1310 Inlets. 1 of 36. Jun Illustrated Parts Breakdown Agilent 6890 Gas Chromatograph Service Manual

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1 30 Inlets This section contains illustrated parts breakdowns for 6890 GC inlets and related components. Split/Splitless Inlet Split/Splitless Inlet Column Liners Split/Splitless Inlet EPC Pneumatic Module Flow Carrier Assembly Split/Splitless Inlet Manual Pneumatic Module Capillary Injection Port (0 to 30 psig) Capillary Injection Port Sub-Assembly (0 to 30 psig) Purged/Packed Inlet Purged/Packed Inlet EPC Pneumatic Module Purged/Packed Inlet Manual Pneumatic Module Packed Column Injection Port Supplies Programmable Cool On-Column Capillary Inlet Programmable Cool On-Column EPC Pneumatic Module Programmed Temperature Vaporization Inlet Programmed Temperature Vaporization Inlet EPC Pneumatic Module Volatiles Interface Assembly Volatiles Interface EPC Pneumatics Module Solvent Vapor Exit Assembly Pneumatics Control Module Illustrated Parts Breakdown of 36

2 30 Inlets Split/splitless inlet Split/splitless inlet. O-rings HPM8 (0/pkg) Septum nut Septum, mm, solid, (25/pkg)* Nut, Merlin Microseal Septum, Merlin Microseal Top insert assembly (EPC), original New insert assembly (EPC, new trap) (Manual assy) New sampling valve/split-splitless insert assembly G G G O-ring,*.239-inch (Order No , 2/pkg) Inlet liner, split mode, standard** Split vent flow line (4.2-inch long x 0.25-inch id) G Split vent trap assembly*** Replacement filter cartridge kit (2/pkg) G G Swagelok nut, /8-inch brass (0/pkg) Swagelok back ferrule, /8-inch brass (0/pkg) Swagelok front ferrule, /8-inch brass (0/pkg) Screw, M4 x 2 mm, Torx T-20 (Captive) Inlet weldment G Heater/Sensor assembly G Screw, M4 x 8 mm, Torx T-20, chromeplated Top insulation G Washer, 2/pkg Thermal block G Block insulation G Thermal nut G Lower inlet seal, gold plated Also in stainless steel (optional) Flat thrust washer (Order no , 2/pkg) Reducing nut Insulation, (lower) G Insulation, order qty Bottom insulation cover Ferrules (identify by internal diameter):* Solid (no hole) ferrule plug Graphite ferrule 0.5 mm id (0/pkg) Graphite ferrule.0 mm id (0/pkg) Column nut* (Order no , 2/pkg) Screw, M3 x 6 mm, Torx T Plastic fitting, HPM8, (0/pkg) of 36 Illustrated Parts Breakdown

3 Inlets 30 Split/splitless inlet * Also refer to the Agilent chemical analysis consumables and accessories catalog. ** See the Column Liners table for more liners, or the Agilent chemical analysis consumables and accessories catalog. Two recommended liners are part no , deactivated split liner, and part no , deactivated splitless liner. *** Order the Replacement Split Vent Trap kit, part no. G , to replace the Split vent trap assembly, part no. G Illustrated Parts Breakdown 3 of 36

4 30 Inlets Split/splitless inlet Figure 30- Split/Splitless Inlet 4 of 36 Illustrated Parts Breakdown

5 Inlets 30 Split/splitless inlet column liners Split/splitless inlet column liners The table below lists some of the liners available for the split/splitless column. Refer to the Agilent chemical analysis consumables and accessories catalog for a complete list of liners and the specifications for each. Single-taper liner with glass wool packing, deactivated (recommended) Single-taper liner without glass wool packing, deactivated Split/Splitless liner Split liner, deactivated (recommended) Split/splitless inlet EPC pneumatic module (Part no. G , 0 to 00 psig or G , 0 to 50 psig). Male connectors /8-inch Swagelok G Screw, M4 x 45 mm, Torx T Inlet supply fitting G Screw, M3 x 2 mm, Torx T O-rings, under connectors and fitting (2/pkg) Split vent On/Off valve G For diagram of screw and O-ring placement in pneumatic modules see Figure 30-7 on page 5 of this section. Illustrated Parts Breakdown 5 of 36

