J, 1/4" O.D. x 12" long, PTFE covered THERMOPROBE, Lead Only, Detachable, Type J ADAPTER, Offset, 24/40 #7, Complete ADAPTER, 24/40, 2 Bore PTFE Stopcock ADAPTER, Offset, 24/40 24/ STOPPER, Glass 24/40 (3) SLEEVES, PTFE 24/40, Pkg/3 (2) JOINT CLIPS, Plastic 24/40, Pkg/ SUPPORT STAND, 29" High x 5/8" Diameter Rod, U Base CLAMP, Three-jaw, Medium CLAMP HOLDER, Regular (4) COMPLETE LITER A complete, general purpose benchtop cylindrical reactor. Self-supported and portable, with a small footprint. Electric heating mantle with digital temperature controller and Type J PTFE-covered thermoprobe for operation from room temperature to 200 C 125mL pressure equalizing addition funnel Reflux condenser Support stand, clamps, clamp holders and joint clips Note! This reactor is available with bottom outlet on flask; phone, fax or for price. FLASK, 2-liter, Cylindrical, 4" (100) Grooved Flange with CAPFE O Ring HEAD, 4" (100) 24/40 Center Neck, (3) 24/40 Side Necks CLAMP, Quick Release, 4" CONDENSER, 24/40, 300 Jacket Length with Ace-Safe Connectors FUNNEL, Addition, 125mL, Pressure Equalizing, 24/40 Joints STIRRING SHAFT, 10, Polished with Ring, 58 cm AGITATOR, PTFE, 4-Blade Multipaddle, 64 dia BEARING, 10, PTFE, 24/40, Complete CHUCK, Flex-Grip, for 10 Rod, 5/16" Motor Shaft STIRRING MOTOR & CONTROLLER, Reversible, Variable Speed, Complete FLEXIBLE SHAFT, 91.4cm (36") HEATING MANTLE, Aluminum Housed, 450 watts, 115v TEMPERATURE CONTROLLER, Digital, Type J, 120 volts THERMOPROBE, Type J, 1/4" O.D. x 12" long, PTFE covered THERMOPROBE, Lead Only, Detachable, Type J ADAPTER, Offset, 24/40 #7, Complete ADAPTER, 24/40, 2 Bore PTFE Stopcock ADAPTER, Offset, 24/40 24/ STOPPER, Glass 24/40 (3) SLEEVES, PTFE 24/40, Pkg/3 (2) JOINT CLIPS, Plastic 24/40, Pkg/ SUPPORT STAND, 36" High x 5/8" Diameter Rod, U Base CLAMP, Three-jaw, Medium CLAMP HOLDER, Regular (4) COMPLETE

Pressure Reactors 13 The following ACE heavy wall borosilicate glass Pressure Reactors have been designed and tested to provide the chemist with a system to perform low to moderate positive pressure

Two types of Pressure Reactors are available: 1 Two-Piece System, with a maximum pressure limit of 35 psig @ 100 C.

13 Pressure Reactors 13 The following ACE heavy wall borosilicate glass Pressure Reactors have been designed and tested to provide the chemist with a system to perform low to moderate positive pressure reactions, synthesis, and catalysis, or simply to run reactions under inert gas conditions. Reactor capacities range from 500mL to 5000mL, and use Ace-Threds to achieve a leak-tight system. Two types of Pressure Reactors are available: 1 Two-Piece System, with a maximum pressure limit of C. 2 One-Piece System, with a maximum pressure limit of C The Two-Piece System consists of a flanged flask and head with a shallow O Ring groove, O Ring and Quick Release Clamp. Flange sizes range from 60 to 150 inside diameter, allowing the use of large agitators and facilitating product removal and clean-out. The One-Piece System provides a 25 center opening, with smaller openings as side necks, and has a higher allowable operating pressure. Both systems offer vessels with or without bottom outlet valves and with or without heating/cooling jackets. These jackets are heat sealed. Complete systems and their components are listed on the following pages. Systems are available with: Mechanical Stirring, using stirring shaft with agitator, and a unique bearing designed with internal O Ring seals. Due to varying conditions, ACE cannot guarantee glassware against breakage caused by pressure or vacuum. Typical Assembly Safety is the foremost concern when operating pressurized glass reactors. With this in mind, ACE offers a separate manifold, 6448, which MUST be used in conjunction with all pressure systems listed in this catalog. It consists of a glass manifold with Ace- Threds, PTFE Adapters, a Pressure Gauge, a Primary adjustable Pressure Release Valve, and a Secondary fixed Pressure Rupture Disc. In addition, approved safety shields, eye and body protection should be used to avoid personal injury. For all complete systems the following accessories have been included: Liquid Addition Funnel Stirring Motor, Controller and Flexible Shaft Heating Mantle and Temperature Control System Thermowell Temperature Controller with Thermocouple Pressure Relief Manifold IMPORTANT General Warnings for Pressurized Glassware Due to varying conditions, ACE cannot guarantee glass vessels from breakage under pressure. ALL LABORATORY SAFETY PROCEDURES SHOULD BE OBSERVED. ALWAYS WORK BEHIND A SHIELD. Do not use with materials which solidify on standing and create excessive stress on glass. Before applying pressure, examine glassware carefully for surface scratches which may weaken its strength. Questions regarding the safe operating conditions of a particular glass vessel under pressure may be directed to ACE GLASS INCORPORATED. Safety coatings: epoxy and plastic coating help prevent scratching and shattering and reduce spills; however, they do not prevent breakage

14 Pressure Reactors Complete ACE Two-Piece Unjacketed Pressure Reactors Bottom Outlet 8081

listing of parts in this assembly) 7299 12681 8124 8044 8075 6024 13530 12110 7506 6433 6517

14 14 Pressure Reactors Complete ACE Two-Piece Unjacketed Pressure Reactors Bottom Outlet Series TWO 5846 Pressure Reactor Manifold, Complete, 6448 (See page 34 for a complete listing of parts in this assembly) Does NOT include stand, base or clamps

15 Pressure Reactors Series TWO Complete System (contains all items listed below) mL, 60 Flange #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 500mL, 60 flange top with bottom outlet Head, 60, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 60, Quick Release Addition Funnel, 60mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 19 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Aluminum Heating Mantle Type J Thermocouple Sensor, PTFE-clad Digital Temperature Controller, J output Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL, 100 Flange #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 500mL, 100 flange top with bottom outlet Head, 100, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 100, Quick Release Addition Funnel, 60mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 19 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Aluminum Heating Mantle Type J Thermocouple Sensor, PTFE-clad Digital Temperature Controller, J output Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL, 100 Flange #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 1000mL, 100 flange top with bottom outlet Head, 100, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 100, Quick Release Addition Funnel, 125mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 19 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Aluminum Heating Mantle Type J Thermocouple Sensor, PTFE-clad Digital Temperature Controller, J output Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete Unjacketed Two-Piece Pressure Reactor Two-piece systems with a maximum pressure limit of ºC. Flask has Bottom Outlet Complete System (contains all items listed below) mL, 100 Flange #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 2000mL, 100 flange top with bottom outlet Head, 100, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 100, Quick Release Addition Funnel, 250mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 19 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Aluminum Heating Mantle Type J Thermocouple Sensor, PTFE-clad Digital Temperature Controller, J output Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL, 150 Flange #15 PTFE Plug ( Complete contains THREE) West Condenser w/ace-threds Flask, 3000mL, 150 flange top with bottom outlet Head, 150, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 150, Quick Release Addition Funnel, 250mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 24 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Aluminum Heating Mantle Type J Thermocouple Sensor, PTFE-clad Digital Temperature Controller, J output Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL, 150 Flange #15 PTFE Plug ( Complete contains THREE) West Condenser w/ace-threds Flask, 5000mL, 150 flange top with bottom outlet Head, 150, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 150, Quick Release Addition Funnel, 500mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 24 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Aluminum Heating Mantle Type J Thermocouple Sensor, PTFE-clad Digital Temperature Controller, J output Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width

16 Pressure Reactors Complete ACE Two-Piece Jacketed Pressure Reactors 6429 Series TWO 8081

this assembly) 7299 8124 12681 8075 8044 6024 13530 7506 6433 6471 6517 6429 13649 Does NOT

16 16 Pressure Reactors Complete ACE Two-Piece Jacketed Pressure Reactors 6429 Series TWO Pressure Reactor Manifold, Complete, 6448 (See page 34 for a complete listing of parts in this assembly) Does NOT include stand, base or clamps. Shown without clamps for better visibility

17 Pressure Reactors Series TWO Complete System (contains all items listed below) mL, 60 Flange #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 500mL, 60 flange top, bottom outlet Head, 60, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 60, Quick Release Addition Funnel, 60mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 19 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL, 100 Flange #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 500mL, 100 flange top, bottom outlet Head, 100, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 100, Quick Release Addition Funnel, 60mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 19 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL, 100 Flange #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 1000mL, 100 flange top, bottom outlet Head, 100, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 100, Quick Release Addition Funnel, 125mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 19 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete Jacketed Two-Piece Pressure Reactor Two-piece systems with a maximum pressure limit of ºC. Flask has Bottom Outlet Complete System (contains all items listed below) mL, 100 Flange #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 2000mL, 100 flange top, bottom outlet Head, 100, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 100, Quick Release Addition Funnel, 150mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 19 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL, 150 Flange #15 PTFE Plug ( Complete contains THREE) West Condenser w/ace-threds Flask, 3000mL, 150 flange top, bottom outlet Head, 150, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 150, Quick Release Addition Funnel, 150mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 24 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL, 150 Flange #15 PTFE Plug ( Complete contains THREE) West Condenser w/ace-threds Flask, 5000mL, 150 flange top, bottom outlet Head, 150, #15 center neck, three side necks Pressure Reactor Manifold, complete Thermowell Clamp, 150, Quick Release Addition Funnel, 500mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, 24 wide Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width

18 Pressure Reactors Complete ACE One-Piece Jacketed Pressure Reactors with Bottom Outlet 8081

listing of parts in this assembly) 12681 7299 8124 8075 8081 6024 7506 13530 6471 6439 13649 Does

