Thermo Scientific. TRACE GC Ultra. Gas Chromatograph Spare Parts Catalog. PN , Revision October 2011

Transcription

1 Thermo Scientific TRACE GC Ultra Gas Chromatograph Spare Parts Catalog PN , Revision October 2011

2 TRACE GC Ultra Spare Parts Catalog October 2011 Edition Part Number Thermo Fisher Scientific Inc. All rights reserved. Printed in Italy Published by Thermo Fisher Scientific S.p.A., Strada Rivoltana, Rodano - Milan - Italy Tel: Fax: Printing History: First Edition, released June 1998 Second Edition, released November 1998 Third Edition, released June 1999 Fourth Edition, released June 2001 Fifth Edition, released January 2002 Sixth Edition, released September 2002 Sevenths Edition, released May 2003 Eighth Edition released, October 2003 Ninth Edition, released April 2004 Tenth Edition, released July 2004 Eleventh Edition, released March 2005 Twelfth Edition, released September 2005 Thirteenth Editions, released January 2006 Fourteenth Edition, released June 2006 Fifteenth Edition, released January 2007 Sixteenth Edition, released May 2007 Seventeenth Edition, released October 2007 Eighteenth Edition, released April 2008 Nineteenth Edition, released July 2008 Twelfth Edition, released April 2009 Twenty-first Edition, released September 2009 Twenty-second Edition, released May 2010 Twenty-third Edition, released December 2010 Twenty-fourth Edition, released October 2011 Disclaimer Technical Information contained in this publication is for reference purposes only and is subject to change without notice. Every effort has been made to supply complete and accurate information; however, Thermo Fisher Scientific assumes no responsibility and will not be liable for any errors, omissions, damage, or loss that might result from any use of this manual or the information contained therein (even if this information is properly followed and problems still arise). This publication is not part of the Agreement of Sale between Thermo Fisher Scientific and the purchaser of a TRACE GC system. In the event of any conflict between the provisions of this document and those contained in Thermo Fisher Scientific s Terms and Conditions, the provisions of the Terms and Conditions shall govern. Reference to System Configurations and Specifications supercede all previous information and are subject to change without notice. Trademarks TRACE GC Ultra is a trademark of Thermo Fisher Scientific Inc., and its subsidiaries. Other brand and product names may be trademarks or registered trademarks of their respective companies.

3 Contents Chapter 1 Electronics... 6 Chapter 2 Pneumatics... 8 Chapter 3 Split/Splitless Injector Chapter 4 Large Volume Splitless Injector Chapter 5 Cold On-Column Injector for Standard Automatic Injections Chapter 6 Cold On-Column Injector Direct Narrow-bore Chapter 7 Cold On-Column Injector Chapter 8 Purged Packed Column Injector Chapter 9 Packed Column Injector Chapter 10 Programmed Temperature Vaporizing Injector Chapter 11 Flame Ionization Detector (FID) Chapter 12 Nitrogen Phosphorus Detector (NPD) Chapter 13 Electron Capture Detector (ECD) Chapter 14 Flame Photometric Detector (FPD) Spare Parts Catalog 3

4 Contents Chapter 15 Photoionization Detector (PID)...40 Chapter 16 Thermal Conductivity Detector (TCD)...42 Chapter 17 Discharge Pulsed Detector (PDD)...44 Chapter 18 Detectors Base Bodies...46 Chapter 19 Adapters for Packed Columns...48 Chapter 20 On-Column Large Sample Volume Injection...54 Chapter 21 Automatic Gas Sampling Valve...58 Chapter 22 Miscellanea...60 Chapter 23 AI/AS 3000 & AI/AS 3000 II Autosamplers...64 Chapter 24 TriPlus Autosampler...68 Chapter 25 TriPlus RSH Autosampler...78 Chapter 26 Valve Oven...80 Chapter 27 Ultra Fast Module Option...82 Appendix A Customer Communication Spare Parts Catalog

5 Contents Spare Parts Catalog 5

6 1 Electronics Table 1-1. Electronics spare parts No 1 Keyboard assembly Motherboard with bracket FID 201 printed circuit board (this board replaces the FID controller printed circuit board PN ) 2 NPD controller printed circuit board ECD controller printed circuit board FPD controller printed circuit board PID controller printed circuit board TCD controller printed circuit board PDD controller printed circuit board DRH 2000 printed circuit board (for Ultra Fast Module applications) External detector printed circuit board CPU printed circuit board CPU/LAN printed circuit board Analog feedback printed circuit board EPC printed circuit board Detector simulator printed circuit board Cryo control printed circuit board Thermocouple card adapter for PTV/HOT OC Semiautomatic OC actuator printed circuit board driver PC board Power assy Power supply assembly without breaker Breaker 16 A (115 V V) for power supply assembly Transformer 48 V (FID/ECD/FPD/TCD/PTV) It Includes: protection disk, metal plate, 6 x 30 mm fixing screws, spacer (PN ) Spare Parts Catalog

7 Chapter 1 Electronics Table 1-1. Electronics spare parts Transformer 48 V (NPD). It includes: protection disk, metal plate, x 20 mm fixing screws, spacer (PN ) Fuse, Slow-blow, 2 A, 5x20 mm Fuse, Slow-blow, 5 A, 5x20 mm Spare Parts Catalog 7

