Formed Sampling Cylinders and Accessories Index amp ling cylinde HOKE Inc.

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1 Formed Sampling Cylinders and Accessories Index Sampling Cylinders 2 Design, Features, Applications Cylinder Accessories 3 Collars, Flanges, Caps, Carrying Handles Safety Relief Devices Cylinder Valves 1700 Series Series Series /3800 Series 10 How to Collect Samples 12 HOKE Inc. PO Box 4866 Spartanburg, SC Phone (864) Fax (864) Sales-hoke@circor.com sampling cylinders

2 Formed Sampling Cylinders & Accessories HOKE Sampling Cylinders are designed and manufactured to stringent U.S. Department of Transportation (DOT) specifications to provide long performance life and maximum safety to the user. These cylinders are fabricated from seamless tubing or pipe with increased wall thickness in the threaded area, which prevents expansion when valves are installed. Completely formed ends maximize strength and eliminate potential leak paths. Internal sandblasting removes surface imperfections and removes foreign particles. Single- and double-ended cylinders are available as standard in a variety of capacities from 10 milliliters to 4 gallons. Typical Applications Sampling hydrocarbons in refineries and petrochemical plants Grab sampling for chromatographic analysis Snubbers in reactor feed lines Surge accumulators in High Pressure Gas Systems High Vacuum Systems as experimental chambers and molecular sieves Chemical reaction vessels HOKE Inc. PO Box 4866 Spartanburg, SC Phone (864) Fax (864) Sales-hoke@circor.com Features & Benefits Choice of 12 different capacities from 10 ml through 4 gallons. Cylinder ends come in 1/8, 1/4, 3/8 and 1/2 NPT female connections (depends on capacity). Standard cylinders are formed from seamless drawn 304 SS, 316 SS or Monel pipe or tubing. Precision spinning operation eliminates internal pockets and provides easy flow of the sample. All models are internally sandblasted to remove surface imperfections and eliminate foreign particles. Single- and double-ended cylinders in most capacities are available as standard. Rugged wall thickness extra strength around threads. Cylinders may be ordered with valves, relief devices, dip tubes, carrying handles, collar and flanges and end caps. The interior of HOKE cylinders are available with a special FEP lining which provides excellent lubricity and very low permeability. To order, add TL following the cylinder part number. Restek, Silcosteel, and Sulfinert surface treatments available for many sizes. Consult factory. Special High Tolerance NPT Thread formed sampling cylinders

3 Formed Sampling Cylinders C A Female NPT C DOUBLE-ENDED CYLINDER B SINGLE-ENDED CYLINDER A Female NPT FOR YOUR SAFETY IT IS SOLELY THE RESPONSIBILITY OF THE SYSTEM DESIGNER AND USER TO SELECT PRODUCTS SUITABLE FOR THEIR SPECIFIC APPLICATION REQUIREMENTS AND TO ENSURE PROPER INSTALLATION, OPERATION AND MAINTENANCE OF THESE PRODUCTS. MATERIAL COMPATIBILITY, PRODUCT RATINGS AND APPLICATION DETAILS SHOULD BE CONSIDERED IN THE SELECTION. IMPROPER SELECTION OR USE OF PRODUCTS DESCRIBED HEREIN CAN CAUSE PERSONAL INJURY OR PROPERTY DAMAGE. Formed Cylinders: 316 Stainless Steel only Pressure ratings up to 5000 psig can be supplied as a special. Consult the factory for quotation of any cylinder rated above 1800 psig. When testing to ASME specifications is required, contact HOKE for quotation and specify maximum pressure and temperature To learn more about DOT-rated Cylinders, please read HOKE Spun Sampling Cylinders catalog, Part # Other Materials Cylinders manufactured from other materials are available. Contact