18 18 Pressure Reactors Complete ACE One-Piece Jacketed Pressure Reactors with Bottom Outlet Series SIX 5846 Pressure Reactor Manifold, Complete, 6448 (See page 34 for a complete listing of parts in this assembly) Does NOT include stand, base or clamps. Shown without clamps for better visibility

19 Pressure Reactors Series SIX Complete System (contains all items listed below) mL #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 500mL with bottom outlet Pressure Reactor Manifold, complete Thermowell Addition Funnel, 60mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 1000mL with bottom outlet Pressure Reactor Manifold, complete Thermowell Addition Funnel, 125mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL #15 PTFE Plug ( Complete contains TWO) West Condenser w/ace-threds Flask, 2000mL with bottom outlet Pressure Reactor Manifold, complete Thermowell Addition Funnel, 150mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete Jacketed One-Piece Pressure Reactor One-piece systems with a maximum pressure limit of ºC. Flask has Bottom Outlet Complete System (contains all items listed below) mL #15 PTFE Plug ( Complete contains THREE) West Condenser w/ace-threds Flask, 3000mL with bottom outlet Pressure Reactor Manifold, complete Thermowell Addition Funnel, 150mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width Complete System (contains all items listed below) mL #15 PTFE Plug ( Complete contains THREE) West Condenser w/ace-threds Flask, 5000mL with bottom outlet Pressure Reactor Manifold, complete Thermowell Addition Funnel, 500mL #15 PTFE Bushing ( Complete contains TWO) Bearing, complete, with Ace-Threds Stir Shaft, Flexible Shaft, complete, 91.4cm Stirrer Blade, PTFE, Krytox High Vacuum Grease Flex-Grip Chuck Bushing, PTFE, #15 with O Ring Polypropylene Tubing, ¼" OD x 0.170" ID Stirrer Motor Controller, Solid State Stirrer Motor with Mounting Rod, Solid State PTFE Sealing Tape, ½" Width

20 Reactor Accessories Individual Items for ACE Two-Piece Reactors 6423 6423 Flask Pressure Reaction, Unjacketed Rugged, heavy wall unjacketed reaction flask, part of the TWO-PIECE Pressure Reactor,

For heating mantle, see 12058. Capacity, ml Flange Size, Depth, Top Repl. O Ring 500 60 210 7855-878 6423-05 500 100 (4 in.

20 20 Reactor Accessories Individual Items for ACE Two-Piece Reactors Flask Pressure Reaction, Unjacketed Rugged, heavy wall unjacketed reaction flask, part of the TWO-PIECE Pressure Reactor, for use at elevated pressures. Schott-type flange supplied with O Ring groove for use with mating grooved head, Catalog No Supplied with CAPFE O Ring (silicone optional). For heating mantle, see Capacity, ml Flange Size, Depth, Top Repl. O Ring (4 in.) (6 in.) Flask Pressure Reaction, Unjacketed, with Bottom Outlet Rugged, heavy wall reaction flask with threaded bottom outlet, part of the TWO-PIECE Pressure Reactor, for use at elevated pressures. Schott-type flange supplied with O Ring groove for use with mating grooved head, Catalog No Supplied with CAPFE O Ring (silicone optional). For heating mantle, see Bottom outlet tube has 28/15 O Ring ball joint connection. Capacity, ml Flange Size, Depth, Bottom Outlet Top Repl. O Ring (4 in.) (6 in.) Flask Pressure Reaction, Jacketed Rugged, heavy wall reaction flask with jacket, part of the TWO-PIECE Pressure Reactor, for use at elevated pressures. Schott-type flange supplied with O Ring groove for use with mating grooved head, Catalog No Supplied with CAPFE O Ring (silicone optional). Cooling/ heating jacket is heat sealed. Inlet/outlet on jacket has easy connect/disconnect size 28/15 O Ring ball joints. Capacity, ml Flange Size, Depth, Top Repl. O Ring (4 in.) (6 in.)

Reactor Accessories 21 Individual Items for ACE Two-Piece Reactors 6518 Flask Reaction, Cylindrical, with ZDS Valve Cylindrical, heavy wall flask with round bottom.

Nominal Capacity, L Bottom Valve Size Flange I.D. I.D., (in.

Bottom Outlet Rugged, heavy-wall reaction flask with jacket and threaded bottom outlet, part of the TWO- PIECE Pressure Reactor, for use at elevated pressures.

Inlet/outlet on jacket and bottom valve have size 28/15 O Ring ball joint connections. Capacity, ml Flange Size, Depth, Bottom Outlet Top Repl. O Ring 500 60 210 0-8 7855-878 6429-09 500 100 (4 in.

21 Reactor Accessories 21 Individual Items for ACE Two-Piece Reactors 6518 Flask Reaction, Cylindrical, with ZDS Valve Cylindrical, heavy wall flask with round bottom. Flask has extra thick flange with O Ring groove. Flask uses 6517 Quick Clamps and heads found in the Ace General Catalog. Comes with one CAPFE O Ring. Bottom outlet is new ZDS (Zero Dead Space) valve. Nominal Capacity, L Bottom Valve Size Flange I.D. I.D., (in.) (4) (4) (6) (4) (6) (6) New Flask Pressure Reaction, Jacketed, with Bottom Outlet Rugged, heavy-wall reaction flask with jacket and threaded bottom outlet, part of the TWO- PIECE Pressure Reactor, for use at elevated pressures. Schott-type flange supplied with a shallow O Ring groove for use with mating head, Catalog No Supplied with CAPFE O Ring (silicone optional). Cooling/heating jacket is heat sealed. Inlet/outlet on jacket and bottom valve have size 28/15 O Ring ball joint connections. Capacity, ml Flange Size, Depth, Bottom Outlet Top Repl. O Ring (4 in.) (6 in.) Flask Pressure Reaction, Unjacketed Rugged, heavy wall unjacketed reaction flask, part of the ONE-PIECE Pressure Reactor, for use at elevated pressures 2. With Ace-Thred Necks for positive connection of stirrer, funnel, thermowell, condenser, etc. Capacity, ml O.D., Depth, Center Neck Side Necks #25 (1) #7; (3) # #25 (1) #7; (3) # #25 (1) #7; (3) # #25 (1) #7; (4) # #25 (1) #7; (4) # One-Piece System, with a maximum pressure limit of C.

22 Reactor Accessories Individual Items for ACE One-Piece Reactors 6437 6437 Flask Pressure Reaction, with Bottom Outlet Rugged, heavy wall reaction flask with threaded bottom outlet, part of the

Bottom outlet is a 28/15 O Ring ball joint and a threaded valve for retrieving contents of flask. Capacity, ml O.D.

6437-20 5000 165 0-10 #25 (1) #7; (4) #15 6437-24 6438 6438 Flask Pressure Reaction, Jacketed Rugged, heavy wall reaction flask with jacket, part of the Cooling/heating jacket is heat sealed.

22 22 Reactor Accessories Individual Items for ACE One-Piece Reactors Flask Pressure Reaction, with Bottom Outlet Rugged, heavy wall reaction flask with threaded bottom outlet, part of the ONE-PIECE Pressure Reactor, for use at elevated pressures 2. With Ace-Thred Necks for positive connection of stirrer, funnel, thermowell, condenser, etc. Bottom outlet is a 28/15 O Ring ball joint and a threaded valve for retrieving contents of flask. Capacity, ml O.D., Bottom Outlet Center Neck Side Necks #25 (1) #7; (3) # #25 (1) #7; (3) # #25 (1) #7; (3) # #25 (1) #7; (4) # #25 (1) #7; (4) # Flask Pressure Reaction, Jacketed Rugged, heavy wall reaction flask with jacket, part of the ONE-PIECE Pressure Reactor, for use at elevated pressures 2. With Ace-Thred Necks for positive connection of stirrer, funnel, thermowell, condenser, etc. Cooling/heating jacket is heat sealed. Inlet/outlet on jacket has easy connect/disconnect size 28/15 O Ring ball joints. Capacity, ml O.D., Center Neck Side Necks Inlet/Outlet Thread to ID Tube (in.) #25 (1) #7; (3) #15 #11-3/ #25 (1) #7; (3) #15 #15-3/ #25 (1) #7; (3) #15 #15-3/ #25 (1) #7; (4) #15 #15-1/ #25 (1) #7; (4) #15 #15-1/ Flask Pressure Reaction, Jacketed, with Bottom Outlet Rugged, heavy wall reaction flask with jacket, part of the ONE-PIECE ressure Reactor, for use at elevated pressures 2. With Ace-Thred Necks for positive connection of stirrer, funnel, thermowell, condenser, etc. Cooling/heating jacket is heat sealed. Inlet/outlet on jacket has easy connect/disconnect size 28/15 O Ring ball joints. Bottom outlet is a 28/15 O Ring ball joint and a threaded valve for retrieving contents of flask. Cap., ml O.D., Center Neck Side Necks Bottom Outlet Inlet/Outlet Thread to ID Tube (in.) #25 (1) #7; (3) # #11-3/ #25 (1) #7; (3) # #11-3/ #25 (1) #7; (3) # #11-3/ #25 (1) #7; (4) # #15-1/ #25 (1) #7; (4) # #15-1/ One-Piece System, with a maximum pressure limit of C.

Reactor Accessories 23 Individual Items for ACE One- and Two-Piece Reactors 7701 Moisture Test Receiver Pressure Used to determine heavier-than-water co-distilling solvent component content of

The 6024-20 Pressure Condenser, above, with #15 Plug, is attached to #15 thread at top of receiver with bushing and O Ring. Receiver capacity is 60mL, graduated in 1mL subdivisions.