8 2 Pneumatics Table 2-1. Digital Carrier Controller (DCC Module) Spare parts No 1 Flow regulator mod 250 kpa for OC or PKD injector Flow regulator mod 1000 kpa for OC or PKD injector Flow regulator mod 250 kpa for PPKD injector Flow regulator mod 1000 kpa for PPKD injector Flow regulator mod 250 kpa for S/SL and PTV injectors Flow regulator mod 1000 kpa for S/SL and PTV injectors Flow regulator mod ECD only (AA) Flow regulator mod ECD, PID, FPD, FID w/o make-up (AB) Flow regulator mod TCD only (AB-HWD) Flow regulator mod NPD, ECD, PID, FPD, FID w/o make-up (AD) Flow regulator mod ECD, PID, FPD, FID with make-up (AC) Table 2-2. Digital Pressure Flow Controller Miscellanea Spare parts No 1 Cable for carrier gas flow regulator 26 poles Cable for detector gas flow regulator 20 poles O-ring for injector/detector to gas regulator connection O-ring PARKER COL TYPE V BROWN Three-way Solenoid valve for DCC switching Built in active carbon filter Column-flow meter connector Charcoal filter kit

9 Chapter 2 Pneumatics Table 2-3. Digital Pressure Flow Controller Gas Fittings No Kit DCC Gas Fittings The kit includes: 1. O-ring for 1/8 union to gas regulator connection 2. Joint 5/16 plus filter 3. Conical ferrule 1/8 4. Nut 5/16 for 1/8 tubing

10 3 Split/Splitless Injector Table 3-1. Split/splitless Injector spare parts No 1 Septum cap Septum cap to be used with TriPlus HS Septum holder Septum Septum support Liner cap A Liner, split 3 mm B Liner, split 5 mm C Liner, splitless 3 mm D Liner, splitless 5 mm E Liner, wide bore columns F Liner, for polar solvent G Liner double gooseneck for nano-volumes injections H Liner, 0.8 mm Liner seal Liner cap removing tool Silver seal Terminal fitting for capillary columns Nut for terminal fitting Graphite ferrule for 0.1 and 0.25 mm ID column Graphite ferrule for 0.32 mm ID column Graphite ferrule for 0.53 mm ID column Fixing nut for column Brass ferrule, 1.6 mm ID Brass ferrule, 2 mm ID S/SL main body including heating block without filter Spare Parts Catalog

11 Chapter 3 Split/Splitless Injector Table 3-1. Split/splitless Injector spare parts (Continued) 15 Kit Assy Split line 1/ a: Tubing split 1/8 b: Brass nut 5/16 for 1/8 tubing c: Brass Front/Back ferrule for 1/8 tubing d: Nut M6x0.75 mm e: 1/16 ID Brass ferrule Brass front/back ferrule for 1/8 tubing (set of 5) Brass nut 5/16 for 1/8 tubing Brass ferrule 1.6 mm ID (set of 10) Nut M6x0.75 mm Blanking disk for leak test S/SL body- Inj/Det cassette fixing nut Adapters for packed columns See Chapter 19 Split line filter Carrier filter Heater 115 V Heater 230 V Temperature sensor Assy Double Injector S/SL71 (w/o heater and temp heater) DoublePro injector heating block (it includes two P/N and two P/N ) Kit SSL-BKF (including the Tee holder and 1 Tee connector with ferrules and nuts) Kit Tee Holder for BKF (Tee holder including 1 Tee connector with ferrules and nuts) Assy Tee connector for BKF holder (including Tee connector with ferrules and nuts, clamp and screw) Tee connector Locking nut M4 carved Graphite ferrule 0.8 mm ID Graphite ferrule 1.0 mm ID Spare Parts Catalog 11

12 Chapter 3 Split/Splitless Injector Table 3-1. Split/splitless Injector spare parts (Continued) Deactivated uncoated precolumn, 2 m length; 0.5 mm ID Stainless Steel Tube 0.5 m length; 0.9 mm OD; 0.5 mm ID for Tee connector a b c de A 6B 6C 6D 6E 6F 6G 6H 12 Spare Parts Catalog

13 Chapter 3 Split/Splitless Injector Spare Parts Catalog 13

14 4 Large Volume Splitless Injector Table 4-1. Large Volume Splitless Injector spare parts No LVI Analytical kit for SSL The kit comprises: the parts 1, 2, 3, 4, 5, 9A, 17, P/N , P/N , P/N , P/N Septum Cap mm OD BTO Septum with center guide Ring Nut Septum Holder LVSL Adapter removing tool O-ring Liner Cap Metal Ring (already installed on the liner; see 9A and 9B) Vespel liner seal (already installed on the liner; see 9A and 9B) --- 9A Glass liner packed with deactivated glass wool Deactivated glass wool (10 g) B Deactivated laminar liner (optional) Liner cap removing tool Silver seal Terminal fitting for cap. columns Nut for terminal fitting Washer Graphite ferrule for 0.25 mm ID column Graphite ferrule for 0.32 mm ID column Graphite ferrule for 0.53 mm ID column Brass ferrule, 1.6 mm ID Brass ferrule, 2 mm ID Fixing nut for column m, 0.32 mm ID, uncoated pre-column Spare Parts Catalog

15 Chapter 4 Large Volume Splitless Injector Table 4-1. Large Volume Splitless Injector spare parts (Continued) Universal glass press-fit for pre-column /column connection S/SL main body including heating block without filter Kit Assy Split line 1/ a: Tubing split 1/8 b: Brass nut 5/16 for 1/8 tubing c: Brass Front/Back ferrule for 1/8 tubing d: Nut M6x0.75 mm e: 1/16 ID Brass ferrule Kit assy dummy filters Brass front/back ferrule for 1/8 tubing (set of 5) Brass nut 5/16 for 1/8 tubing Brass ferrule 1.6 mm ID (set of 10) Nut M6x0.75 mm L syringe (0.63/50/cone) removable needle S/SL body- Inj/Det cassette fixing nut Blanking disk for leak test Split line filter Heater 115 V Heater 230 V Temperature sensor Spare Parts Catalog 15