HOKE for quotation. Dimensions & How to Order Pressure Rating Internal Volume psig [bar] A inch 2 Formed Sampling Cylinders & Accessories PTFE-lined Cylinders The interior of HOKE cylinders are available with a special FEP lining which provides excellent lubricity and very low permeability. To order add PTFE-lined following the cylinder part number. How to Order To order a HOKE Sampling Cylinder, specify the model number based on capacity required, single- or double-end connections and end connection size. Ordering Numbers Dimensions inch [mm] Weight lb (kg) Single Ended Double Ended Length B Outside Diameter C 304 Stainless Steel, 400 psig [28 bar] 400 [28] 1000 ml 1/2 * 8LD [627] 3.5 [89] 4.5 [2.0] 2250 ml 1/2 * 8LD [387] 4.0 [102] 7.0 [3.0] 3000 ml 1/2 * 8LD [489] 4.0 [104] 8.4 [3.8] 1 gal. 1/2 * 8LD1G [603] 4.0 [104] [4.6] 304 Stainless Steel, 1800 psig [124 bar] [124] 75 ml 1/4 4HS75 4HD75 5 [127] 1.5 [38] 0.75 [0.33] 75 ml 3/8 6HS75 6HD75 5 [127] 1.5 [38] 0.75 [0.33] 150 ml 1/4 4HS150 4HD150 9 [229] 1.5 [38] [0.61] 150 ml 3/8 6HS150 6HD150 9 [229] 1.5 [38] [0.61] 300 ml 1/4 4HS300 4HD [248] 2.0 [51] 2.0 [0.9] 300 ml 3/8 6HS300 6HD [248] 2.0 [51] 2.0 [0.9] 500 ml 1/4 4HS500 4HD [368] 2.0 [51] 3.0 [1.4] 500 ml 3/8 6HS500 6HD [368] 2.0 [51] 3.0 [1.4] 1000 ml 1/2 8HS1000 8HD [279] 3.5 [89] 7.25 [3.3] 2250 ml 1/2 8HS2250 8HD [432] 4.0 [102] 13.4 [6.0] 3000 ml 1/2 8HS3000 8HD [559] 4.0 [102] [7.6] 1 gal. 1/2 8HS1G 8HD1G [679] 4.0 [102] 20.6 [9.3] 2.5 gal. 1/2 8HD21/2G 24.5 [622] [168] [19.9] 4 gal. 1/2 8HD4G 36 [914] [168] 61.5 [28] 316 Stainless Steel, 1800 psig [124 bar] [124] 10 ml 1/8 2HSY10 2HDY10 4 [102] [16] [0.06] 30 ml 1/4 4HSY30 4HDY [121] 1.0 [25] 0.44 [0.20] 75 ml 1/4 4HDY [121] 1.5 [38] 0.75 [0.34] 150 ml 1/4 4HDY150 9 [229] 1.5 [38] 1.4 [0.6] 300 ml 1/4 4HDY [241] 2.0 [51] 2.0 [0.9] 500 ml 1/4 4HDY [368] 2.0 [51] 2.9 [1.3] Monel ** 5000 [345] 95 ml 1/4 4HSM95 4HDM [133] 121/32 [42] 1.5 [0.7] 150 ml 1/4 4HSM150 4HDM [165] 129/32 [48] 2.4 [1.0] 300 ml 1/4 4HSM300 4HDM [298] 129/32 [48] 4.0 [1.8] 500 ml 1/4 4HSM500 4HDM [495] 129/32 [48] 6.13 [2.8] 3500 [241] 1000 ml 1/4 4HSM1000 4HDM [292] 3.5 [89] 11.4 [5.0] * For single-ended applications, order double-ended cylinder with plug part number 502B. ** Standard models are non-dot rated

4 Cylinders Accessories & Valves Collars, Flanges, Caps, Carrying Handles To enable the user to safely transport pressurized samples, HOKE offers a variety of collar and flange assemblies, protective end caps and carrying handles. Collars can only be assembled at the HOKE factory. Other accessories can come completely assembled to a cylinder or may be ordered for field installation. To order, specify the cylinder part number followed by the part number of the accessory. Carrying Handles, Valve Protection End Caps Order by Catalog Part Number Cylinder Number Dimensions Collar & Flange Assy. # End Cap Part # Carrying Handle Kit Part # High Pressure Low Pressure A Outside Diameter B HD300 6HD300 4HD500 4HD300 6HD300 4HD HD500 6HD HD1000 8HD HD2250 8HD HD3000 8HD HD1G 8HD1G HD21/2GF HD4GF HDM HDM HDM500 2 in 51 mm 2 in 51mm 31/2 in 89mm 4 in 102mm 4 in 102 mm 4 in 102 mm 8 in 203 mm 129/32 in 48 mm 129/32 in 48 mm 129/32 in 48 mm All angle pattern valves shown in this catalog can be used with protective end caps. The globe pattern valves 3752M4Y2 shown on page 10 are the only globe pattern valves which can be used with protective end caps. Dip Tubes Dip tubes provide a vapor space of the specified volume in cylinders containing liquefied gases, allowing the liquid to expand as the temperature increases. Without adequate vapor