23 Reactor Accessories 23 Individual Items for ACE One- and Two-Piece Reactors 7701 Moisture Test Receiver Pressure Used to determine heavier-than-water co-distilling solvent component content of reaction mixture. For use with ACE Pressure Reactors with #15 Ace-Thred. Side arm is connected to #15 Ace-Thred on Pressure Reactor Head with 7506 Bushing and O Ring. The Pressure Condenser, above, with #15 Plug, is attached to #15 thread at top of receiver with bushing and O Ring. Receiver capacity is 60mL, graduated in 1mL subdivisions. Bottom outlet stopcock is a 0-3 with FETFE O Rings. Pressure rating, 45 C. Complete consists of Receiver and Bushing with O Ring. Condenser and #15 Plug NOT supplied order separately. Receiver, only, 60 ml, # Bushing, Nylon, #15, w/fetfe O Ring (2) Complete Moisture Test Trap Pressure Adapter and receiver used to determine heavier-than-water co-distilling solvent component content of reaction mixture. For use with ACE Pressure Reactors with #15 Ace-Thred. Adapter side arm is connected to #15 Ace-Thred on Pressure Reactor Head with 7506 Bushing and O Ring. The Pressure Condenser, above, with #15 Plug, is attached to #15 thread at top of adapter with bushing and O Ring , 48mL Pressure Tube (not graduated) with #15 Ace-Thred is attached to bottom of adapter via #15 Bushing and O Ring. Rated to 45 C. Complete item includes Adapter, Pressure Tube/Receiver and Bushing with FETFE O Ring. Condenser and #15 Plug NOT supplied, order separately. Adapter, Moisture Trap, only, # Pressure Tube/Receiver, only, 48 ml, # Bushing, Nylon, #15, w/fetfe O Ring (3) Complete Optional: Pressure Tube/Receiver, only, 15 ml, # Pressure Tube/Receiver, only, 100 ml, #

24 Reactor Accessories 6452 Sparger Easy Action Stopcock and Hose Connection Sparger tube with Ace Frit at one end and an Easy Action

, Order Code 400 A (145-174 micron) 0-3 5/16 (C) 10 6452-03 400 B (70-100 micron) 0-3 5/16 (C) 10 6452-05 400 C (25-50 micron) 0-3 5/16

Stopcock with #7 Ace-Thred connection at opposite end for 7 O.D. tube connection. Supplied with 5029-10 Nylon Bushing and FETFE O Ring.

24 24 Reactor Accessories 6452 Sparger Easy Action Stopcock and Hose Connection Sparger tube with Ace Frit at one end and an Easy Action Stopcock with 90 degree hose connection at opposite end. Overall Length, Porosity Stopcock Size Tubing Size (in.) Tube O.D., Order Code 400 A ( micron) 0-3 5/16 (C) B ( micron) 0-3 5/16 (C) C (25-50 micron) 0-3 5/16 (C) Sparger Easy Action Stopcock and #7 Ace-Thred Sparger tube with Ace Frit at one end and an Easy Action Stopcock with #7 Ace-Thred connection at opposite end for 7 O.D. tube connection. Supplied with Nylon Bushing and FETFE O Ring. Overall Length, Porosity Stopcock Size Tube O.D., 400 A ( micron) B ( micron) C (25-50 micron)

Reactor Accessories 25 12177 Baffle Glass Borosilicate glass Baffle fits through standard taper joint of Reaction Flasks to increase agitation and promote mixing.

Shaft of Baffle is sized to be secured using 5030 Ace-Thred Adapter with Nylon bushing and FETFE O Ring.

Order Baffle, Adapter and optional ferrule separately. Baffle codes -10 and -13 fit through 24/40 joint and larger; codes -19 and -23 fit through 45/50 and larger. Custom sizes can be made to order.

25 Reactor Accessories Baffle Glass Borosilicate glass Baffle fits through standard taper joint of Reaction Flasks to increase agitation and promote mixing. Takes the place of indented or Morton vessels that can be a problem when using pressure or vacuum. Shaft of Baffle is sized to be secured using 5030 Ace-Thred Adapter with Nylon bushing and FETFE O Ring. This connection allows vertical and rotational adjustment of the Baffle inside the flask for optimum effect. In place of O Ring, a PTFE ferrule can be used for maximum chemical resistance. Order Baffle, Adapter and optional ferrule separately. Baffle codes -10 and -13 fit through 24/40 joint and larger; codes -19 and -23 fit through 45/50 and larger. Custom sizes can be made to order. Shaft Diameter, Shaft Length, Fits Ace-Thred Size Baffle W x L x D, Overall Length, Order Code #11 18 x 60 x #11 18 x 90 x #15 36 x 65 x Baffle PTFE Fabricated from virgin PTFE (meets USP Class 6 requirements), this fully encapsulated, seamless Baffle with a Stainless Steel reinforcing core fits through standard taper joint of Reaction Flasks to increase agitation and promote mixing. Takes the place of indented or Morton vessels that can be a problem when using pressure or vacuum. Shaft of Baffle is sized to be secured using 5028/5030 Ace-Thred Adapter with Nylon bushing and FETFE O Ring. This connection allows vertical and rotational adjustment of the Baffle inside the flask for optimum effect. In place of O Ring, a PTFE ferrule can be used for maximum chemical resistance. Order Baffle, Adapter and optional ferrule separately. Baffle codes -145 and -148 fit through 24/40 joint and larger; codes -152, -154 and -157 fit through 45/50 and larger. Shaft Diameter, Shaft Length, Fits Ace-Thred Size Baffle W x L x D, Overall Length, Order Code #7 18 x 152 x #11 18 x 150 x #15 30 x 150 x #15 30 x 250 x Reaction Flask Jacketed Cylindrical flask with neck opening of 4 inches (102). Inlet and outlet connections are size 28/15 O Ring ball joints, both sealed tangentially, one at top and one at bottom of jacketed section. Capacity, ml Approx. Depth, cm Reaction Flask Rugged cylindrical flask with neck opening of 4 inches. Uses 6496 Clamp for securing flask head to flask. Capacity, ml Approx. Depth, cm

26 Reactor Accessories 6477 6477 Reaction Flask with Indents Same as 6476, except with side indents for improved stirring characteristics. Not suitable for vacuum operation.

3 6477-25 6479 6479 Reaction Flask Rugged spherical flask with neck opening of 4 inches (102). Standard size flasks use regular Glas-Col heating mantles of equivalent capacity.

Capacity, ml 3000 6479-05 5000 6479-10 6480 6480 Reaction Flask Jacketed Spherical flask with neck opening of 4 inches.

, ml 3000 6480-05 5000 6480-10 6511 6511 Flask Reaction, with O Ring Groove Cylindrical heavy-wall reaction flask, with flat bottom rounded inside wall, and extra-thick flat flange, similar to

26 26 Reactor Accessories Reaction Flask with Indents Same as 6476, except with side indents for improved stirring characteristics. Not suitable for vacuum operation. Uses 6496 Clamp for securing flask head to flask. Capacity, ml Approx. Depth, cm Reaction Flask Rugged spherical flask with neck opening of 4 inches (102). Standard size flasks use regular Glas-Col heating mantles of equivalent capacity. Length of straight section including flange, approximately 9.5cm (3¾-inches). Uses 6496 Clamp for securing flask head to flask. Capacity, ml Reaction Flask Jacketed Spherical flask with neck opening of 4 inches. Inlet and outlet connections are size 28/15 O Ring ball joints, both sealed tangentially, on jacketed section. Uses 6496 Clamp for securing flask head to flask. Cap., ml Flask Reaction, with O Ring Groove Cylindrical heavy-wall reaction flask, with flat bottom rounded inside wall, and extra-thick flat flange, similar to , previous page, except flange has an O Ring groove for use with CAPFE (PTFE encapsulated silicone rubber) O Ring instead of gasket. Without constriction at top to facilitate introduction/removal of material and allow for ease of cleaning. For reaction heads, see 6512, 6513 and Flask is supplied with one CAPFE O Ring. For clamp, see 6508 or Capacity, ml O.D. of Bottom, Height, Repl. O Ring

Reactor Accessories 27 9656 Reaction Flask Instatherm Heated Same flask as listed under 6476, except with Instatherm.

The response is rapid and accurate attention can be directed toward contents instead of the pot. Supplied with 9698-20 cord for connection to variable voltage or termperature controller.

For controllers, see 12080-10 Autotransformer or ACE Proportional Temperature Controllers with voltage limiting output 12125, 12324. Use 6496 Clamp for securing head to flask. Capacity, ml Max.

27 Reactor Accessories Reaction Flask Instatherm Heated Same flask as listed under 6476, except with Instatherm. This integral heating element eliminates the local super-heating coonly associated with more conventional heating methods. Eliminates cumbersome and dangerous oil baths. The response is rapid and accurate attention can be directed toward contents instead of the pot. Supplied with cord for connection to variable voltage or termperature controller. Flask is coated to within 38 of the flange for 200ºC operation, 360 C max. on special order. Interchangeable with all ACE reaction tops. For controllers, see Autotransformer or ACE Proportional Temperature Controllers with voltage limiting output 12125, Use 6496 Clamp for securing head to flask. Capacity, ml Max. Voltage Watts Flask Reaction, Cylindrical, Plain Rugged cylindrical reaction flask with Schott flat flange with O Ring groove, for use with 6517 Quick Release Clamp. 10 liter and larger are supplied with capacity reference graduations. Each flask is supplied with one CAPFE O Ring (PTFE encapsulated silicone O Ring). Plain silicone O Rings are also available. For reaction heads, see 6528 or For cooling/heating coils, see Capacity, Liters Full Capacity, Liters Approx. Depth, Nominal Flange I.D., (in.) Repl. CAPFE O Ring Use Clamp (4) (4) (4) (8) /6472 Flask Reaction, Cylindrical, with Bottom Outlet Similar to 6521 but with an Easy Action Plug bottom outlet with Chemraz O Rings for draining contents. Bottom outlet has 28/15 O Ring ball joint. Ten liter and larger are supplied with capacity reference graduations. Each flask is supplied with one CAPFE O Ring (PTFE encapsulated silicone O Ring). Plain silicone O Rings are also available. Cap., Liters Full Cap., Liters Approx. Depth, Nominal Flange I.D. Repl. CAPFE O Ring Use Clamp Outlet Size, (4") (4") (4") (8")

28 Reactor Accessories 6523 Flask Reaction, Cylindrical, Jacketed Rugged cylindrical reaction flask with Schott flat flange and O Ring groove, for use with 6517 Quick Release Clamp.

Flask supplied with 5853 Connectors. Each flask is supplied with one CAPFE O Ring (PTFE encapsulated silicone O Ring) for flange. Plain silicone O Rings are also available.