16 Chapter 4 Large Volume Splitless Injector a b c de b A 9B 16 Spare Parts Catalog

17 Chapter 4 Large Volume Splitless Injector Spare Parts Catalog 17

18 5 Cold On-Column Injector for Standard Automatic Injections This inlet works in combination with the TriPlus autosampler allowing standard injections into a 0.53-mm ID capillary column. Table 5-1. Cold on-column Injector for TriPlus autosampler spare parts No 1 Seal, PTFE Clip Needle guide Seal Holder O-ring OC base Vespel ferrule for 0.25 mm ID column Vespel ferrule for 0.32 mm ID column Vespel ferrule for 0.53 mm ID column Backwasher/cooling sleeve for OC Column retaining nut and backwasher for OC Cooling fan 115 V Cooling fan 230 V Solenoid valve, secondary cooling Kit On-Column Actuator for TriPlus The kit includes: A = Cold on-column injector head for TriPlus sample B = Automatic actuator Assy C = Control Interface D = Control interface to TriPlus sampler connecting cable Spare Parts Catalog

19 Chapter 5 Cold On-Column Injector for Standard Automatic Injections A B C D Spare Parts Catalog 19

20 6 Cold On-Column Injector Direct Narrow-bore This inlet works in combination with the TriPlus autosampler allowing direct injections into a 0.25/0.32-mm ID capillary column without the need of using a pre-column. Table 6-1. Cold on-column Injector for TriPlus autosampler spare parts No 1 Seal, PTFE Clip Needle guide Seal Holder Vespel ferrule for 0.25 mm ID column Vespel ferrule for 0.32 mm ID column Vespel ferrule for 0.53 mm ID column Backwasher/cooling sleeve for OC Column retaining nut and backwasher for OC Kit On-Column direct narrow-bore for TriPlus Cooling fan 115 V Cooling fan 230 V Solenoid valve, secondary cooling On-Column injector head assy Kit upgrade OC direct narrow bore for TriPlus Syringe 10 L for OC narrow-bore Spare needle for syringe PN Crimp caps, 11 mm (set of 100) Snap cap, 20 mm (set of 10) Rubber o-ring for 11 mm caps (Set of 100) Rubber o-ring for 20 mm caps (Set of 10) Tin discs (set of 100) Crimp-top vial, 2 ml (set of 100) Vials, 10 ml (set of 5) Spare Parts Catalog

21 Chapter 6 Cold On-Column Injector Direct Narrow-bore Spare Parts Catalog 21

22 7 Cold On-Column Injector Table 7-1. Cold on-column Injector spare parts No Manual cold on-column injector head Seal, PTFE Clip Needle guide (manual injections) OC base Vespel ferrule for 0.25 mm ID column Vespel ferrule for 0.32 mm ID column Vespel ferrule for 0.53 mm ID column Backwasher/cooling sleeve for OC Column retaining nut and backwasher for OC Cooling fan 115 V Cooling fan 230 V Solenoid valve, secondary cooling HOT OC kit Spare Parts Catalog

23 Chapter 7 Cold On-Column Injector Spare Parts Catalog 23

24 8 Purged Packed Column Injector Table 8-1. Purged Packed Column Injector spare parts No 1 Septum cap Septum cap for TriPlus HS Septum Septum support A Liner, wide bore 2 mm B Liner, wide bore 4 mm Liner seal Adapter for wide bore columns Adapter retaining nut Graphite ferrule for 0.53 mm ID column Fixing nut for capillary column Blanking disk for leak test PPKD Heating Block (without heater element and sensor) Heater 115 V Heater 230 V Temperature sensor Kit for capillary columns on packed injector Please refer to Packed Column Injector (on page 26) for parts relevant to the use of this injector with packed columns. 24 Spare Parts Catalog

25 Chapter 8 Purged Packed Column Injector Spare Parts Catalog 25

26 9 Packed Column Injector Table 9-1. Packed Column Injector spare parts No 1 Septum cap Septum cap for TriPlus HS Septum Septum support Brass ferrule 6 mm OD metal column Retaining nut for 6 mm OD column Retaining nut for 6 mm OD column and ferrule Adapters for packed columns See Chapter 19 8 Brass front/back ferrule for 1/8 OD metal column Retaining nut for 1/8 mm OD column and ferrule O-ring, Viton for 6 mm OD glass column PTFE ferrule for 6 mm OD glass column Stainless steel washer Knurled nut Nut, o-ring and washer kit for 6 mm OD glass column Nut, o-ring and washer kit for 6 mm OD glass column Stainless steel ferrule 1/4 OD metal column PKD Heating Block (without heater element and sensor) Heater 115 V Heater 230 V Temperature sensor Kit for capillary columns on packed injector Please refer to Purged Packed Column Injector (on page 24) for parts relevant to the use of this injector with wide bore (0.53 mm ID) columns. 26 Spare Parts Catalog

27 Chapter 9 Packed Column Injector 9 Spare Parts Catalog 27

28 10 Programmed Temperature Vaporizing Injector Table Programmed Temperature Vaporizing Injector spare parts No 1 Septum cap Septum cap to be used with TriPlus HS Septum holder Septum Septum support a Septum support for PTV 816 RP Liner cap a Liner cap for PTV 816 RP Liner seal A Silcosteel liner, 2 mm ID B Silcosteel liner, 1 mm ID C Glass liner, 2 mm ID D Deactivated glass liner, 1 mm ID E Silcosteel liner for simile On-column injections F Silcosteel liner for Large Volume Injections G Glass sintered deactivated liner for Large Volume Injections H Deactivated glass liner with baffles I Deactivated glass liner for split and splitless injections L 2 mm ID Glass Liner with silica wool M 2 mm ID Deactivated Glass Liner with 60 mm of silica wool Spacer PTV 816 (RP-2004) main body, including heater, thermocouple without filter Graphite ferrule for 0.25 mm ID column Graphite ferrule for 0.32 mm ID column Graphite ferrule for 0.53 mm ID column Fixing nut for column Spare Parts Catalog

