High Pressure Valves. MX Series II Modules Manual Sample Injection Switching

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1 High Pressure Valves MX Series II Modules Manual Sample Injection

2 Introduction to High Pressure Valves HIGH Pressure Valves High Pressure Valves Introduction Rheodyne valves fit virtually any flow control application. As you ll see from the table below and on the following pages, there are valves for preparative, analytical, nano, and microscale analysis in a variety of flow configurations. Pressure ratings of the valves in this chapter range from psi (9 bar) to,000 psi (0 bar). Rheodyne is committed to providing cutting-edge, user-friendly products. MX Series II Modules are actuated electronically and can be easily adapted to existing instrumentation using contact closure, BCD, I C, USB, or used as stand alone devices. Rheodyne s industry standard sample injectors and switching valves are designed for manual actuation. Locate the valve module and flow configuration of choice using the table below. Valve Configurations: Valve Module MXT Modules: Very High Pressure (<,000 psi) MXP Modules: High Pressure (<,000 psi) MXX Modules: Low Pressure (< psi) Manual Sample Injectors Manual Valves Flow Configuration -position, -port -position, 7-port Selection -position, -port (analytical and nano scale) -position, -port Vertical Port -position, 0-port Selection (analytical and nano scale) -position, 7-port Selection -position, -port (analytical and prep scale) -position, -port Double -Way -position, 7-port Selection (analytical and prep scale) 0-position, -port Selection Dual Mode Analytical, Micro and Preparative Scale Injector Single Mode Analytical and Micro Scale Injectors -position, -port -position, -port -Way and -Way -position, 7-port Selection Connecting Tubing Size Page / OD 8 / or / OD / or /8 OD.00, / or /8 OD / or /8 OD , 9 9 Genuine Rheodyne valve accessories are also featured in this chapter. Please see the pages indicated below for more information on these valve consumables: Vespel, Tefzel, and PEEK Rotor Seals; Stainless Steel, PEEK, and Propriety Material Stators (page 9) Rheodyne RheBuild Kits (page 9) stainless Steel and PEEK Sample Loops (page 9 and 97) Needle Port Accessories, Mounting Brackets, and the Rheodyne Wrench (page 00 and 0) Upchurch Scientific Micro Injection Port Adapters are also available on page 0. ORDER ONLINE ORDER

3 HIGH Pressure Valves Introduction to Rheodyne MX Series II Modules MX Series II Valves Introduction Stack Channels The new line of Rheodyne MX Series II automated fluidic valves provide productivity enhancing solutions for today s demanding analytical methods. Combine MX Series II modular valves with your current instrument to support complex fluid switching and sample injection needs. Flexible Automation The MX Series II modular valves are flexible to meet changing needs. Several options are available for connecting the valves to your analytical instrument or PC, including contact closure, BCD, I C, and USB. Commands can be sent to the MX Series II valves using your chromatography software or TitanMX software (included) for timed-events programmability. MX Series II valves can be controlled remotely or operated manually using the push-button front panel with LED position indicator. Increase Laboratory Capability The MX Series II modules are available in a variety of flow paths including options for Nano, Semi-prep, Low Pressure, and Fast Chromatography applications up to,000 psi (,0 bar). These modules feature the reliable automation of Titan valves, saving valuable resource time and increasing overall productivity. Snap Channels REMOTE Valve Position Indicator Manual Operation Forward Position Selector Backward Position Selector Remote Operation Snap n Stack Ribs Remote Operation Button Remote Operation Indicator Light Reduce Downtime The High Pressure and Fast Chromatography MX Series II modular valves feature the Rapid Replacement Pod design for easy maintenance. The Rapid Replacement Pod is a complete, factory assembled and tested liquid-end, providing virtually zero downtime maintenance. Traditional RheBuild kits are also available. The Low Pressure MX Series II modular valves make changing fluidic connections quick and easy with our patented TitanEX fitting-less tubing connection system. These long-life polymer valves meet the reliability needs of demanding applications. Versatile MX Series II Modules are designed to increase productivity, expand laboratory capabilities, save time, and make life easier. Rheodyne s MX Operating Manual including installation instructions is available at instructions.aspx. 8 ORDER