CAPFE O Ring Use Clamp 1 1.5 180 100 (4") 6517-25 7855-880 6523-12 2 2.2 260 100 (4") 6517-25 7855-880 6523-14 3 2.

Schott flat flange with O Ring groove, for use with 6517 Quick Release Clamp but with indents for greater agitation.

For cooling/heating coils, see 12067. NOT suitable for vacuum or pressure operation. Capacity, Liters Full Capacity, Liters Nominal Flange I.D. Approx. Depth, Use Clamp Repl.

2 260 100 (4") 6517-25 7855-880 6526-12 6537 6537 Flask Reaction, Spherical, Indented Style Rugged spherical reaction flask with Each flask is supplied with one CAPFE O Ring (PTFE

NOT suitable for vacuum or pressure operation. Capacity, Liters Full Capacity, Liters Approx. Diameter, Nominal Flange I.D. Use Clamp Repl. O Ring 3 3.

28 28 Reactor Accessories 6523 Flask Reaction, Cylindrical, Jacketed Rugged cylindrical reaction flask with Schott flat flange and O Ring groove, for use with 6517 Quick Release Clamp. Inlet and outlet connec tions on jacket, sealed tangentially, are O Ring ball joints. Ten liter and larger are supplied with capacity reference graduations. Flask supplied with 5853 Connectors. Each flask is supplied with one CAPFE O Ring (PTFE encapsulated silicone O Ring) for flange. Plain silicone O Rings are also available. For reaction heads, see 6528 or For cooling/heating coils, see Capacity, Liters Full Capacity, Liters Approx. Depth, Nominal Flange I.D. Repl. CAPFE O Ring Use Clamp (4") (4") (4") (8") Flask Reaction, Cylindrical, Indented Style Rugged cylindrical reaction flask with Schott flat flange with O Ring groove, for use with 6517 Quick Release Clamp but with indents for greater agitation. Each flask is supplied with one CAPFE O Ring (PTFE encapsulated silicone O Ring). Plain silicone O Rings are also available. For reaction heads, see For cooling/heating coils, see NOT suitable for vacuum or pressure operation. Capacity, Liters Full Capacity, Liters Nominal Flange I.D. Approx. Depth, Use Clamp Repl. O Ring (4") (4") Flask Reaction, Spherical, Indented Style Rugged spherical reaction flask with Schott flat flange with O Ring groove, for use with 6517 Quick Release Clamp but with indents for greater agitation. Each flask is supplied with one CAPFE O Ring (PTFE encapsulated silicone O Ring). Plain silicone O Rings are also available. For reaction heads, see 6528 or For cooling/heating coils, see NOT suitable for vacuum or pressure operation. Capacity, Liters Full Capacity, Liters Approx. Diameter, Nominal Flange I.D. Use Clamp Repl. O Ring (4") (4") (6") Mantle Cylindrical type for use with 6476, 6477, and 6497 Reaction Flasks. Upper temperature limit, 450ºC. For Flask Cap., ml I.D. x Depth, inches Wattage x 2½ 250w-115v x w-115v x w-115v x w-115v x w-115v

Reactor Accessories 29 6478 Mantle Aluminum Housed Cylindrical type for use with 6476, 6477, and 6497 Reaction Flasks. With aluminum housing.

x Depth, inches Wattage 500 4 5 8 x 2½ 250w-115v 6478-45 1000 4 5 8 x 5 5 8 300w-115v 6478-47 1500 4 5 8 x 6 5 8 380w-115v 6478-49 2000 4 5 8 x 8 7 8 450w-115v

3L 6521 reaction flasks. For Flask Cap., ml I.D. cm Depth, cm Wattage 1000 4.5" 4.5" 270 12075-08 2000 4.5" 7.5" 400 12075-10 3000 4.

Upper temperature limit, 450ºC. Note: Corning and/or Schott 50 liter flasks take different mantles. For Flask Cap.

29 Reactor Accessories Mantle Aluminum Housed Cylindrical type for use with 6476, 6477, and 6497 Reaction Flasks. With aluminum housing. Upper temperature limit, 450ºC. For Flask Cap., ml I.D. x Depth, inches Wattage x 2½ 250w-115v x w-115v x w-115v x w-115v x w-115v Mantle Cylindrical, Aluminum Housed Series TM cylindrical resin kettle mantle specifically for 1, 2 and 3L 6521 reaction flasks. For Flask Cap., ml I.D. cm Depth, cm Wattage " 4.5" " 7.5" " 11" Mantle With metal housing, consisting of an aluminum shell protecting the outside of the heating mantle. Upper temperature limit, 450ºC. Note: Corning and/or Schott 50 liter flasks take different mantles. For Flask Cap., ml Wattage w-115v w-115v Mantles For use with 6504 or 6511 Reaction Flasks. Upper temperature limit, 450 C. For Flask Cap., ml I.D. x Depth, cm Wattage x w-115v x w-115v x w-115v x w-115v x w-115v

30 Reactor Accessories 12058 12058 Mantles Aluminum Housing For Reaction Flasks, 6504 or 6511. Similar to 12036, but provided with aluminum housing. For Flask Cap.

protrude below heater. Upper temperature limit, 450ºC. For Flask Cap., ml I.D.

6494-25 6495 Gasket PTFE A.8 thick gasket intended primarily to be used with ACE Reaction Flasks with neck opening of 4 inches.

Slight clamp pressure makes completely effective seal, reduces breakage to a minimum. Wall thickness is.020 inches; overall thickness of.030 inches.

30 30 Reactor Accessories Mantles Aluminum Housing For Reaction Flasks, 6504 or Similar to 12036, but provided with aluminum housing. For Flask Cap., ml I.D. x Depth, cm Wattage x w-115v x w-115v x w-115v x w-115v x w-115v Flask Heater Specially designed with bottom opening and zipper for use with 6491, 6492, 6493 and 6522 Flasks to allow stopcock to protrude below heater. Upper temperature limit, 450ºC. For Flask Cap., ml I.D. x Depth, inches Wattage x w-115v x w-115v x w-115v x w-115v Gasket PTFE A.8 thick gasket intended primarily to be used with ACE Reaction Flasks with neck opening of 4 inches. Material PTFE Gasket PTFE, Grooved Precision machine grooved PTFE gasket for sealing two ground glass or metal surfaces. Slight clamp pressure makes completely effective seal, reduces breakage to a minimum. Wall thickness is.020 inches; overall thickness of.030 inches. Use with 6504 and 6511 Reactors. For Kettle Size Flange O.D., in Gasket FETFE A.020" thick FETFE (a fluoroelastomer with special TFE additives) gasket for sealing two ground glass or metal surfaces. Slight clamp pressure makes completely effective, leak-free seal and reduces breakage to a minimum. Use with 6504 and 6511 Reactors For Kettle Size Flange O.D., in

Reactor Accessories 31 6525 Gasket Crescent Ring PTFE crescent ring gaskets for use with 6525 Coupling. Consists of a ring with locating skirt. Temperature limit, 200 C.

Consists of two halfrings, plastic (phenolic resin) for Codes -20, 25, 30; grey cast iron for codes -33, 38. Gaskets, 6525, are placed between the ground surfaces of the glass flanges.

31 Reactor Accessories Gasket Crescent Ring PTFE crescent ring gaskets for use with 6525 Coupling. Consists of a ring with locating skirt. Temperature limit, 200 C. For Flange Size, For Flange Size, Coupling Coupling for clamping Reaction Flask to Reaction Flask Head like Consists of two halfrings, plastic (phenolic resin) for Codes -20, 25, 30; grey cast iron for codes -33, 38. Gaskets, 6525, are placed between the ground surfaces of the glass flanges. Complete coupling consists of two half-rings and appropriate number of cadmium-plated steel bolts, with nuts and washers. For gaskets, see , 46, 51, 53, 56 below. Preset T-Handle torque wrench, 30 in-lbs max., and ¼ inch socket available for safe tightening of coupling. For Flange Size, For Flange Size, Torque Wrench, only Socket, ¼", only Containment Tray Low Density Polyethylene, w/spigot Trays are made of rugged, molded Low Density Polyethylene (LDPE). Models listed below feature a wide lip at the top and a ½" spigot for easy draining of fluids. Size (L"xW"xH") For Vessel or Reactor Size 12 x 16 x 3 1 to 2L x 20 x 3 up to 6L

32 Reactor Accessories 8044 Bearing Pressure, with Ace-Threds, 10 Glass bearing with #15 Ace-Thred at each end and glass tubing between for use with 10 O.D. 8075 Stirring Shafts.

Top bushing also has an internal O Ring seal for additional seal on shaft to allow pressure reactions. Maximum operating speed 600 rpm. Coupling and Bushing supplied with O Rings.