6 30 Inlets Split/splitless inlet EPC pneumatic module 2 Rear view 3 4 Front view 5 Figure 30-2 Split/Splitless inlet EPC pneumatic module 6 of 36 Illustrated Parts Breakdown

7 Inlets 30 Pneumatic carrier assembly G585A Pneumatic carrier assembly G585A. Flow support bracket G Flow module back-up plate G Flow carrier assy. G PPIP manifold assy, 0 to 00 psi (with inlet) G Spacer, pressure gauge Screw, M4 25 mm, Torx T Screw, M4 2 mm, Torx T Flow cover G S/SL manifold assy., 0 to 30 psi G Nut, hex w/lkwr Reg/Gauge assy. (order part no. G577A) Chemical trap bracket Screw, machine, flat head, M4 0, Torx T Chemical trap assy Label plate, blank G Label plate, PPIP G NS Label plate, S/SL G NS Note Minimum Replacement Level is G Illustrated Parts Breakdown 7 of 36

8 30 Inlets Pneumatic carrier assembly Pneumatic carrier assembly (see Pg.7) (See Page 9) Figure 30-3 Pneumatic carrier assembly 8 of 36 Illustrated Parts Breakdown

9 Inlets 30 Split/splitless inlet manual pneumatic module Split/splitless inlet manual pneumatic module (Module and Inlet Assy. part no. G ). Flow module bracket Solenoid valve assembly, 3-way, 24Vdc G Jumper weldment Purge pressure regulator (septum) Vent tube weldment Pressure gauge spacer Pressure gauge, 0 to 30 psi Gauge jumper weldment Backpressure regulator, 0 to 30 psi Mass flow controller, 0 to 400 ml/min Chemical trap assembly Solenoid valve cable assembly G HPM8 plastic fitting pk 4. M8 O-ring pk 5. Hex nut, 5/6-inch NS Blank label plate G NS S/SL label plate G Illustrated Parts Breakdown 9 of 36

10 30 Inlets Split/splitless inlet manual pneumatic module P S C 3 4 Figure 30-4 Split/Splitless inlet manual pneumatic module 0 of 36 Illustrated Parts Breakdown

11 Inlets 30 Capillary injection port (0 to 30 psig) Capillary injection port (0 to 30 psig). SCR-Mach M mm LG SCR-Mach M4 2 mm, T-20 Torx Thread cutting screw Capillary injection port subassembly (0 to 30 psig) (Part no. G ). O-ring.239-inch (Order no /pkg) SCR-M4 8 T-20 Torx-chrm plt Reducing nut Column nut /pk 5. Gold plated seal Septum nut assembly Vent torque plate Purge regulator Insert assembly series II Washer, flat SS /pk. -mm Solsept (Order no ) 50/pkg 2. Ferrule, no hole Cap top insulation G Flow controller inlet fitting-replacement Cap inlet block insulation G Cap bottom insulation G Cap heated block G Cap thread insert G Cap thermal nut G S/S Solenoid cable assembly G Cap solenoid valve G Cap inj. heater/sensor assembly G Cap shell weldment G NS Replacement flow controller O-ring kit See also the parts list for the Split/Splitless Inlet with EPC. Illustrated Parts Breakdown of 36

12 30 Inlets Purged/packed inlet Purged/packed inlet. Screws, Torx T-20, M4 2 mm Top cover plate G Top insulation G Septum nut Septum, mm, low bleed (50/pkg) Nut, Merlin Microseal Septum, Merlin Microseal Top insert weldment Viton O-ring (Pkg/2) Heater/Sensor assembly G Screw, Torx T-0, M3 6 mm Inlet weldment G Top gasket insulation (not shown) G Thermal block G Bottom nut G PPIP insulation G PPIP bottom insulation G Glass insert (pkg/25) Vespel ferrule (pkg/0) Tubing nut (/4-inch brass) /pkg µ Column liner (see the Agilent chemical analysis consumables and accessories catalog) /8-inch Column adapter (optional) Nut warmer insulation Nut warmer cup Ferrules (identify by internal diameter): Solid ferrule plug (no hole) Graphite ferrule 0.5 mm ID /pkg Graphite ferrule.0 mm ID Column nut (Order no /pkg of 36 Illustrated Parts Breakdown