space, a small temperature increase can cause the liquid to expand, increasing the pressure dramatically. Refer to local regulations and other appropriate guidelines for safe cylinder filling limits for your application. Dip tubes may be ordered in outages of 10, 20 and 30% to provide a respective filled capacity of 90, 80 or 70%. A 30% outage tube would dip into a cylinder to a point equivalent to the liquid level of a cylinder filled to 70% of its capacity. Dip tubes in other outages can also be ordered, contact the factory. To ensure leak-tight performance, dip tubes must be properly welded to a fitting, valve, or relief device. When ordering dip tubes on valves without cylinders, the cylinder model number or capacity must be identified. Typical Dip Tube Installation Formed Sampling Cylinders & Accessories 3

5 Cylinder Accessories & Valves Safety Relief Devices Saf-tee relief devices can be used with HOKE sampling cylinders as an inexpensive safety device or as a pipe size adapter for connecting valves in the make-up of cylinder assemblies. Two basic models are available to satisfy most pressure ranges. Spring relief models are recommended for applications where re-closure is required. Rupture Disc models are supplied with a pre-bulged rupture disc which provides excellent resistance to a broad range of hold-down plug and rupture disc to prevent damage due to torque transmission during assembly. A safety screen minimizes fragment release through the plug vents. The maximum operating system pressure should be limited to 80% of the nominal rating of the rupture disc for static operating pressure and ambient temperature. It should be limited to 70% if pressure pulsations occur or used at elevated temperature. The burst tolerance is within the ASME code guidelines. Technical Data Operating Temperature Range: 20 F to +250 F ( 29 C to +121 C) L4Y Forged Body Style with Rupture Disc Materials of Construction Key Description Rupture Disc Models Spring Relief Models 1 Body 316SS 316SS 2 Gasket PCTFE PCTFE 3 Safety Screen 316SS 4 Slip Ring 316SS 5 Rupture Disc Inconel 6 Seat Holder 303SS 303SS 7 Seat Ring 316SS 316SS 8 Seat Viton Viton 9 Spring 18-8SS 6712L4Y Rupture Disc Models Inlet Outlet NPT Male NPT Female Order by Number Add Code Letter Replacement Rupture Disc Kit 1/4 1/4 6712L4Y D psi SP6712K1 3/8 1/4 6712L6 4Y G psi SP6712K 2 E* psi SP6712K 3 F psi SP6712K4** H psi SP6712K 5** * Normally supplied with DOT 3E-1800 and DOT 3A-1800 ** Special order only. Please contact HOKE for details. Rupture Disc Kits Replacement rupture disc kits include rupture disc, safety screen, slip ring, gasket and instruction sheet. Spring Relief Models Inlet NPT Male Outlet NPT Female Order by Number Add Code Letter 1/4 1/4 6711L4Y C psi 3/8 1/4 6711L6 4Y D* psi FOR YOUR SAFETY L64Y Forged Body Style with Spring Relief 4 Formed Sampling Cylinders & Accessories Ordering Instructions 1. Determine whether the relief range you require is served by a spring relief or a rupture disc model. 2. Order by part number, followed by code of the desired range. For example: No. 6712L4Y. 3. Replacement rupture disc kits may be ordered by part number shown in the rupture disc model chart. IT IS SOLELY THE RESPONSIBILITY OF THE SYSTEM DESIGNER AND USER TO SELECT PRODUCTS SUITABLE FOR THEIR SPECIFIC APPLICATION REQUIREMENTS AND TO ENSURE PROPER INSTALLATION, OPERATION AND MAINTENANCE OF THESE PRODUCTS. MATERIAL COMPATIBILITY, PRODUCT RATINGS AND APPLICATION DETAILS SHOULD BE CONSIDERED IN THE SELECTION. IMPROPER SELECTION OR USE OF PRODUCTS DESCRIBED HEREIN CAN CAUSE PERSONAL INJURY OR PROPERTY DAMAGE.