29 Chapter 10 Programmed Temperature Vaporizing Injector Table Programmed Temperature Vaporizing Injector spare parts (Continued) Brass ferrule, 1.6 mm ID Brass ferrule, 2 mm ID Liner removing tool Screwdriver Ceramic washer a Clip for ceramic washer Viton O-ring for sintered liner Kalrez O-ring for sintered liner Sealing cup for PTV liner. To be used with or Blanking disk for leak test T-shaper connector (PTV backflush) Kit upgrade SVE Valve 230 V without electronic board Kit upgrade SVE Valve 130 V without electronic board Kit PTV-BKF (including the Tee holder and 1 Tee connector with ferrules and nuts) Kit Tee Holder for BKF (Tee holder including 1 Tee connector with ferrules and nuts) Assy Tee connector for BKF holder (including Tee connector with ferrules and nuts, clamp and screw) Tee connector Locking nut M4 carved Graphite ferrule 0.8 mm ID Graphite ferrule 1.0 mm ID Deactivated uncoated precolumn, 2 m length; 0.5 mm ID Stainless Steel Tube 0.5 m length; 0.9 mm OD; 0.5 mm ID for Tee connector 24V/2-way Parker HT SVE valve for PTV Large Volume Solenoid valve heater 115V Solenoid valve heater 230V Solenoid valve Temperature sensor Cooling fan 115 V Cooling fan 230 V Spare Parts Catalog 29

30 Chapter 10 Programmed Temperature Vaporizing Injector 4a 14 14a 5a Injection Side A B C D E F G H I L M Column Side 30 Spare Parts Catalog

31 Chapter 10 Programmed Temperature Vaporizing Injector Spare Parts Catalog 31

32 11 Flame Ionization Detector (FID) Table Flame Ionization Detector spare parts No FID cell, complete FID collecting electrode Ceramic insulator Collecting electrode pin Retaining screw Flame ignition coil/polarization electrode assembly FID jet Jet removing tool Spring contact probe Add-on FID kit (cell, board, standard outfit) ECD-stacked FID kit (cell, board, standard outfit, pneumatics) Spare Parts Catalog

33 Chapter 11 Flame Ionization Detector (FID) 8 Spare Parts Catalog 33

34 12 Nitrogen Phosphorus Detector (NPD) Table Nitrogen Phosphorus Detector spare parts No NPD cell, complete NPD collecting electrode Ceramic insulator Collecting electrode pin Retaining screw TS-2 source (standard) TS-1 source for ENS mode NPD jet NPD (deactivated Silcosteel) jet Jet removing tool Add-on NPD kit (cell, board, standard outfit) ECD-stacked NPD kit (cell, board, standard outfit, pneumatics) Spare Parts Catalog

35 Chapter 12 Nitrogen Phosphorus Detector (NPD) Spare Parts Catalog 35

36 13 Electron Capture Detector (ECD) Table Electron Capture Detector spare parts No ECD cell, complete ECD cell, complete (USA version) Upper seal, aluminum ECD collecting electrode Temperature sensor / heater assembly ECD fixing tool Sleeve AL OD Lower seal, silver ECD blocking nut Temperature sensor/heater extension cable ECD simulator connector Add-on ECD kit (board, standard outfit) Adapter for stack configuration Nut 304 6MB Rubber holder Heating block for stack configuration (including heater and RTD) Cover for heating block Kit Carbon Filter for ECD Maintenance Kit Spare Parts Catalog

37 Chapter 13 Electron Capture Detector (ECD) Spare Parts Catalog 37

38 14 Flame Photometric Detector (FPD) Table Flame Photometric Detector spare parts No Assy FPD cell Mirror plug A Graphite seal 2 2B Heat shield 2 2C Maintenance kit for FPD Viton TM O-ring D Viton TM O-ring 1 2E Viton TM O-ring 1 3 Detector body Aluminium O-ring FPD jet FPD (deactivated Silcosteel) jet Flange and relevant Viton TM O-ring Interferential filter for phosphorus Interferential filter for sulphur Interferential filter for tin Filter Holder Photomultiplier Heater/sensor/coil cable FPD blocking nut FPD fixing tool FPD simulator connector Add-on FPD kit (cell, board, standard outfit) ECD-stacked FPD kit (cell, board, standard outfit, pneumatics) Fixing nut Spare Parts Catalog

39 Chapter 14 Flame Photometric Detector (FPD) Spare Parts Catalog 39

40 15 Photoionization Detector (PID) Table Photoionization Detector spare parts No PID cell, complete Detection cell assembly for PID Seal Seal Fixing tool Viton TM O-ring for lamp holder UV lamp 9.6 ev (including 2 Viton TM O-rings) UV lamp 10.6 ev (including 2 Viton TM O-rings) UV lamp 11.8 ev (including 2 Viton TM O-rings) Viton TM O-ring for UV lamp Silver seal Capillary adapter Jet and metal cell body Lamp polishing kit Add-on PID kit (cell, board, standard outfit) Spare Parts Catalog

41 Chapter 15 Photoionization Detector (PID) Spare Parts Catalog 41

42 16 Thermal Conductivity Detector (TCD) Table Thermal Conductivity Detector spare parts No 1 TCD cell, complete TCD cell with coated filament Heater and temperature sensor assembly for TCD cell Heater for TCD base 230 V Heater for TCD base 115 V Temperature sensor for TCD base Adapter for capillary columns (kit) Retaining nut for 6 mm OD metal column and ferrule Brass front/back ferrule for 1/8 OD metal column Retaining nut for 1/8 mm OD column and ferrule Knurled nut, O-ring and washer for 6 mm OD glass column Nut, ferrule and washer for 6 mm OD glass column Transfer heating base Inlet fitting base Please refer to Detector Base Bodies for further details on parts for column connection. 42 Spare Parts Catalog