13 Inlets 30 Purged/packed inlet Figure 30-5 Exploded diagram of the purged packed inlet Illustrated Parts Breakdown 3 of 36

14 30 Inlets Purged/packed inlet EPC pneumatic module Purged/packed inlet EPC pneumatic module (Part no. G ). /8-inch Swagelok male connector SAE, brass G Inlet fitting G Screw, M4 45 mm, Torx T O-rings,.239 id (order part no , 2/pkg) 5. PPIP/EPC inlet manifold kit, not shown G For diagram of screw and O-ring placement in pneumatic modules see Figure 30-7 on page 5 of this section. 4 of 36 Illustrated Parts Breakdown

15 Inlets 30 Purged/packed inlet EPC pneumatic module 3 (see drawing below) 5 2 Front view Rear view Figure 30-6 Purged/Packed inlet EPC pneumatic module Caution Aluminum bracket removed for clarity, DO NOT completely remove the bracket during valve replacement. Aluminum bracket Screws Supply fitting O-ring Inlet split vent fitting Septum purge fitting Figure 30-7 Serviceable parts drawing for any EPC pneumatic module Illustrated Parts Breakdown 5 of 36

16 30 Inlets Purged/packed inlet manual pneumatic module and inlet Purged/packed inlet manual pneumatic module and inlet (Part no. G ). Mass flow controller, 0 to20 ml/min Gauge jumper weldment Purge vent tube weldment Pressure gauge spacer Pressure gauge (0 to 00 psi) Flow module bracket Septum purge regulator Chemical trap assembly M8 O-ring, ungreased M8 plastic fitting Vent torque plate Hex nut, 5/6-inch NS Fitting, MFC/PPIP adapter G NS PPIP/PCOC MNL-EPC adapter assy G NS Blank label plate G NS PPIP label plate G NS Torx screw, M3 6, T NS Torx screw, M4 2, T Packed Inlet Optional Flow Restrictors Colored dot code Supply pressure Flow range (ml/min) Part no. Red and purple 50 0 to Blue and purple 50 0 to Green and purple 50 0 to of 36 Illustrated Parts Breakdown

17 Inlets 30 Purged/packed inlet manual pneumatic module and inlet Figure 30-8 Purged/Packed inlet manual pneumatic module Illustrated Parts Breakdown 7 of 36

18 30 Inlets Packed column injection port supplies Packed column injection port supplies Purged packed column injection port kit Contains: -mm septa; Graphite/Vespel ferrules; Viton O-rings Deactivated disposable glass inserts Septum-purged packed column port. Septum nut Headspace retainer nut Merlin microseal Nonpurging septum nut assembly for manual flow control only Septa, -mm OD, no-hole /pkg 3. Top insert weldment Viton O-rings /pkg 5. Vespel ferrules /pkg 6. Nut, /4-inch brass /pkg 7. Liners without glass inserts: /8-inch column liner /4-inch column liner Liners with glass inserts: Series 530-µ column liner /8-inch column liner /4-inch column liner Disposable glass inserts /pkg Disposable glass inserts (deactivated) /pkg 8 of 36 Illustrated Parts Breakdown