6 Cylinder Valves 1700 Series Heavy Duty Cylinder Valves Heavy duty compact line of 316 stainless steel and Monel forged body globe pattern valves features an integral bonnet suitable for 1/4 and 3/8 NPT ended cylinders. Features Dyna-Pak packing provides a leak-tight seal with low operating torque Packing below stem threads prevents fluid from contacting threads Non-rotating hardened 17-4PH stainless steel or replaceable PCTFE stem tip prevents galling and extends valve life Hardened 450 stainless steel or Monel combination packing nut and thread gland for long stem thread cycle life Lock-nut secures packing nut, preventing accidental removal Flat wrench pads on body for easy valve installation Integral stem backstop for added safety 1711L4Y Technical Data Maximum Operating Pressure Temperature Range Orifice Size Cv Factor psig [414 barg] 65 F to +450 F [ 54 C to +232 C] (metal stem tip) 20 F to +250 F [ 29 C to +121 C] (PCTFE stem tip) Materials of Constructions Description 316SS Valves Monel Valves Body 316SS Monel Stem 316SS Monel Stem Tip Soft PCTFE PCTFE Hard 17-4 PHSS Monel Dyna-Pak Packing TFE/316SS Wafers TFE/Monel Wafers Handle Aluminum Aluminum 1711[ ] 1751[ ] Dimensions & How to Order 1700 Series Globe Pattern Valves Basic Material Stem tip End Connections Ordering Number Dimensions inch (mm) Inlet A Outlet B D E F H 316 SS Metal 1/4 NPT Male 1/4 NPT Male 1711M 4Y 3 (76) 23/16 (56) 21/8 (54) 7/ 16 (12) Metal 1/4 NPT Male 1/4 NPT Female 1711L4Y 3 (76) 21/8 (54) 21/8 (54) 7/ 16 (12) PCTFE 3/8 NPT Male 3/8 NPT Male 1751M6Y 3 (76) 23/16 (56) 17/8 (48) 7/ 16 (12) Monel Metal 1/4 NPT Male 1/4 NPT Male 1711M 4M 3 (76) 23/16 (56) 21/8 (54) 7/ 16 (12) PCTFE 1/4 NPT Male 1/4 NPT Male 1751M4M 3 (76) 23/16 (56) 23/16 (56) 7/ 16 (12) Dimensions are for reference only and are subject to change FOR YOUR SAFETY IT IS SOLELY THE RESPONSIBILITY OF THE SYSTEM DESIGNER AND USER TO SELECT PRODUCTS SUITABLE FOR THEIR SPECIFIC APPLICATION REQUIREMENTS AND TO ENSURE PROPER INSTALLATION, OPERATION AND MAINTENANCE OF THESE PRODUCTS. MATERIAL COMPATIBILITY, PRODUCT RATINGS AND APPLICATION DETAILS SHOULD BE CONSIDERED IN THE SELECTION. IMPROPER SELECTION OR USE OF PRODUCTS DESCRIBED HEREIN CAN CAUSE PERSONAL INJURY OR PROPERTY DAMAGE. Formed Sampling Cylinders & Accessories 5

7 Cylinder Valves 1900 Series Cylinder Valves This durable line of angle pattern valves features a low profile shrouded handle which protects the valve against damage. Dyna-Pak TFE wafer packing provides a leak tight seal with low operating torque even at 6000 psi (414 bar) pressure. Features 316SS or Monel construction Low profile aluminum shrouded stem handle protects stem against damage Dyna-Pak packing provides leak tight seal with low operating torque Packing below the stem