43 Chapter 16 Thermal Conductivity Detector (TCD) Spare Parts Catalog 43

44 17 Discharge Pulsed Detector (PDD) Table Discharge Pulsed Detector spare parts No PDD detector cell PDD fixing tool Lower seal, silver PDD blocking nut PDD pulse module PDD fitting kit PDD He purifier 220 V power supply PDD He purifier 110 V power supply High voltage discharge cable Please refer to Detector Base Bodies for further details on parts for column connection. 44 Spare Parts Catalog

45 Chapter 17 Discharge Pulsed Detector (PDD) Spare Parts Catalog 45

46 18 Detectors Base Bodies Table Spare parts for Detectors Base Bodies No CB71 CAP CB70 PKD/WB Heating Block for CB Adapter for flow measurement Brass blind cap Silicon seal Blind jet Seal, silver Adapter for capillary column Graphite ferrule for 0.25 mm ID column Graphite ferrule for 0.32 mm ID column Graphite ferrule for 0.53 mm ID column Fixing nut for column Adapters for packed column on capillary column base body See Chapter 19 9 Brass ferrule 6 mm OD metal column Brass front/back ferrule for 1/8 OD metal column Retaining nut for 6 mm OD column Retaining nut for 6 mm OD column and ferrule Retaining nut for 1/8 OD column Viton o-ring for 6 mm OD glass column PTFE ferrule for 6 mm OD glass column Stainless steel washer Knurled nut Nut, o-ring and washer kit for 6 mm OD glass column Nut, o-ring and washer kit for 6 mm OD glass column Stainless steel ferrule 1/4 OD metal column Anti-turn fixing plate for capillary and packed injector base body Spare Parts Catalog

47 Chapter 18 Detectors Base Bodies Table Spare parts for Detectors Base Bodies (Continued) Nut, 1/4 for PKD detector base body Aluminium seal for PKD detector base body Nut, 1/8 for capillary detector base body Aluminium seal for capillary detector base body Wide bore kit for packed column detector base body Heater 115 V Heater 230 V Temperature sensor Spare Parts Catalog 47

48 19 Adapters for Packed Columns Table Spare parts for Adapters for Packed Columns No 1 Adapter for S/SL 6 mm and 1/4 columns Adapter for S/SL 1/8 columns Adapter for S/SL 1/16 columns Adapter cap for S/SL Adapter seal for S/SL Adapter PTFE ferrule Adapter for PKD/PPKD 6 mm and 1/4 columns Adapter for PKD/PPKD 1/8 columns Adapter for PKD/PPKD 1/16 columns Adapter for capillary base body 6 mm and 1/4 columns Adapter for packed base body 1/8 columns Adapter for packed base body 1/16 columns Adapter for packed base body 6 mm and 1/4 columns Adapter for capillary base body 1/8 columns Adapter for capillary base body 1/16 columns Adapter for TCD base body 6 mm and 1/4 columns Adapter for TCD base body 1/8 columns Adapter kit for packed columns on capillary injector and base body (includes items 1, 2, 8, 11, 13) Spare Parts Catalog

49 Chapter 19 Adapters for Packed Columns Spare Parts Catalog 49

50 Chapter 19 Adapters for Packed Columns Spare Parts Catalog

51 Chapter 19 Adapters for Packed Columns Spare Parts Catalog 51

52 Chapter 19 Adapters for Packed Columns 52 Spare Parts Catalog

53 Chapter 19 Adapters for Packed Columns Spare Parts Catalog 53

54 20 On-Column Large Sample Volume Injection Table Spare parts for On-Column Large Volume Injection No 1 T-shaped connector Fixing nut for column Vespel ferrule 0.9 mm hole (for connecting the T-piece to SVE) Graphite ferrule for 0.25 mm ID column Graphite ferrule for 0.32 mm ID column Graphite ferrule for 0.53 mm ID column Temperature sensor Solenoid valve HT for solvent vapor exit with connector (without heater) Heater 115 V, solvent vapor exit valve Heater 230 V, solvent vapor exit valve Restrictor for solvent vapor exit valve, 25 cm x 25 m ID Disposable filter for solvent vapor exit bottle UNCORET column, 15 m, 3 m coated with SE-54, 0.25 m f.t UNCORET column, 15 m, 3 m coated with SE-54, 0.45 m f t Syringe for LVI, 250 µl, with set of 6 x 80 mm needles Needle for syringe PN Syringe for LVI, 250 l (0.47/80/cone) removable needle Needle for syringe PN Membrane UNISET - compatible with vials P/N Membrane UNISET - compatible with vials P/N P/N and P/N Spare Parts Catalog

55 Chapter 20 On-Column Large Sample Volume Injection Spare Parts Catalog 55

56 Chapter 20 On-Column Large Sample Volume Injection 56 Spare Parts Catalog

57 Chapter 20 On-Column Large Sample Volume Injection Spare Parts Catalog 57

58 21 Automatic Gas Sampling Valve Table Spare parts for Automatic Gas Sampling Valve No 1 Loop 250 l Loop 500 l Loop 1 ml Loop 5 ml Spare Parts Catalog

59 Chapter 21 Automatic Gas Sampling Valve 1 Spare Parts Catalog 59

60 22 Miscellanea Table Oven spare parts Heater with diaphragm and temperature sensor (230 V) Heater with diaphragm and temperature sensor (115 V) Oven temperature sensor Replacement oven blower motor with bracket Stepping motor for flapper Door switch assembly Column support Oven Fan Hydrogen sensor Table Cables Generic start/stop cable (integrator) Autosampler start/stop cable RS232 cable for TRACE/PC communication, 2.5 m RS232 cable for TRACE/Autosampler communication, 1.5 m Analog cable for detector connection to integrator Connector, 4 positions, for cable Loop-back for multi-run Power cable 16A; 250 Vac Power cable 20A; 125 Vac Door switch cable assembly Spare Parts Catalog