19 Inlets 30 Programmable cool on-column capillary inlet Programmable cool on-column capillary inlet. Needle guide top (optional) Septum nut base assembly (short) Septum nut base G Manual cooling tower assembly (optional) Duckbill (for use with cooling tower, above) /pkg 6. Screw M4 8 Torx T-20 chromeplate Heatsink fin G Heater/Sensor assembly G Septa Solid /pkg Thru-hole /pkg 0. Insert spring Inserts (identify by number of rings on insert): Narrow bore insert; 200 µ silver ring Wide bore insert; 320 µ 5 silver rings Megabore insert; 530 µ 0 rings Capillary Insert (glass columns) 3 silver rings AL megabore 4 rings µ bore insert 6 rings T-20 screws (captive) M4 2 mm T-0 Torx M3 6-mm screw Inlet weldment G Inlet weldment insulation G Cavity sleeve Ferrules (identify by internal diameter): Solid ferrule plug (no hole) Graphite ferrule 0.5 mm ID /pkg Graphite ferrule.0 mm ID /pkg 8. Column nut (Order no /pkg) Illustrated Parts Breakdown 9 of 36

20 30 Inlets Programmable cool on-column capillary inlet Figure 30-9 Exploded diagram of the programmable cool on-column inlet 20 of 36 Illustrated Parts Breakdown

21 Inlets 30 Programmable cool on-column EPC pneumatic module Programmable cool on-column EPC pneumatic module 0 to 00 psig (part no. G ). Male connect /8-inch Swagelok Inlet block fitting G EPC valve replacement kit G Screws, inlet block, M3 2 mm, not shown For diagram of screw and O-ring placement in pneumatic modules see Figure 30-7 on page 5 of this section. 3 2 Front view Rear view Figure 30-0 Programmable cool on-column pneumatic module Illustrated Parts Breakdown 2 of 36

22 30 Inlets Programmed temperature vaporization inlet Programmed temperature vaporization inlet. Septumless head G Septum head* G Septum nut* PTV inlet assy G PTV cryo insulator (not shown) G PTV LCO 2 cooling jacket G PTV LN 2 cooling jacket G Silver seal (5/pk) Graphpack inlet adapter 0.2 mm Column ID mm Column ID mm Column ID Ferrules for graphpack inlet 0.2 mm Column ID (0/pk) mm Column ID (0/pk) mm Column ID (0/pk) mm Column ID (0/pk) Split nut for inlet adapters Screws, M mm 3 3. PTV insulation block G PTV septumless gang weldment G PTV septum gang FTG weldment G Replacement filter kit G PTV front trap assy G Trap nut G Teflon ferrule (needle seal) Kalrez seal** Valve body** Pressure spring** Viton seal Sealing element PTV column adapter tube G D Graphpak ferrules, not shown (5/pkg) D Graphpak assembly Tool, not shown G *See the Agilent chemical analysis consumables and accessories catalog for Merlin assemblies. **Service kit, part no , consists of items 20, 2, and of 36 Illustrated Parts Breakdown

23 Inlets 30 Programmed temperature vaporization inlet 4, ,7 25 Septum head Figure 30- Exploded diagram of the programmed temperature vaporization inlet Illustrated Parts Breakdown 23 of 36

24 30 Inlets Programmed temperature vaporization inlet calibrated manifold assembly Programmed temperature vaporization inlet calibrated manifold assembly (part no. G ). PTV thermocouple PCB G PTV thermocouple PCB cable G Calibrated manifold assembly G Male connectors /8-inch Swagelok G Inlet fitting block G For diagram of screw and O ring placement in pneumatic modules see Figure 30-7 on page 5 of this section. 24 of 36 Illustrated Parts Breakdown

25 Inlets 30 Programmed temperature vaporization inlet calibrated manifold assembly Figure 30-2 PTV flow module Illustrated Parts Breakdown 25 of 36

26 30 Inlets PTV LCO 2 cryo assembly PTV LCO 2 cryo assembly (part no. G ) (Recommended replacement level). PTV LCO 2 brazement (valve to IP tube) G PTV LCO 2 valve bracket G CO 2 cryo valve G Cap prot W/O Flg Scr-mach inch /8-inch male conn W/O O-ring G Gland seal LCO 2 G TFE seal G ,3 Figure 30-3 PTV LCO 2 cryo assembly 26 of 36 Illustrated Parts Breakdown