32 32 Reactor Accessories 8044 Bearing Pressure, with Ace-Threds, 10 Glass bearing with #15 Ace-Thred at each end and glass tubing between for use with 10 O.D Stirring Shafts. PTFE coupling, with internal O Ring seal, connects bottom of bearing to either #15 or #25 Ace-Thred on vessels such as 6433 Pressure Reactor Head or one-piece Pressure Reactors. Top bushing also has an internal O Ring seal for additional seal on shaft to allow pressure reactions. Maximum operating speed 600 rpm. Coupling and Bushing supplied with O Rings. For replacement O Rings: for #15 #15 Coupling, external, internal; for #15 #25 Coupling, and external, internal; for #15 Bushing, external, internal. For Coupling to #15 Ace-Thred For Coupling to #25 Ace-Thred Glass Bearing, only, #15-# Glass Bearing, only, #15-# Coupling, PTFE, #15-# Coupling, PTFE, #15-# Bushing, PTFE, # Bushing, PTFE, # Complete Complete Filter Disc Support For use with 5838 or 5857 Bottom Adapters. Replaces screen support and retainer ring. Simply snap into bottom of adapter. Supplied in either polyethylene (PE) or borosilicate glass For Thread Size PE 100 micron Por. B ( micron) Borosilicate Por. C (25-50 micron) Por. D (10-20 micron) Pkg. Qty Adapter Bushing, Thermometer For thermometers having a 10/30 joint Inner Outer 10/30 14/ /30 24/ /30 29/ ADAPTER Thermometer, Mini #7 Ace-Thred With ground joint at bottom and threaded bushing at top which tightens into #7 Ace-Thred to form an O Ring compression seal with thermometers, bleed tubes, etc. Nylon bushing comes complete with FETFE O Ring. 10/18 size will accoodate thermometers up to 6.5 diameter, all others will accoodate 7 diameters. Suitable for vacuum work. Supplied complete with Nylon bushing. For extra O Rings, see Joint 10/ / / /

Reactor Accessories 33 5221 Adapter Connecting, Outer Socket Joint Outer Joint Connects to Size 10 tube 28/15 5221-05 #11 Ace-Thred 28/15

5221-28 5221-11 5221-09 12187 Clamp Hose Connection, Stainless Steel Ace Glass universal pilot plant / circulator adapters and fittings

12187 28/15 Glass Ball Joint to 28/15 Stainless Adapter 12187-28 35/25 Glass Ball Joint to 35/25 Stainless Adapter 12187-35 5268/9089 Adapter

5268-21 45/50 5268-58 35/25 5268-35 5268-54 9089-40 5268-10 9089-08 5268-35 5269 Adapter Offset, with Ace-Thred Offset adapter with #15

33 Reactor Accessories Adapter Connecting, Outer Socket Joint Outer Joint Connects to Size 10 tube 28/ #11 Ace-Thred 28/ #15 Ace-Thred 28/ ¾" tube 35/ #15 Ace-Thred 35/ #25 Ace-Thred 35/ Clamp Hose Connection, Stainless Steel Ace Glass universal pilot plant / circulator adapters and fittings designed for use with various manufacturer s circulators and our reaction systems /15 Glass Ball Joint to 28/15 Stainless Adapter /25 Glass Ball Joint to 35/25 Stainless Adapter /9089 Adapter Offset WITHOUT DRIP TIP WITH DRIP TIP Joints Joints 14/ / / / / / / / / Adapter Offset, with Ace-Thred Offset adapter with #15 Ace-Thred offset to a 14 OD tube with O Ring groove. For use with Ace Pressure Reactors to locate condenser, etc., away from stirrer. NOT supplied with bushing or O Ring. Order for Bushing and O Ring

34 34 Reactor Accessories A B Tube Fittings, Connectors PTFE tube fittings and connectors for use in making solenoid-to-vessel connections in the ACE Bioassay Diluter System or other tubing connections. All fittings have male NPT thread at one end and tube compression, barb or NPT thread at other. A C A B A B B Style Fits Tubes O.D., NPT Size (in.) Material A, Dimensions B, C, Elbow 6.4 (¼ in.) 1/4 PTFE Elbow 9.5 ( 3 8 in.) 1/4 PTFE Elbow 9.5 3/8 PTFE Elbow 12.7 (½ in.) 3/8 PTFE Elbow /2 PTFE Connector 6.4 1/4 PTFE Connector 9.5 1/4 PTFE Connector 6.4 3/8 PTFE Connector 9.5 3/8 PTFE Connector /8 PTFE Connector /2 PTFE Nipple 1/4 PTFE Nipple 3/8 PTFE Nipple 1/2 PTFE Barb 1/4 PTFE Barb 3/8 PTFE To #7 Ace-Thred and , Manifold Pressure, Epoxy Coated Complete Glass manifold, fitted with pressure gauge, primary adjusable pressure relief valve and secondary rupture low safer operation of Pressure Filter Reactors Pressure Gauge is a 0-60 psi stainless steel internal, with 1½ inch face and 1 8 inch npt male connection for use with Adapter in #15 Ace-Thred Pressure Relief Valve is adjustable from 3-50 psig by adjusting set screws to desired cracking pressure. Ends are ¼ inch npt for connecting to #15 Ace-Thred on Manifold with Adapter Rupture Disc is a secondary and last resort safety device that, in the event of an overpressure (one that cannot be handled by the 8767 Relief Valve) will rupture at a predetermined burst rating; 55 psig (±3 psig) for -12 version, 65 psig (±3 psig) for -41 version. Disc is manufactured from high-purity carbon with a PTFE coating on the underside. No springs or moving parts, disc is secured directly in #25 Ace-Thred of Manifold with Adapter. Manifold is connected to #7 Ace-Thred on 6433 Head using Adapter and Tubing Connectors with 1/4 inch tubing. Adapter, PTFE, #7 1/8" npt Adapter, PTFE, #15 1/8" npt Adapter, PTFE, #15 1/4" npt (3) Adapter, PTFE, #25 1/4" npt, w/o O Ring Rupture Disc, Graphite, 55 psig Rupture Disc, Graphite, 65 psig (for pressure version only) Manifold, Glass, (4) #15, (1) #25, Epoxy Coated Valve, Pressure Relief, 1/4" npt, 3 50 psig Coupling Body, 1/8" mpt Coupling Body, 1/4" mpt Coupling Insert, for 1/4" O.D. tubing (2) Tubing, PP, 1/4" O.D. x.170" I.D., 100' Gauge, Pressure, 0 60 psi, 1/8" mpt Complete (with Rupture Disc) Complete, Pressure Version (with Rupture Disc)

Reactor Accessories 35 6020/9270 Condenser Spiral With spiral condensing tube having both inlet and outlet connections at top, on same side.with inner and outer joints at bottom and top.

Coil Length, Joints Tubing Size 100 14/20 5/16" or 3/8" (B) 9270-04 200 24/40 3/8" (D) 6020-02 250 24/40 3/8" (D) 6020-04 300 24/40 3/8" (D) 6020-06 400 24/40 3/8" (D) 6020-08 6020 9270 6024/6029

6024-20 supplied with #15 Ace-Thred at top for 5846 Plug (not supplied) and drip stem with groove, and long enough to be secured in #15 Ace-Thred with 7506-06 Bushing and O Ring (not supplied) to

35 Reactor Accessories /9270 Condenser Spiral With spiral condensing tube having both inlet and outlet connections at top, on same side.with inner and outer joints at bottom and top. Length between joints is approximately longer than coil length. See page 5 for more detailed Hose Connection information. Coil Length, Joints Tubing Size /20 5/16" or 3/8" (B) /40 3/8" (D) /40 3/8" (D) /40 3/8" (D) /40 3/8" (D) /6029 Condenser West West style condenser for use with 6433 threaded or 6527, 6528 or 6529 jointed heads supplied with #15 Ace-Thred at top for 5846 Plug (not supplied) and drip stem with groove, and long enough to be secured in #15 Ace-Thred with Bushing and O Ring (not supplied) to restrict blowout. With #7 Ace-Thred on inlet/outlet for use with Ace-Safe 5853 Tubing connectors. Supplied with bushing and connectors for ¼ inch I.D. tubing supplied with 24/40 joint at top and bottom and D size (see page 5 for sizing) barbed hose connection on inlet/outlet for ¼ inch I.D. tubing Use with Head No. Jacket Length, ,6528, Funnel Powder Dispensing Side operated screw feed funnel for addition of powders and solids, up to 25 mesh, to reactions without problems of seizing or binding. Features a flexible PTFE screw thread wrapped on a precision PTFE-ceramic shaft and contained within a precision bore housing. This offers a unique flexibility in that the thread can move aside temporarily; as one spacing increases, the adjacent spacing decreases, thereby maintaining an average feed rate. Completely inert materials allow flushing with solvents without fear of contamination. #15 Ace-Thred offers easy disassembly for cleaning. Large 1¼ inch knob makes turning smooth and easy. Top outer and bottom inner joints are TS 24/40. TS 14/20 outer joint atop inner joint is for easier flushing. Capacity, ml

36 Reactor Accessories 7298 7298/7299 Funnel Addition, Pressure Equalizing Funnel for use with 6433 threaded or 6527, 6528 or 6529 jointed heads.

7299 (use with 6433 Head) supplied with #15 Ace-Thred at top for 5846 Plug (not supplied) and drip stem with groove and long enough to be secured in a #15 Ace-Thred with 7506-06 Bushing and O Ring

, ml Stopcock Orifice, For 7298 60 0-3 7299-06 0-3 8192-261 125 0-3 7298-05 7299-12 0-5 8192-263 250 0-3 7298-10 7299-25 500 0-3 7298-15 7299-34 For 7299 1000 0-5 7298-24 0-3 8189-43 7233 7233 Funnel

Features a flexible PTFE screw thread wrapped on a precision PTFE-ceramic shaft and contained within a precision bore housing.

Completely inert materials allow flushing with solvents without fear of contamination. #15 Ace-Thred at top offers easy disassembly for cleaning. Large 1¼ inch knob makes turning smooth and easy.

Capacity, ml 50 7233-20 100 7233-30 9485 Funnel Powder Dispensing A vertical, compact, screw feed funnel for addition of powders and solids, up to 25 mesh, into reactions without seizing or binding.

36 36 Reactor Accessories /7299 Funnel Addition, Pressure Equalizing Funnel for use with 6433 threaded or 6527, 6528 or 6529 jointed heads (use with 6527,6528, or 6529 Head) supplied 24/40 joint at top and bottom, with threaded PTFE stopcock shutoff (use with 6433 Head) supplied with #15 Ace-Thred at top for 5846 Plug (not supplied) and drip stem with groove and long enough to be secured in a #15 Ace-Thred with Bushing and O Ring (not supplied) to restrict blowout. With threaded PTFE stopcock shutoff Replacement Plugs Cap., ml Stopcock Orifice, For For Funnel Powder Dispensing, Vertical A vertical, compact, screw feed funnel for addition of powders and solids, up to 25 mesh, into reactions without seizing or binding. Features a flexible PTFE screw thread wrapped on a precision PTFE-ceramic shaft and contained within a precision bore housing. This offers a unique flexibility in that the thread can move aside temporarily; as one spacing increases, the adjacent spacing decreases, thereby maintaining an average feed rate. Completely inert materials allow flushing with solvents without fear of contamination. #15 Ace-Thred at top offers easy disassembly for cleaning. Large 1¼ inch knob makes turning smooth and easy. Top side port is TS 14/20 outer joint, bottom inner joint is TS 24/40. Overall height, 9½ inches. Capacity, ml Funnel Powder Dispensing A vertical, compact, screw feed funnel for addition of powders and solids, up to 25 mesh, into reactions without seizing or binding. Features a flexible PTFE screw thread wrapped on a precision PTFE-ceramic shaft and contained within a precision bore housing. This offers a unique flexibility in that the thread can move aside temporarily; as one spacing increases, the adjacent spacing decreases, thereby maintaining an average feed rate. Completely inert materials allow flushing with solvents without fear of contamination. #7 Ace Thred offers easy disassembly for cleaning. Top outer and bottom inner joints are TS 14/20. Approximate capacity, 15mL ,25, Clamp Quick Release Stainless Steel Quick Release clamp for use with two-piece Pressure Reaction Flasks and Heads with Schott flanges. Available with or without extension rod for clamping to support frame. Note: Welded extension rod is 5/8 inch OD x 12 inches long for stabilizing reactor only. Reactors should be supported from below in usual manner, namely cork rings, mantle, etc , -56 WITHOUT EXTENSION WITH EXTENSION For Flange Size, (4") (6")

Reactor Accessories 37 7669 Clamp Pinch Type, Stainless Steel Spherical joint clamps made of stainless steel. With strong spring-closed, forked jaws. 7669 Size No.