threads prevents process fluid from contacting stem threads Non-rotating hardened 17-4PH stainless steel or replaceable PCTFE stem tip prevents galling and extends valve life Hardened 450 stainless steel combination packing nut and thread gland for long stem thread cycle life Integral stem backseat provides added safety and prevents accidental removal of stem Variety of end connections satisfy most cylinder valve applications Bonnet lock prevents accidental removal of threaded bonnet Angle flow pattern Lock-nut secures packing nut against accidental removal Flat wrench pads on body for easy valve installation Integral stem backstop for added safety 1935L64Y Technical Data Maximum Operating Pressure Operating Temperature Range 6000 psig (414 bar) Orifice Metal Stem Tip PCTFE Stem Tip Cv Factor Metal Stem Tip PCTFE Stem Tip F to +450 F [ 54 C to +232 C] (metal stem tip) 20 F to +250 F [ 29 C to +121 C] (PCTFE stem tip) Materials of Construction Description 316SS Valves Monel Valves Body 316SS Monel Stem 316SS Monel Stem Tip Soft PCTFE PCTFE Hard 17-4 PHSS Monel Packing (Dyna-Pak) TFE/316SS Wafers TFE/Monel Wafers Handle Aluminum Aluminum Handle Turns vs Cv Number of Turns of Valve Handle Metal Stem Tip (0.156 orifice) Cv Kel-F Stem Tip (0.187 orifice) Pressure Temperature Curve Operating Pressure PSIG BARG F C Temperature Formed Sampling Cylinders & Accessories

8 Cylinder Valves 1900 Series Cylinder Valves F F D D B B H A H A E E 1925L[ ]Y 1965L[ ] Dimensions & How to Order 1900 Series Angle Pattern Valves Basic Material Stem Tip End Connections Ordering Dimensions, in. [mm] Inlet A Outlet B Number D E F H Metal 1/4 NPT Male 1/4 NPT Female 1925L4Y 33/ 16 [81] 11/2 [38] 13/4 [44] 15/16 [33] 316 SS PCTFE 1/4 NPT Male 1/4 NPT Female 1965L4Y 33/ 16 [81] 11/2 [38] 13/4 [44] 15/16 [33] Metal 3/8 NGT Male* 1/4 NPT Female 1925L64Y 33/ 16 [81] 11/2 [38] 13/4 [44] 13/8 [35] PCTFE 3/8 NGT Male* 1/4 NPT Female 1965L64Y 33/ 16 [81] 11/2 [38] 13/4 [44] 13/8 [35] Monel PCTFE 1/4 NPT Male 1/4 NPT Female 1965L4M 33/ 16 [81] 11/2 [38] 13/4 [44] 15/16 [33] * NGT Male Ended Valves: Screw thread standard per Federal Services Handbook H-28, section 9. These threads allow longer thread engagement into the cylinder. Dimensions are for reference only and are subject to change FOR YOUR SAFETY IT IS SOLELY THE RESPONSIBILITY OF THE SYSTEM DESIGNER AND USER TO SELECT PRODUCTS SUITABLE FOR THEIR SPECIFIC APPLICATION REQUIREMENTS AND TO ENSURE PROPER INSTALLATION, OPERATION AND MAINTENANCE OF THESE PRODUCTS. MATERIAL COMPATIBILITY, PRODUCT RATINGS AND APPLICATION DETAILS SHOULD BE CONSIDERED IN THE SELECTION. IMPROPER SELECTION OR USE OF PRODUCTS DESCRIBED HEREIN CAN CAUSE PERSONAL INJURY OR PROPERTY DAMAGE. Formed Sampling Cylinders & Accessories 7