27 Inlets 30 PTV LN 2 cryo assembly PTV LN 2 cryo assembly (part no. G ) (Recommended replacement level). PTV LN 2 nut plate G PTV LN 2 supply tube G PTV/CFO LN 2 insulation cover G PTV LN 2 -cell inlet tube G Cryo valve G PTV inlet tube insulation G PTV solenoid bracket G PTV jumper cable G Nut /4-inch tubing SS Connector Connector male /4-inch ferrule set SST Tape industrial 4. Cap protective 5. MS LG Figure 30-4 PTV LN 2 cryo assembly Illustrated Parts Breakdown 27 of 36

28 30 Inlets Volatiles interface Volatiles interface. VI top cover G Top insulation G Screw, M4 x Clamping plate G Volatiles interface G NS Ferrule, /6-inch, (0/pk) NS Blanking nut /6-inch SS NS Male nut, /6-inch VI heater/sensor assy G Heater block assy G VI insulation htr block G Pneumatic gang fitting assy G Contains: Gen. make-up restrictor O-ring Torx screw Replacement filter kit G or 0. Filter trap assy (not shown) G RP filter G /pk 2. Nut, male /6-inch swage Vol. front trap assy G Trap nut G *Also refer to the Agilent chemical analysis consumables and accessories catalog. 28 of 36 Illustrated Parts Breakdown

29 Inlets 30 Volatiles interface Figure 30-5 VI manifold assembly 0 to 00 psig Illustrated Parts Breakdown 29 of 36

30 30 Inlets Volatiles interface calibrated manifold assembly Volatiles interface calibrated manifold assembly (part no. G ). Male connectors /8-inch Swagelok G Screw, M4 45 mm, Torx T Inlet supply fitting G Screw, M3 20 mm, Torx T O-rings, under connectors and fitting (2/pkg) For diagram of screw and O ring placement in pneumatic modules see Figure 30-7 on page 5 of this section. 30 of 36 Illustrated Parts Breakdown

31 Inlets 30 Volatiles interface calibrated manifold assembly 2 3A 3 4 Figure 30-6 Volatiles interface flow module Illustrated Parts Breakdown 3 of 36

32 30 Inlets Solvent vapor exit accessory Solvent vapor exit accessory (part no. G ). SVE valve/fitting assembly G Valve jumper cable G Mach. screw, M4 x NS SVE software kit G NS SVE calculator SW disk G NS SVE manual-installation and Operation G NS SVE Tri-column assembly G NS Union SS /6-inch tubing NS Chemical sample ECD kit NS /6-inch tube SS 560 mm NS Graphite ferrule (2/pk) ( /pk) NS 320 µm graphite/vespel ferrule ( /ea.) NS 0.4 mm, 200, 250 µm ferrule ( /ea.) NS Bleed column, 50 µm, 2M G NS Valve driver cable G NS Unboxed HP-5MS 30 m, 0.25 mm, S-433A NS Column nut NS SVE pre-column assembly G *Also refer to the Chemical Analysis Consumables and Accessories Catalog. 32 of 36 Illustrated Parts Breakdown

33 Inlets 30 Solvent vapor exit accessory 2 3 Figure 30-7 Solvent vapor exit accessory Illustrated Parts Breakdown 33 of 36

34 30 Inlets Pneumatics control module Pneumatics control module (part no. G ). /8-inch SwageLok male connector, SAE, brass G PSIG inlet supply fitting G Screw, M4 45 mm, Torx T O-rings,.239 ID (Order part no , 2/pkg) NS PCM gang weldment G Front view Rear view Figure 30-8 Pneumatics control module 34 of 36 Illustrated Parts Breakdown

35 Inlets 30 Pneumatics control module Aluminum bracket Screws Supply fitting O-ring Septum purge fitting Figure 30-9 Serviceable parts drawing pneumatic control module Illustrated Parts Breakdown 35 of 36

36 30 Inlets Pneumatics control module 36 of 36 Illustrated Parts Breakdown

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