61 Chapter 22 Miscellanea Table Fans Rear fan 115 V Rear fan 230 V Table Cryo Spare Parts Solenoid valve assembly for CO 2 Oven cryo option (External Cryo Module) Solenoid valve assembly for N 2 Oven cryo option (External Cryo Module) Solenoid valve [A2012-S 83A-24/60] assembly for CO 2 Oven cryo option (Cryo Control pcb) Solenoid valve [A2016-S /60] assembly for N 2 Oven cryo option (Cryo Control pcb) Solenoid valve [A2012-S 83A-24/60] assembly for CO 2 PTV cryo option (Cryo Control pcb) Solenoid valve [A2016-S /60] assembly for N 2 PTV cryo option (Cryo Control pcb) Tube for CO Tube for N Table Test mixtures Test mix for FID Test mix for FID with LVSL injector Test mix for UFM Test mix for NPD/FPD/PID Test mix for ECD Test mix for TCD Test mix for PDD (1 ml ampoule of C12, C14, C16 in quantity of 1 g/ml each) Column (TR-5, 7 m x 0.32 mm) for GC test Spare Parts Catalog 61

62 Chapter 22 Miscellanea Table Syringes Syringe 10 µl, 50 mm needle for packed and split injection Syringe 10 µl, 70 mm needle for splitless injection Syringe 10 µl, 75 mm needle for manual OC injection Table Merlin Microseal High Pressure Valve Option Spare Parts Microseal Valve for SSL and PTV inlets systems Syringe 10 µl, 50 mm needle for injections in SSL inlet - split mode Syringe 10 µl, 80 mm needle for injections in SSL inlet - splitless mode Syringe 100 µl for Large Volume injections in PTV inlet Syringe 250 µl for Large Volume injections in PTV inlet Merlin septum cap for the PTV injector P/N Merlin Vespel Seal Merlin Vespel Seal (set of 5) Table PTV Backflush Option Spare Parts Solenoid valve assembly Graphite ferrule 0.8 mm ID Graphite ferrule 1 mm ID T-shaper connector Table Large Volume Solvent Waste bottle assy Table Insulation Cassettes Insulation Bottom cassette Insulation Top cassette Spare Parts Catalog

63 Chapter 22 Miscellanea Table Nuts and Ferrules Nut 6MB Aluminium ferrule, 1.6 mm ID Aluminium ferrule, 2 mm ID Stainless steel ferrule, 1.6 mm ID Brass ferrule, 1.6 mm ID Brass ferrule, 2 mm ID Table Tools Flow meter: Thermo Scientific GFM Pro Flowmeter Leak detector: Thermo Scientific GLD Pro Table SSL Purge & Trap Adapter Purge & Trap Adapter P&T Silcosteel SSL Septum Cap for Large Volume Splitless Injector Septa BTO 9 mm OD for Large Volume Splitless Injector Septum Holder for Large Volume Splitless Injector Spare Parts Catalog 63

64 23 AI/AS 3000 & AI/AS 3000 II Autosamplers Table Tower Assy Complete tower assy for AI/AS Complete tower assy for AI/AS 3000 II Complete top cover assy AS 3000 M/S printing circuit boards assy AS 3000 II M/S printing circuit boards assy Slide stepping motor for AI/AS Slide stepping motor for AI/AS 3000 II Flat Cable H-FLEX 26F/16F+10F (FC1389) for AI/AS Flat Cable H-FLEX 26F/16F+10F (FC1526) for AI/AS 3000 II Elastic for injection head Front door AI Front door AS Front door AI 3000 II Front door AS 3000 II L syringe (Standard) µl, 50 mm needle syringe for microvolumes S/SL injector L syringe (for Merlin Microseal Valve) L syringe for nano-volumes injections Table Base Assy (Sheet 1 of 2) Complete Base assy for AI/AS Complete Base assy for AI/AS 3000 II Waste bottle complete with septum and cap (Set of 5) Tray 8-position assy Tray 105-position assy Tray 105-position with holder Spare Parts Catalog

65 Chapter 23 AI/AS 3000 & AI/AS 3000 II Autosamplers Table Base Assy (Sheet 2 of 2) Power supply Vac/24Vdc Round cable H-FLEX 34-pin (FC1377) for AI/AS Round cable H-FLEX 34-pin (FC1524) for A/AS 3000 II Table Vials and Septa 2 ml screw top vials, set of (require screw top cap with septa PN ) 2 ml screw top vials plus screw-top caps with septa. (Thermo Scientific brand combination of vials P/N and caps/septa P/N ) 2 ml Crimp-top vials, 11 mm finish, set of (require 11 mm aluminum caps and seals P/N ) 4 ml screw top solvent vials, set of (require screw top cap with septa P/N ) 300 L micro-volume sampling vials, set of (require screw top cap with septa P/N ) Screw top caps 2 ml, 4 ml and 300 L vials complete with septa, set of mm aluminum caps, with teflon faced septa, set of Septa for Waste bottle, set of Screw caps for Waste bottle, set of Table Cables RS232 cable (9-pin) GC - AI/AS 3000 and AI/AS 3000 II cable (6-pin) Power cable 10A/250V Power cable 10A/125V Table Alignment Brackets with Centering Plate Centering Plate for S/SL injector Centering Plate for Merlin Adapter on S/SL injector Centering Plate for PTV injector and Merlin Adapter on PTV injector Spare Parts Catalog 65

66 Chapter 23 AI/AS 3000 & AI/AS 3000 II Autosamplers Table Autosampler Brackets Bracket for mounting AI/AS 3000 and AI/AS 3000 II on right side Bracket for mounting AI/AS 3000 and AI/AS 3000 II on left side Table Upgrade kits Kit Merlin Microseal Valve for AI/AS 3000 and AI/AS 3000 II (requires P/N ) AS 3000 Upgrade kit for AI 3000 II Nano-volumes kit for S/SL inlet system (includes 0.5 l syringe P/N and the double gooseneck liner P/N ) Kit AS 3000 II Gemini Spare Parts Catalog