Stainless steel vertical rod available 25 O.D. x 70cm (27 inches) long; 25 O.D. x 92cm (36 inches); or 25 O.D. x 122cm (48 inches).

Code -38, for connecting up to 220 O.D. vessels. Stand, only, 25 O.D. x 70cm 13550-21 Clamp Holder, only 13550-25 Stand, only, 25 O.D. x 92cm 13550-23 Chain Clamp 11079-24 Stand, only, 25 O.

Heavy base, six pounds, can accoodate vessels up to 18" in diameter within its U shape.

Two additional threaded holes in base legs to accoodate extra support rods. Complete item consists of one base and one rod.

37 Reactor Accessories Clamp Pinch Type, Stainless Steel Spherical joint clamps made of stainless steel. With strong spring-closed, forked jaws Size No. For Joint 28 28/ / /11079 Support Stand/chain Clamp Stand: Rugged, with H shaped base for use with Filter Reaction Flasks. Stainless steel vertical rod available 25 O.D. x 70cm (27 inches) long; 25 O.D. x 92cm (36 inches); or 25 O.D. x 122cm (48 inches). Clamp Holder: For connecting up to 13 O.D. mounting rod to 25 O.D. support rod. Chain Clamp: Code -24, for connecting up to 165 O.D. vessels. Code -38, for connecting up to 220 O.D. vessels. Stand, only, 25 O.D. x 70cm Clamp Holder, only Stand, only, 25 O.D. x 92cm Chain Clamp Stand, only, 25 O.D. x 122cm Chain Clamp Support Stand All-stainless-steel support stand. Heavy base, six pounds, can accoodate vessels up to 18" in diameter within its U shape. Support rod is 5 8 inch diameter, approximately 29" or 36" high, fastened to base with stainless steel lock nuts. Two additional threaded holes in base legs to accoodate extra support rods. Complete item consists of one base and one rod. For extra rods, order 29 inch, ; 36 inch, Rod Height, in See page 11 for Bench Reactor Stand Plate Support Shelf Adjustable cast alloy, black epoxy coated support shelf. With knob, measures 7 inches x 10 inches. Fits up to 5 8 inch OD rod. Plain or with 4 inch diameter hole and with 1 inch rubber around perimeter. Style/Size Solid, No Hole " Hole

38 Reactor Accessories 6433 6527/6528/6529 * Note! 60 Flange Size not as illustrated. Joints are angled.

, ml Flange I.D., (in.) Center Neck Side Necks 150-600 60 (2.

Schott-style flange and joints for use with 6384, 6386 or 6388 Reactor Bodies. 60 size has three 24/40 joints; 4 inch and 6 inch sizes have four 24/40 joints. Cap., ml Flange I.D., (in.

38 38 Reactor Accessories /6528/6529 * Note! 60 Flange Size not as illustrated. Joints are angled Head For Pressure or Filter Reactors, Ace-Threds Reactor Head, only, with Schott-style flange and Ace-Threds for use with 6384, 6386 or 6388 Reactor Bodies. Pressure rating is 35 psi. Cap., ml Flange I.D., (in.) Center Neck Side Necks (2.4") #15 (2)#15-(1)# (4") #15 (3)#15-(1)# (6") #15 (4)#15-(1)# /6528/6529 Head For Filter Reactors, Joints Reactor Head, only, with Schott-style flange and joints for use with 6384, 6386 or 6388 Reactor Bodies. 60 size has three 24/40 joints; 4 inch and 6 inch sizes have four 24/40 joints. Cap., ml Flange I.D., (in.) (2.4") (4") (6") Reaction Flask Head 3 Necks Standard 4 inch neck for use with 6475, 6476, 6477, 6479, 6480, 6481, 6491, 6492, 6493, 6497, 6498 and 9656 ACE Reaction Flasks. Supplied with three socket joints. Use 6496 Clamp for securing to flasks. Center Joint Side Joints 35/25 35/ Reaction Flask Head with Thermometer Joint For use with 6511 Flasks. With three in-line joints and a 10/30 side joint for thermometer. For Flask Cap., ml Center Joints Side Joints /40 24/ /40 24/ /42 24/ /50 24/ Head Reaction Flask, for 100 (4 inch) Flange, Four Necks Flat ground flange for use with all Reaction Flasks that have a 100 (4 inch) Schott ground mating flange. Supplied with three in-line ground joints and one 90 joint, for thermal probe connection. For adapter with #7 Ace-Thred for connecting thermometer or other type probe and permits easy vertical depth adjustment, see For clamp, see Center Joint Side Joints 24/40 24/ /42 24/ /50 24/ Head Reaction Flask, for 100 (4 inch) Flange, Five Necks Flat ground flange for use with all Reaction Flasks that have a 100 (4 inch) Schott ground mating flange. Supplied with three in-line ground joints and two 90 joints, for thermal probe connection, etc. For adapter with #7 Ace-Thred for connecting thermometer or other type probe and permits easy vertical depth adjustment, see For clamp, see Center Joint Side Joints 24/40 24/ /42 24/ /42 29/ /50 24/

Reactor Accessories 39 6529 Head Reaction Flask, for 150 (6 inch) Flange, Four Necks Flat ground flange for use with all Reaction Flasks that have a 150 (6 inch) Schott ground mating flange.

For adapter with #7 Ace-Thred for connecting thermometer or other type probe and permits easy vertical depth adjustment, see 5028. For clamp, see 6517.

Flasks that have a 150 (6 inch) Schott ground mating flange. Supplied with three in-line ground joints and two 90 joints, for thermal probe connection, etc.

Reaction Flasks that have a 200 (8 inch) Schott ground mating flange. Supplied with single, three, four or five ground joints. For clamp, see 6517.

39 Reactor Accessories Head Reaction Flask, for 150 (6 inch) Flange, Four Necks Flat ground flange for use with all Reaction Flasks that have a 150 (6 inch) Schott ground mating flange. Supplied with three in-line ground joints and one 90 joint, for thermal probe connection. For adapter with #7 Ace-Thred for connecting thermometer or other type probe and permits easy vertical depth adjustment, see For clamp, see Center Joint Side Joints 24/40 24/ /42 24/ /50 24/ Head Reaction Flask, for 150 (6 inch) Flange, Five Necks Flat ground flange for use with all Reaction Flasks that have a 150 (6 inch) Schott ground mating flange. Supplied with three in-line ground joints and two 90 joints, for thermal probe connection, etc. For adapter with #7 Ace-Thred for connecting thermometer or other type probe and permits easy vertical depth adjustment, see For clamp, see Center Joint Side Joints 24/40 24/ /42 24/ /42 29/ /50 24/ Head Reaction Flask, for 200 (8 inch) Flange Flat ground flange for use with all Reaction Flasks that have a 200 (8 inch) Schott ground mating flange. Supplied with single, three, four or five ground joints. For clamp, see Center Joint Side Joints 45/ /50 (3) 24/ /50 (2) 29/ /50 (3) 29/ /50 (3) 45/ /50 (2) 45/50 (2) 29/ O Ring Replacement Replacement O Rings for use with 6511 only Reaction Flasks with groove in ground flange. Offered in silicone or CAPFE (a resilient silicone rubber core encapsulated in continuous, thick, non-porous FEP PTFE). For Flask CAPFE Silicone Cap., ml Replacement O Rings for use with 6521, 6522, 6523, 6524, 6525, 6533, 6536 and 6537 only Reaction Flasks with groove in ground flange For Flange CAPFE Silicone I.D., in

40 Reactor Accessories 6541 Reactor Jacketed, Five Necks, with Low Dead Volume Bottom Outlet One-piece, 500mL or 1000mL jacketed Reaction Vessel with three in-line 24/40 joints; 500mL capacity vessel

#7 Ace-Threds and bushings accoodate thermocouples, inlet tubes, baffles, etc., with 6.25 to 7.25 O.D. Bottom ZDS valve is a threaded, hollowed stem with two sets of three 5 holes.

Jacket inlet and outlet are 28/15 O Ring ball joints sealed tangential to the body.