4 Rheodyne MX Series II Modules HIGH Pressure Valves Application Note Typical Solutions S ample Injection T wo- Selection A lternating Regeneration H igh Speed Sample Enrichment H igh Speed Sample Clean Up C olumn Backflushing Position Position Flow path of MXT Two-Position, Six-Port Valve. Multi-Dimensional Proteomic Peptide Separation Sample S olvent Selection F raction Collection S ix Selection These applications are discussed and illustrated in Rheodyne s MX Series II Solutions Guide at rheodyne/operating_instructions.aspx Sample Position Position Flow path of MXT Two-Position, Six-Port as an Injection Valve. MX Series II Module Specifications: Maximum Pressure Power Requirements MXT:,000 psi (,0 bar) MXP:,000 psi ( bar) MXX: psi (9 bar) Nano: 0.0 mm (0.00 ) diameter Analytical: 0. mm (0.00 ) diameter Preparative:. mm (0.00 ) diameter 00-0 VAC, 0-0 Hz Regulatory Compliance CE Mark Remote Control USB, IC, BCD, Level Logic Operating Temperature 0 0 C, non-condensing Storage Temperature 0 7 C Dimensions ( H x W x D) 7 mm x 7 mm x 8 mm (. x.0 x.0 ) Flow Passages Position Position ORDER Position Flow path of MX Series II Six-Position, Seven-Port Selector Valve. Position 7 Flow path of MXP and MXX Two-Position, Six-Port Valve. Position Flow Path of MX Series II Double Three-way Valve. Position Flow path of MX Series II Two-Position, Ten-Port Valve Position 0 Sample Position Flow path of MXP and MXX Two-Position, Six-Port as an Injection Valve. 8

5 HIGH Pressure Valves MX Series II Valves MXT Valves for Fast Chromatography New valves for ultra-high performance applications can withstand up to,000 psi (,0 bar) made from Stainless Steel UltraLife material Available in a two-position and a six-position version The MXT7-000 is a new -position, -port switching valve. This valve model is ideal for use as a two-column switching valve, enabling the same system to be used with more than one column to easily accommodate multiple users and applications. It can also be used in a traditional injection valve configuration and offers the Rheodyne patented MBB (Make-Before-Break) feature for improved reproducibility and system stability. The MXT7-0 is a -position, 7-port selector valve. This valve is ideal for use in conjunction with a second identical valve for rapid column selection and applications which include more than two columns (see Application Note on page ). MXT valves feature UltraLife materials and are capable of withstanding up to,000 psi (,0 bar). Each valve has minimal port-to-port volume of 0. µl. Each MXT valve comes complete with the fittings required to make initial tubing connections. As an added benefit, MXT valves feature the popular Rapid Replacement Pod design for quick and easy maintenance. Within seconds you can easily remove the entire valve pod from the actuator and insert a spare pod, reconnect your fittings, and begin running your application. Please Note: Please contact us regarding replacement rotor seals for the new MX Series II Valves. MXT Valve Dimensions - inches (mm) TOP SELLER see starred products in price block. 8 ORDER MXT HPLC VALVES Material MXT position, -port Valve Stainless Steel UltraLife $,9.0 MXT7-0 -position, 0-port Valve Stainless Steel UltraLife,89.0 MXT7-0 -position, 7-port Selector Valve Stainless Steel UltraLife,7.0 RAPID REPLACEMENT PODS PD7-000 Rapid Replacment Pod for MXT7-000 ea. $ 9.70 PD7-0 Rapid Replacment Pod for MXT7-0 ea.,0.0 Fast Chromatography Sample Loops* Volume µl Stainless Steel Sample Loop ea. $ µl Stainless Steel Sample Loop ea µl Stainless Steel Sample Loop ea µl Stainless Steel Sample Loop ea µl Stainless Steel Sample Loop ea Replacement FITTINGS UH-9x Stainless Steel Ferrules 0-pk $ 9.7 UH-9x Stainless Steel Nut, with UH-9 Ferrules, 0- * All Fast Chromatography loops are rated to,000 psi. 0-pk 98.