9 Cylinder Valves 2400 Series 1/2 Cylinder Valves 2400 Series 316 stainless steel, forged body angle pattern valves, come with a union bonnet for increased safety and ease of maintenance. Available with pressure rupture discs or spring relief devices as an integral part of the valve. Features Forged body union bonnet design for ease of maintenance and maximum reliability Non-rotating hardened 17-4PH stainless steel tip prevents galling and extends valve life Dyna-Pak packing below stem threads prevents lubricant washout & contamination of process fluids Stem backseat provides added safety Available with integral rupture disc or spring relief Technical Data Maximum Operating 5000 psig [345 barg] Pressure Temperature Range Metal stem tip: 40 F to +350 F ( 40 C to +177 C) TFE stem tip: 20 F to +250 F ( 29 C to +121 C) 2464L84Y with rupture disc All burst discs & spring relief devices: 20 F to +250 F ( 29 C to +121 C) Orifice Size Cv Factor 2.2 Materials of Constructions Body & Bonnet 316SS Stem 17-4PH Thread Gland 416SS Packing Nut 303SS Ring Gland 303SS 2466L84Y with spring relief 2462L84Y 8 Formed Sampling Cylinders & Accessories

10 Cylinder Valves Valves with Rupture Discs Order by Part Number PTFE Packing Inlet Outlet PTFE Stem Tip Metal Stem Tip Add Code Letter D psi G psi 1/2 1/4 NGT NPT 2464L84Y 2424L84Y E* Male Female psi F psi H psi * Normally supplied with DOT 3E-1800 and DOT 3A-1800 ** Special order only. Please contact HOKE factory. Rupture Disc Kits SP6712K1 SP6712K 2 SP6712K 3 SP6712K4** SP6712K 5** 2462L84Y 2422L84Y Valves without Relief Devices Order by Part Number PTFE Packing Inlet Outlet PTFE Stem Tip Metal Stem Tip 1/2 NGT Male 1/4 NPT Female 2462L84Y 2422L84Y 25 8 [67] 4½ Open [114] Valves with Spring Relief Devices Order by Part Number PTFE Packing Inlet Outlet PTFE Stem Tip Metal Stem Tip 1/2 NGT Male 1/4 NPT Female 2466L84Y 2426L84Y Add Code Letter C psi D* psi * Normally supplied with DOT Ordering Instructions for Valves with Relief Devices 1. Determine whether the relief range you require is served by a spring relief or a rupture disc model. 2. Order by part number, followed by code of the desired range. For example: No. 2424L84YD. ½ NGT 1¾ [44] ¼ FNPT 1¾ [45] 2424L84Y 2466L84Y Formed Sampling Cylinders & Accessories 9

11 Cylinder Valves 3700 & 3800 Series Cylinder Valves The 3700 & 3800 Series forged body cylinder valves are supplied in stainless steel for cylinders with 1/8 through 3/8 NPT threads. Features Compact size for restricted areas Dyna-Pak packing provides a leak-tight seal and low operating torque Integral bonnet design Ergonomic black ABS plastic handle Flat wrench pads on body for easy valve installation Replaceable PCTFE stem tip or integral metal stem tip Choice of 303 or 316 stainless steel construction