40 40 Reactor Accessories 6541 Reactor Jacketed, Five Necks, with Low Dead Volume Bottom Outlet One-piece, 500mL or 1000mL jacketed Reaction Vessel with three in-line 24/40 joints; 500mL capacity vessel has angled joints at top, 1000mL capacity vessel joints are vertical, plus two #7 Ace-Threds, and with a low dead space (0.5mL) bottom ZDS valve for draining contents. #7 Ace-Threds and bushings accoodate thermocouples, inlet tubes, baffles, etc., with 6.25 to 7.25 O.D. Bottom ZDS valve is a threaded, hollowed stem with two sets of three 5 holes. Turn clockwise until top O Ring seats to close; counterclockwise and the flask drains. Annular space of jacket is kept to a minimum to permit rapid turnover of heating/cooling liquids. Jacket inlet and outlet are 28/15 O Ring ball joints sealed tangential to the body. Top #7 Ace-Thred joint supplied with Nylon bushing and FETFE O Ring; bottom drop valve is supplied with FETFE O Ring. Chemraz or Kalrez O Rings are available. Complete item includes Body, ZDS Outlet Valve with FETFE O Rings (one -011, two -111), #7 Bushings with FETFE O Rings (-008). Capacity, ml Approx. Height, Approx. Jacket, O.D Components: Body, 500 ml, only Body, 1000 ml, only ZDS Valve, with FETFE O Rings Bushing, #7 Nylon (2) Replacement O Rings: Size -008, FETFE Size -011, FETFE Size -111, FETFE Size -008, Chemraz Size -011, Chemraz Size -111, Chemraz Temperature Monitor J-Kem, Model DM120 Monitors and displays the temperature of an attached piece of equipment on a bright LED display. Built-in USB port and free data logging software allows remote temperature monitoring, and provides a GMP, GLP compliant temperature history. Audible digital alarm available as an option. A 230VAC, CE-approved model is also available via special order. 2.5 x 4.75 x 5.5 (HxWxD) / 120vac, 50 watts, USB 2.0 J-Kem Model Temperature Range (ºC) Thermocouple Type DM120-T 200 to 250 T DM120-J 0 to 800 J DM120-K 50 to 1200 K Temperature Controller J-Kem, Model 210/Timer Same power and versatility as the Model 210, above, but also contains a 100-hour digital timer to turn heating OFF or ON at a user-specified time. A new safety feature automatically disconnects power from the heater following recovery from a power failure. Comes complete with USB port and data logging and control software. Power control computer provides 0.1 C regulation of anything. A 230VAC, CE-approved model is also available via special order. 3.5 x 6.75 x 6 (HxWxD) / 120vac, 10 amps, 1200 watts J-Kem Model With Sensor, Cord and Adapter Temperature Range (ºC) Thermocouple Type 210/Timer-T No 200 to 250 T /Timer-J No 0 to 800 J /Timer-K No 50 to 1200 K /Timer-Pt No 200 to 400 RTD /Timer-T-S Yes 200 to 250 T /Timer-J-S Yes 0 to 800 J /Timer-K-S Yes 50 to 1200 K /Timer-Pt-S Yes 200 to 400 RTD

41 Reactor Accessories Thermowell without Joint For use with 5030 Midi Ace-Thred Adapter. The completely adjustable depth feature of this combination means the well is less expensive and more versatile than the jointed style. Outside diameter, For Flask Cap., ml Length, Thermowell For use with TWO-PIECE Pressure Reactors in #15 Ace-Thred. Well has a shoulder that rides against bottom of bushing to prevent blowout. O Ring groove makes thermowell suitable for full vacuum as well as pressure use. Inner diameter of Well at top is approximately 5. Order Thermowell and Bushing separately. For Reactor Cap., ml Length, 500 (60) (4") Bushing with FETFE O Ring, only Thermowell with Joint For reaction flasks, can be used with either cylindrical or spherical type. With Length measurement is distance below joint to bottom of tube. For Flask Cap., ml Length, For Flask Cap., ml Length, /35 joint. 6500

42 Reactor Accessories 13530-10 13649-09 13649 Stirrer Laboratory, Solid State Totally enclosed, 1/40 hp., permanent magnet motor with dual 8 ( 5 16 inch) armature and gear shafts with milled flats.

42 42 Reactor Accessories Stirrer Laboratory, Solid State Totally enclosed, 1/40 hp., permanent magnet motor with dual 8 ( 5 16 inch) armature and gear shafts with milled flats. Armature shaft with maximum speed of 0 to 4000 r.p.m.; 18:1 ratio gear shaft rated 4.2 Kg. cm torque, 0 to 333 r.p.m. Baked blue enamel finish, precision die-cast housing, lifetime lubricated ball bearings with steel inserts in die-casting. Motor: Supplied with 1.5 meter 3-wire cable with plug and ground lead for connection to controller. Controller: ACE 13530* solid state 120v 60Hz, 10 amp AC or 0-120v, 6 amp DC. Features rear ring stand clamp, Fwd-Off-Rev switch. Supplied with heavy-duty 1.8 meter 3-wire power cord with NEMA plug. Controller measures 4 inches x inches x inches. Weight: 680g. Supplied with ½ A fuse plus spare to protect stirrer motor. Complete consists of motor, controller and mounting rod. Stand not included. For stand, see Motor, only, w/mounting Rod Controller, only Complete Temperature Controller Economy Model Controller, only Sensor, Type J Thermocouple, 318, 1/4" Complete Features & Specifications Bar mountable or benchtop operation. Single loop type, downsized and lightweight. Temperature Range: 50 to 800 C, adjustable. 0.1 C* or 0.1 F Temperature resolution, selectable. Absolute accuracy: ±0.25% of range, max. ±2 C. Control Accuracy: ±0.1 C typical. Microprocessor-based 1/32 DIN model for digital accuracy and reliability. Dual four-digit LED display for instant recognition of process temperature and setpoint 1 value. Auto tune PID control can maintain ±0.1 under normal conditions. Ramp and Soak, field selectable, 16 segment with hold or shut-off. Field selectable output % power limit when heating smaller vessels or when using very low setpoints. See OEM Manual (SIOH) Secure menu, affects all heaters. Output circuitry utilizes zero crossing fired solid state relay proportional control that provides interference free power (RFI) to electrical heater type resistive loads. Rear heater outlet provides time proportional control, meaning overshoot is minimized. Percent output decreases as set temperature is approached. Input power: 120 volts, 50/60 Hz, 15 amps max. Unit measures: 2 inches high x inches wide x inches deep; weight: 2 lbs, 2 oz. Operating instruction label on top for quick reference. Three-year warranty

Reactor Accessories 43 Truebore Stirrer Accessories Use the ace flexible shaft for added convenience and safety Safer when stirring corrosive liquids Safer when stirring liquids with explosive vapor

Designed with a ball bearing motor coupling at one end, for connection to any motor with an 8, (5/16-inch) diameter shaft.

The hand-piece can be supported by a standard lab clamp or hand held. The shafts operate up to 14,000rpm. Shafts should run in a counter-clockwise direction.

43 Reactor Accessories 43 Truebore Stirrer Accessories Use the ace flexible shaft for added convenience and safety Safer when stirring corrosive liquids Safer when stirring liquids with explosive vapor Available in two lengths ADAPTER (G) MOTOR COUPLING (C) HANDPIECE (B) FLEXIBLE SHAFT (A) 8081 Flexible Shaft Fully flexible drive shaft connects the motor to any size or type of reactor stir shaft. Designed with a ball bearing motor coupling at one end, for connection to any motor with an 8, (5/16-inch) diameter shaft. The other end has a detachable hand-piece with an 8 round steel pin adapter ( ) for connection to our 8124 chucks, (supplied separately). The hand-piece can be supported by a standard lab clamp or hand held. The shafts operate up to 14,000rpm. Shafts should run in a counter-clockwise direction. Typical torque ratings: sharp bend in shaft, (4 inch loop) 4.7 Kg-cm, (4 in-lbs). Straight shaft- 28 Kg cm, (24 in-lbs). Shafts measure approximately 91.4 cm, (36 inches) or cm, (60 inches) with hand-piece and motor coupling attached. Optional adapter allows for connection to motors with 9.5 (3/8-inch) O. D. shaft. Operating and lubrication instructions included. Complete units consist of: either shaft A or shaft A-1, , motor coupling for 8 motor shaft, , hand-piece with 1/4-inch collett and adapter, chuck wrench and key chain Chuck Flex-Grip, Light Weight Nylon chuck for use with 8081 Flexible Shaft and with stirring shafts or other shafts of approximately the same dimensions. Chuck has flexible insert that allows for misalignment of stirring shaft without danger of breakage. Fits standard 5 16" motor shaft or Flexible Shaft. Order Size Code For Stirring Shafts approximately For Stirring Shafts approximately For Stirring Shafts approximately Order Code (A) Flexible Shaft only, 91.4cm (A-1) Flexible Shaft only, 152.4cm (B) Handpiece with 8 adapter (G), with " and ¼" Collet, only (C) Motor Coupling for 8 shaft, only COMPLETE, 91.4cm (Consists of A, B, C & E) COMPLETE, 152.4cm (Consists of A-1, B, C & E) Additional Parts: Safety and convenience at your fingertips! Chuck Flexible Shaft 8081 Chuck wrench with key and chain Shaft Lubrication, 30mL (G) Adapter, Handpiece Adapter, Connecting ( 3 8" OD motor shaft to motor coupling) Motor see on page 565 Controller

44 Reactor Accessories For stirring up to 20 liters (H 2 O) 13523 Stirrer Variable Speed, Scale IKA RW 20 Digital Robust, slimline, ergonomic design, with digital display.