67 Chapter 23 AI/AS 3000 & AI/AS 3000 II Autosamplers Spare Parts Catalog 67

68 24 TriPlus Autosampler Consumables and Accessories Table Sample Vials Adapters for 1 ml Crimp-top vials; set of Adapters for 1 ml Crimp-top vials; set of ml Crimp-top vials, 8 mm finish; set of (require 8 mm aluminum caps and seals P/N ; compatible also with LVI enhanced performance seals P/N ) 2 ml Screw-top vials, 8 mm finish, set of (require 8 mm plastic screw-top caps P/N and teflon faced seals P/N ; compatible also with LVI enhanced performance seals P/N ) 2 ml Crimp-top vials, 11 mm finish, set of (require 11 mm aluminum caps and seals P/N ) 2 ml screw top vials plus screw-top caps with septa. (Thermo Scientific brand combination of vials P/N and caps/septa P/N ) 2 ml Screw-top vials, set of (require screw-top caps with septa P/N ) 300 L micro-volume sampling vials, set of (require screw top cap with septa PN ) 2.5 ml Crimp-top vials, 11 mm finish, set of (require 11 mm aluminum caps and seals P/N ; compatible also with ring shaped silicon septa with Teflon membrane for LVI P/N , set of 100) 8 mm aluminum caps with teflon faced septa, set of mm plastic screw-top caps, set of mm teflon faced seals set of Spare Parts Catalog

69 Chapter 24 TriPlus Autosampler Table Sample Vials (Continued) Screw-top caps for 2 ml vials P/N complete with septa, set of mm aluminum caps, with teflon faced septa, set of LVI enhanced performance seals for crimp-top vials P/N and P/N , with 11 mm aluminium caps, set of 100 LVI enhanced performance seals for vials P/N and P/N , set of 100 LVI enhanced performance seals for vials P/N and P/N with 8mm screw-top caps, set of ml Crimp-top vials, 20 mm finish, set of (require 20 mm aluminum caps and seals and spacers only for the HS oven) 20 ml Crimp-top vials, 20 mm finish, set of (require 20 mm aluminum caps and seals) 20 mm aluminum crimp-top caps with buthyl rubber seals, set of Suitable for low temperatures applications 20 mm aluminium crimp-top caps with teflon-coated buthyl rubber seals, set of 100. Suitable for temperature up to 100 C. 20 mm aluminium crimp-top caps with high performance septa, set of Suitable for high temperature applications or when multiple samplings are performed from the same vials. 20 mm snap caps and teflon faced septa for liquid applications, set of mm teflon faced septa for liquid applications, set of mm ring shaped silicon septa, and 20mm crimp-top aluminum caps, (set of 100) suitable for LVI liquid applications Stainless steel spacers for 10 ml vials, set of (used only in the HS oven). Accessories Hand crimper for 8 mm vials Hand crimper for 11 mm vials Spare Parts Catalog 69

70 Chapter 24 TriPlus Autosampler Table Sample Vials (Continued) Hand crimper for 20 mm vials Decapping tool for septum removal from glass vials Magnetic caps for Bar Code Reader, assembled with 9 mm caps and septa, set of 100 Labels for bar code reading, set of Table Washing Station Vials 10 ml Crimp-top washing solvent vials, complete of 20 mm snap-cap seals and teflon faced septa, set of ml washing solvent bottle ml Crimp-top waste vial with 2m long drain tube and fittings mm snap caps with teflon faced septa, set of mm ring shaped silicon septa with 20 mm crimp-top aluminum caps, set of Table Syringe Holders TriPlus AS Syringe holder for 50 mm needle length for 5, 10, L syringes Syringe holder for 50 mm needle length for 0.5, 10, L syringes Syringe holder for 80 mm needle length for 5, 10, L syringes Syringe holder for 80 mm needle length for 0.5, 10, L syringes TriPlus HS Syringe holder TriPlus SPME SPME fiber holder SPME syringe adapter Spare Parts Catalog

71 Chapter 24 TriPlus Autosampler TriPlus AS Table Syringes and needles 5 L syringe (0.47/50/cone) fixed needle, suitable for Split injections L syringe (0.5/50/cone) fixed needle, suitable for Split injections L syringe (0.47/80/cone) fixed needle, suitable for Splitless and OC injections 10 L syringe (0.63/50/cone) suitable for Merlin valve, suitable for Split injections 10 L syringe (0.63/80/cone) suitable for Merlin valve, suitable for Splitless injections 10 L syringe (dual gauge: /50/cone) suitable for PTV-simil OC with Merlin Valve 100 L syringe (0.63/50/side hole) removable needle, suitable for PTV-LVI 250 L syringe (0.63/50/side hole) removable needle, suitable for PTV-LVI L syringe (0.63/50/cone) removable needle, suitable for LV-SL L syringe (0.47/80/cone) removable needle, suitable for OC-LVI Set of 2 needles (0.63/50/side hole) suitable for PTV-LVI Set of 5 needles (0.47/80/cone) suitable for OC-LVI Set of 5 needles (0.63/50/cone) suitable for LV-SL TriPlus HS Gas tight syringe 1.0 ml capacity, without plunger (0.72/80/side hole) Gas tight syringe 2.5 ml capacity, without plunger (0.72/80/side hole) Gas tight syringe 5.0 ml capacity, without plunger (0.72/80/side hole) Gas tight syringe 2.5 ml capacity, without plunger (0.64/80/side hole), suitable for Merlin valve Gas tight syringe 1.0 ml capacity, complete with plunger and adapter Gas tight syringe 2.5 ml capacity, complete with plunger and adapter Gas tight syringe 5.0 ml capacity, complete with plunger and adapter Spare Parts Catalog 71