6 MX Series II HIGH Pressure Valves MXP High Pressure Valves for HPLC New switching, selection, and injection valve models Can withstand up to,000 psi ( bar) chemically compatible for use with most mobile phase compositions Available with analytical and nano-scale flow paths The Rheodyne MXP valve is the standard -position, -port switching valve designed for traditional HPLC and related techniques, used for traditional sample injections or to provide dual-column functionality in your system. For applications where biocompatibility is needed, consider the MXP , and when performing nanoscale applications, use the MXP model. The MXP is a -position, 0-port switching valve that easily facilitates an alternating column regeneration process which can reduce your per-sample run time and can dramatically increase your overall sample throughput annually. For biocompatible applications, Rheodyne provides the MXP , and for nano-scale applications, the MXP is available. The MXP is a -position, 7-port switching valve and is ideal for use in conjunction with a second identical valve to facilitate rapid column selection for applications using more than two columns. MXP is a special -position, -port injection valve featuring a vertical injection port and includes a needle-port fitting for syringeloaded injections. These MXP valves are capable of withstanding up to,000 psi ( bar). Each standard valve features a small port-to-port volume of only 0. µl or less, while the nano-scale valves offer port-to-port volumes of less than 0 nl. Each valve comes complete with the fittings required to make initial tubing connections. MXP Valve Dimensions - inches (mm) MXP valves feature the popular Rapid Replacement Pod design for quick and easy maintenance. Within seconds, you can easily remove the entire valve pod from the actuator and insert a spare pod, reconnect your fittings, and begin running your application. Please Note: Please contact us regarding replacement rotor seals for the new MX Series II Valves. TOP SELLER see starred products in price block. ORDER MXP HPLC VALVES Material MXP position, -port Valve Stainless Steel DuraLife $,8.70 MXP position, -port Vertical Port Valve Stainless Steel DuraLife,.0 MXP position, 0-port Valve Stainless Steel DuraLife,7.0 MXP position, 7-port Selection Valve Stainless Steel DuraLife,.00 MXP position, -port Nano Valve Titanium DuraLifeII,9.0 MXP position, 0-port Nano Valve Titanium DuraLifeII,7.0 MXP position, -port Valve, PEEK,9.90 Biocompatible MXP position, 0-port Valve, Biocompatible PEEK,.0 RAPID REPLACEMENT PODS PD7900 Rapid Replacement Pod for MXP ea. $ 7.0 PD790 Rapid Replacement Pod for MXP ea PD790 Rapid Replacement Pod for MXP ea. 8.0 PD7970 Rapid Replacement Pod for MXP ea. 8.0 PD7980 Rapid Replacement Pod for MXP ea.,.0 PD798 Rapid Replacement Pod for MXP ea.,.0 PD9900 Rapid Replacement Pod for MXP ea PD990 Rapid Replacement Pod for MXP ea..0 Replacement FITTINGS Stainless Steel Standard Fittings, 0-pk $.90 with Ferrules, /, RheFlex One-piece Fittings, 0-pk 9.70 /, 0-, PEEK, Natural M RheFlex Fittings, /, PEEK, Natural 0-pk 8.0 8

7 HIGH Pressure Valves MX Series II MXX Low Pressure Valves New switching and selection valve models Can withstand up to psi (9 bar) Rheodyne proprietary polymer combination allows interface for long life All models accept / or /8 tubing and fittings The MXX777-0 is the standard -position, -port switching valve designed for traditional low pressure chromatography and applications including sample injections and flow diversion for your system. All MXX valves accept either / or /8 tubing. Both ferrule sizes are shipped with all models. Analytical scale models come with / ferrules installed in the valve, and Large Bore models come with /8 ferrules installed. Simply unscrew the spanner and remove the ram to access and switch the ferrules to accommodated the other size tubing. For higher flow rates and semi-preparative applications the large bore MXX777- is available. The MXX777-0 and MXX777- are -position, 7-port selection valves for analytical and semi-preparative applications, respectively. These valves work well for either pre-pump solvent selection or for post-column fraction collection. For even greater application versatility, try the MXX position, -port selection valve. The MXX777-0 is a -position, -port valve with a double three-way flow path, offering two, -way diverter valves in one platform. These MXX valves are capable of withstanding up to psi (9 bar) and utilize proprietary RPC-7 proprietary polymer combination. An additional, unique feature of the low-pressure MXX valves is their fitting-less tubing connection, where no threaded fittings are required only special ferrules, which are included to facilitate the initial tubing connections, are needed. MXX Valve Dimensions - inches (mm) Please Note: Please contact us regarding replacement rotor seals for the new MX Series II Valves. 8 ORDER MXX LOW PRESSURE VALVES Material MXX777-0 position, -port Valve RPC-7* $,.0 MXX777-0 position Double Three-Way Valve RPC-7,0.0 MXX777-0 position, 7-port Selection Valve RPC MXX777- -position, -port Large Bore Valve RPC MXX777- -position, 7-port Large Bore Selection Valve RPC MXX position, -port Selection Valve RPC-7,.90 Replacement FITTINGS Ferrules for /8 OD tubing -pk $ Ferrules for /8 tubing 0-pk Ferrules for /8 tubing 00-pk Ferrules for / OD tubing -pk Ferrules for / tubing 0-pk Ferrules for / tubing 00-pk O-rings for / OD tubing -pk.0 * RPC-7 Proprietary Polymer Combination

High Pressure Valves. MX Series II Modules Manual Sample Injection Switching

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