For stirring tasks up to 20 L H 2 With constant power-drive, mechanically controlled Two speed ranges for universal use from 60-2,000 rpm Push-through agitator shafts Input Power Input Power 115V

44 44 Reactor Accessories For stirring up to 20 liters (H 2 O) Stirrer Variable Speed, Scale IKA RW 20 Digital Robust, slimline, ergonomic design, with digital display. Unit features technical improvements on the trusted RW 20 series design. For stirring tasks up to 20 L H 2 With constant power-drive, mechanically controlled Two speed ranges for universal use from 60-2,000 rpm Push-through agitator shafts Input Power Input Power 115V 50/60 Hz V 50/60 Hz Specifications: MODEL Maximum viscosity 10,000 cps Motor rating, input/output 70/35W Output at stirring shaft 26W Maximum ON time 100% Maximum torque at stirring shaft per 60 rpm per 100 rpm 150 Ncm per 1,000 rpm Speed range I (50 Hz) rpm Speed range II (50 Hz) rpm Speed range I (60 Hz) Speed range II (60 Hz) Speed display digital Chuck range Hollow shaft, inner dia Diameter/length of extension arm 13 /160 Dimensions: (W x D x H) 88 x 188 x 294 Weight 212 kg, 6.8 lbs. Permissible ambient temperature 5 40 C Protection Class acc. to DIN EN IP Stirrer Basic, Variable Speed, Digital IKA Eurostar power control-visc Powerful digital laboratory stirrer for tasks up to the high viscosity range. Same features as 13516, except Labworld software* is available to allow speed and torque parameters to be controlled, regulated and documented via a PC. All features listed above for 13516, plus: Digital display presents rated actual speed Integrated torque trend display for viscosity control Analog interface for recording speed and torque RS 232 interface Input Power 115V 50/60 Hz V 50/60 Hz Specifications: For stirring up to 40 liters (H 2 O) MODEL Maximum viscosity 50,000 mpas Motor rating, input/output 130/110W Output at stirring shaft 105W Maximum ON time 100% Maximum torque at chuck 60 Ncm Speed range rpm Speed display digital Chuck range Hollow shaft, inner diameter 11 Diameter/length of extension arm 16/200 Dimensions: (W x D x H) 80 x 190 x 253 Weight 3.8 kg Permissible ambient temperature 5 40 C Permissible humidity 80% Protection Class acc. to DIN EN IP 42 Interface RS 232/analog Torque measurement trend

Reactor Accessories 45 13544 Stirrer Laboratory, Medium Torque, Variable Speed Handles light to syrupy mixtures, or up to 100L water Variable speed up to 2000 rpm, Direct Drive Constant torque

60 hz Motor shaft is 3/8" (9.5) 13544-20 Totally enclosed, non-ventilated, permanent magnet D.C.

required Overload protection a manually resetable circuit breaker for total safety On/Off switch for quick stopping if necessary Stirrers come complete as shown, including 9/16" dia.

45 Reactor Accessories Stirrer Laboratory, Medium Torque, Variable Speed Handles light to syrupy mixtures, or up to 100L water Variable speed up to 2000 rpm, Direct Drive Constant torque throughout speed range is 2.43 in-lbs. 1/15 hp motor operates at 120 VAC, 60 hz Motor shaft is 3/8" (9.5) Totally enclosed, non-ventilated, permanent magnet D.C. motor for long service life Eye level, heavy cast aluminum control box integrated with motor for safe and easy operation of stirrers Control knob electronically regulates speed of application required Overload protection a manually resetable circuit breaker for total safety On/Off switch for quick stopping if necessary Stirrers come complete as shown, including 9/16" dia. x 10" long aluminum support rod 100% backed by the best guarantee in the business: 30 Day Satisfaction Guarantee 6 Month Unconditional Guarantee Stirrer Digital Heidolph R2R Standard Series Designed for power and reliability. Easy to operate, safe, suitable for continuous operation. Stirrers are equipped with a maintenance-free brushless D.C. capacitor motor with overheating protection feature, reset by power switch. Large speed range of 40 to 2000 rpm has a mechanical speed adjustment and is monitored via a digital speed display on and making them ideal for reproducible applications; on the speed is adjusted and monitored with the help of a scaled control knob. Supplied with 13 O.D. x 160 long (approximately ½ x 6.3 ) motor support rod and key adjustable metal chuck,.5 to 10.5, for metal shafts like ACE 8074, 10 O.D. (Units feature a shaft that can be extended through the top to allow variable depth adjustment. To accomplish this, you need to order 7 O.D. shafts, supplied by Heidolph. Contact ACE for details.) To use 10 O.D. glass or PTFE shafts, metal chuck should be replaced with ACE Flex-Grip Chuck Stirrer Digital Heidolph RTR Control Electronic Series Similar to Standard Series, except with added features such as constant power. The electronic automatic control allows almost constant torque over respective speed range. The two-stage gear provides excellent mixing results even in highly viscous media, using only as much energy as actually needed. The speed desired is kept constant under changing loads, even in overload mode. (Power can be increased for a limited time to 175% or 200%, so there is no premature cutoff when overloaded.) Changes in viscosity during the process can be followed via a digital display of the torque on both and Also, both models are equipped with an analog interface enabling output of speed and torque reading to an external device (such as a chart recorder), or specification of the desired speed via PC. Analog speed and torque output, along with computer controllability (speed), is 0-10 V/4-20 ma

46 Reactor Accessories New 12840 Bench Reactor Stand New stand assembly for bench reactors from 1L to 6L sizes. Fits both pressure and filter versions as well as a standard round bottom flasks.

Motor mount accepts popular models of stir motors. Base also raises and lowers to accoodate bottom valves or large size flasks.

The flasks sit on a rubber base plate attached to the stand base.

46 46 Reactor Accessories New Bench Reactor Stand New stand assembly for bench reactors from 1L to 6L sizes. Fits both pressure and filter versions as well as a standard round bottom flasks. It will accept flasks with or without a bottom valve. Motor mount raises and lowers, as does vessel clamping system which aids in easy alignment of overhead stir motors. Motor mount accepts popular models of stir motors. Base also raises and lowers to accoodate bottom valves or large size flasks. Flask are supported bottom and top, with quick clamp for easy access to remove heads for cleaning. All primary stand components are either powder-coated or anodized aluminum. The flasks sit on a rubber base plate attached to the stand base Temperature Controller Model 410 The Model 410 is designed for heaters that cannot be operated as high as 120VAC, such as some styles of Instatherm oil baths. Maximum output voltage of the Model 410 is selected using the power output knob on the front of the controller. Selectable output voltage limit provides precise power and temperature control while protecting low voltage heaters. Comes complete with USB port and data logging and control software. Power control computer provides 0.1 C regulation of anything. 3.25" x 5.25" x 7.25" (HxWxD) / 10, 20, 40M, 60, 120 vac, 10 amps, 1200 watts J-Kem Model With Sensor Cord and Adapter Temperature Range (ºC) Thermocouple Type Order Code 410-T No 200 to 250 T J No 0 to 800 J K No 50 to 1200 K Pt No 200 to 400 RTD T-S Yes 200 to 250 T J-S Yes 0 to 800 J K-S Yes 50 to 1200 K Pt-S Yes 200 to 400 RTD Temperature Controller Model 270 Designed for processes requiring uncompromising safety. The only temperature controller available with a built-in, independent backup controller to guard against heating accidents resulting from equipment failure. The desired temperature is entered into the main temperature controller, which regulates heating, and then a high-temperature cut-off is entered into the backup limit controller. If the reaction reaches the high-temperature limit, or if a thermocouple should break, power is turned off to the heater until the controller is manually reset. Both meters independently monitor the reaction temperature. In the event that one meter fails, the other takes over to prevent a heating accident. Provides 100% redundant control. 3.75" x 7.75" x 9.25" (HxWxD) / 120vac, 15 amps, 1800 watts total 1200 watts maximum per channel J-Kem Model With Sensor, Cord and Adapter Temperature Range (ºC) Thermocouple Type Order Code 270-T No 200 to 250 T J No 0 to 800 J K No 50 to 1200 K T-S Two of each 200 to 250 T J-S Two of each 0 to 800 J K-S Two of each 50 to 1200 K

Reactor Accessories 47 12319 Temperature Controller Model 250 The Model 250 has both heating and cooling outlets for maximum versatility.

The third outlet, also 1800 watts and normally used for cooling, is prograable to provide power above, below, or at the set point. Comes complete with USB port and data logging and control software.

25" (HxWxD) / 120vac, 15 amps, 1800 watts J-Kem Model With Sensor Cord and Adapter Temperature Range (ºC) Thermocouple Type Order Code 250-T No 200 to 250 T 12319-01 250-J No 0 to 800 J 12319-03

12319-31 12319 14062-10 Vacuum Regulator No Mercury Designed for use with diaphragm vacuum pumps. In some systems, pressure is regulated by turning the vacuum pump itself on and off.

47 Reactor Accessories Temperature Controller Model 250 The Model 250 has both heating and cooling outlets for maximum versatility. Two heating outlets supply 1800 watts of power for large equipment and heating mantles up to 22 L. The third outlet, also 1800 watts and normally used for cooling, is prograable to provide power above, below, or at the set point. Comes complete with USB port and data logging and control software. Power control computer provides 0.1 C regulation of anything. 3.5" x 7.75" x 9.25" (HxWxD) / 120vac, 15 amps, 1800 watts J-Kem Model With Sensor Cord and Adapter Temperature Range (ºC) Thermocouple Type Order Code 250-T No 200 to 250 T J No 0 to 800 J K No 50 to 1200 K Pt No 200 to 400 RTD T-S Yes 200 to 250 T J-S Yes 0 to 800 J K-S Yes 50 to 1200 K Pt-S Yes 200 to 400 RTD Vacuum Regulator No Mercury Designed for use with diaphragm vacuum pumps. In some systems, pressure is regulated by turning the vacuum pump itself on and off. This unit extends the life of diaphragm pumps by never forcing the pump to start against an established vacuum, which can increase pump life by 100%. J-Kem Model DVR Precision Vacuum Regulator Perfect for vacuum distillation, unit automatically compensates for leaks in the equipment under test and maintains precise pressure, even in systems with a continuous gas purge. This computer (built-in) controlled vacuum regulator maintains pressure in the range of 0.1 to 760 Torr (atm pressure) in test instruments with volumes as small as 1 ml. Standard features include 16-step prograable pressure ramp and serial counications for PC control and data logging. J-Kem Model DVR Proportioning Valves Stainless Steel Select one for use with Digital Vacuum Regulator , above. J-Kem Model For Reactor Volumes Cv Orifice Size PSV-2 1 ml to 2 L in PSV-3 25 ml to 4 L in PSV ml to 22 L in PSV-5 1 L to 50 L in PSV-6 Large Capacity in PSV-7 Large Capacity in PSV-8 Large Capacity in PSV-9 Large Capacity in DVR-PNV Stainless Steel Needle Valve, improves regulation

48 ACE GLASS Benchtop Reactors P.O. Box 688 Vineland, NJ Fax: TOLL-FREE: FAX:

Instatherm ACE. The Safest Heating Method! Eliminate the need for heating tapes, immersion heaters and heating mantles P.

Instatherm ACE. The Safest Heating Method! Eliminate the need for heating tapes, immersion heaters and heating mantles P. ACE For Glass Vessels Borosilicate Glass Fused-to-Glass Conductive Heating Film Integral Outer Insulation Instatherm The Safest Heating Method! Eliminate the need for heating tapes, immersion heaters and