72 Chapter 24 TriPlus Autosampler Table Syringes and needles (Continued) PTFE seal for plunger of 1.0 ml syringe PTFE seal for plunger of 2.5 ml syringe PTFE seal for plunger of 5.0 ml syringe Table Trays Tray holder, configurable in field as Primary or Secondary Primary Tray, positions 1-150, for 1, 2, 2.5 ml vials Primary Tray, positions 1-54, for 10, 20 ml vials Secondary Tray, positions , for 1, 2, 2.5 ml vials Secondary Tray, positions , for 10, 20 ml vials Cooled/heated tray holder Primary cooled/heated tray 1-96 positions Primary cooled/heated tray 1-33 positions Secondary cooled/heated tray positions Secondary cooled/heated tray positions Spare Parts Table Print Circuit Boards MFS_XY motor driver board MFS_XY 1200 motor driver board MFS_ZP ASSY motor driver board MFS_ZP HS motor driver board MFS_TC temperature controller board MFS_SY syringe identification MFS_CP main CPU board Spare Parts Catalog

73 Chapter 24 TriPlus Autosampler Table Print Circuit Boards (Continued) MFS_FN incubation oven and stirrer board MFS_HS hs syringe board MFS_PI power interface board MFS_EI external interface board MFS_TI tray identifier board MFS_CR bar code reader board MFS_TR tray reader board 1 MFS_TR W.A. programmed for Washing Station 4 solvents MFS_TR W.B. programmed for Washing Station 2 solvents MFS_TR TRAY programmed for Tray Holders MFS_OC on-column presence board MFS_OD on-column driver board 1 MFS_OD ACT A programmed for Actuator A MFS_OD ACT B programmed for Actuator B Table Fuses 2A time-lag IEC127/III (5 x 20 mm) for 230 V ac power supply A time-lag IEC127/III (5 x 20 mm) for 115 V ac power supply Table Assembled Parts Truck motor assy XY crossrails assy XY extended crossrail assy Turret AS assy Turret HS assy External power module Spare Parts Catalog 73

74 Chapter 24 TriPlus Autosampler Table Assembled Parts (Continued) External power module + LAN Incubation Oven/Agitator Pressure regulator modulator (it is a part of P/N ) Assy front door for TriPlus AS Assy front door for TriPlus HS Heated Syringe Holder for TriPlus HS Fast Washing Station solvents Washing Station solvents Washing Station Table Cables Autosampler 9M/F cable pin M-DIN M/M cable Table Miscellanea 2-m Black plastic tube Spring injection head AS Spring injection head HS Crossrail Y - Guide pin with washer Crossrail Y - Plate assy for Z axis connection Label for Y axis Spare Parts Catalog

75 Chapter 24 TriPlus Autosampler Table Miscellanea (Continued) Needle Guide assembly for 50 mm and 80 mm syringe needle (AS) Screwdriver for 3-mm Allen screw Phillips screwdriver Table Installation Kits Kit External Tube (for TriPlus HS) OC actuator TriPlus HS Table TriPlus for HS Spare Parts Septum cap for S/SL suitable for HS and SPME Septum cap for PTV suitable for HS and SPME Septum cap for Merlin Valve - S/SL-PTV TriPlus for SPME Table TriPlus for SPME Spare Parts Liners 0.8 mm ID for S/SL (Set of 5) Liners 1 mm ID for PTV (Set of 2) Septum cap for S/SL suitable for HS and SPME Spare Parts Catalog 75

76 Chapter 24 TriPlus Autosampler Table TriPlus for SPME Spare Parts Septum cap for PTV suitable for HS and SPME Septum cap for Merlin Valve - S/SL-PTV Spare Parts Catalog

77 Chapter 24 TriPlus Autosampler Spare Parts Catalog 77

78 25 TriPlus RSH Autosampler Consumables and Accessories Table Kits Headspace upgrade Kit 1 1R Preventive Maintenance Kit 1 1R Gas Tube Replacement kit 1 1R Complete Z-Head for Direct Exchange 1 1R Kit motor assy for X-axis 1 1R Kit motor assy for Y-axis 1 1R Kit motor assy for Z-axis 1 1R Kit motor assy for Needle Guide 1 1R Kit motor assy for Syringe Plunger 1 1R Kit motor assy for Agitator 1R Kit motor assy for Vortexer 1 1R CPU Board 1 1R Security Key 1 1R Electronic Mainboard Kit 1 1R Electronic Board Kit of the Z-Head 1 1R Electronic Board Kit of the Agitator 1 1R Electronic Board Kit of the ATC Station 1 1R Electronic Board Kit of the Cooled Stack 1 1R Main Power Supply 1 1R Spare Parts Catalog

79 Chapter 25 TriPlus RSH Autosampler Spare Parts Catalog 79

80 26 Valve Oven Table Valve Oven Spare Parts Heather flexible Temperature sensor Valve oven assy PCB Solenoid valve SMC 24 Vcc Portable power supply 24V 45W Table Pneumatic Valves Spare Parts Pneumatically actuated, 4-ports valve (Valco Valve, UWP type, 175 C max, for 1/16 fittings) Pneumatically actuated, 6-ports valve (Valco Valve, UWP type, 175 C max, for 1/16 fittings) Pneumatically actuated, 8-ports valve (Valco Valve, UWP type, 175 C max, for 1/16 fittings) Pneumatically actuated, 10-ports valve (Valco Valve, UWP type, 175 C max, for 1/16 fittings) Pneumatically actuated, 4-ports liquid valve (Valco Valve, W type, with 0.1 l internal sample loop, for 1/16 fittings) Adjustable restrictor Table Purged Gas Valves Spare Parts Pneumatically actuated, 6-ports purged valve, installed and unplumbed (Valco Valve, UWE-PH type, 175 C max, for 1/16 fittings) Pneumatically actuated, 8-ports purged valve, installed and unplumbed (Valco Valve, UWE-PH type, 175 C max, for 1/16 fittings) Spare Parts Catalog