Globe or angle flow patterns 3752M4Y[ ] Series are designed for use with cylinder protective caps and collars on 300 and 500 ml size cylinders. Low profile and extended end allows the valve and handwheel to clear the cap and cylinder collar Angle 3802L4Y Technical Data Maximum Operating Pressure: Temperature Range: 5000 psig (345 bar) 65 F to +450 F (metal stem tip) 20 F to +250 F (PCTFE stem tip) Orifice Sizes: 0.060, 0.170, Cv Factor: 0.07 to 0.55 Materials of Construction Description 303SS Valves 316SS Valves Body 303SS 316SS Stem 316SS 316SS Stem Tip (Softseat) PCTFE PCTFE Dyna-Pak Packing PTFE/316SS PTFE/316SS Handle* ABS ABS * 303 stainless steel metal handle is provided on models 3752M4Y[ ] Globe 3752M4Y1 Handle Turns vs. Cv Pressure-Temperature Curve Number of Turns of Valve Handle V Stem Point (0.060 orifice) Metal Stem Point (0.170 orifice) Cv Kel-F Stem Point (0.170 orifice) Operating Pressure PSIG bar F C Temperature Formed Sampling Cylinders & Accessories

12 Cylinder Valves 3700 & 3800 Series Cylinder Valves Angle 3862L64Y Dimenions & How to Order 3700 & 3800 Series Cylinder Valves Globe 3752M4Y1 Basic Material Cv Stem Tip End Connections Ordering Dimensions inch [mm] Number Inlet A Outlet B D E F H Globe Pattern Orifice Size SS 0.07 Metal V-stem 1/4 NPT Male 1/4 NPT Male 3732M4Y 23/16 [56] 13/4 [44] 17/16 [36] 25/64 [10] Globe Pattern Orifice Size SS SS 0.35 PCTFE 1/4 NPT Male 1/4 NPT Male 3752M4S 21/8 [54] 2 [51] 17/16 [36] 3/8 [10] PCTFE Globe Pattern Orifice Size /4 NPT Male 1/4 NPT Female 3852L4S 211/16 [68] 17/8 [48] 127/64 [36] 1/2 [13] Metal 1/4 NPT Male 1/4 GYROLOK 3712H4Y 21/8 [54] 17/8 [48] 17/16 [36] 3/8 [10] PCTFE 1/4 NPT Male 1/4 GYROLOK 3752H4Y 21/8 [54] 17/8 [48] 17/16 [36] 3/8 [10] Metal 1/4 NPT Male 1/4 NPT Male 3712M4Y 21/8 [54] 2 [51] 17/16 [36] 3/8 [10] PCTFE 1/4 NPT Male 1/4 NPT Male 3752M4Y 21/8 [54] 2 [51] 17/16 [36] 3/8 [10] PCTFE 1/4 NPT Male 1/4 NPT Male 3752M4Y2* 113/ 16 [46] 23/4 [70] 1 [25] PCTFE 3/8 NPT Male 3/8 NPT Male 3852M6Y 213/16 [71] 17/8 [48] 17/8 [48] 1/2 [13] PCTFE 1/2 NPT Male 1/4 NPT Male 3752M4Y1* 113/ 16 [46] 3 [76] 1 [25] 316 SS 0.55 Metal 3/8 NPT Male 3/8 NPT Male 3812M6Y 225/ 32 [71] 29/16 [65] 17/8 [48] 31/6 4 [12] Angle Pattern Orifice Size SS 0.5 Metal 1/4 NPT Male 1/4 GYROLOK 3722H4Y 21/8 [54] 119/ 32 [40] 17/16 [36] 7/8 [22] Metal PCTFE Metal PCTFE 1/4 NPT Male 1/4 NPT Male 3/8 NPT Male 3/8 NPT Male 1/4 NPT Female 1/4 NPT Female 1/4 NPT Female 1/4 NPT Female * Models 3752M4Y[ ] are designed for use with cylinder protective caps and collars on 300 and 500 ml. cylinders. Dimensions are for reference only and are subject to change 3802L4Y 211/16 [68] 127/64 [36] 17/16 [36] 31/32 [25] 3862L4Y 211/16 [68] 127/64 [36] 17/16 [36] 31/32 [25] 3802L64Y 211/16 [68] 127/64 [36] 17/16 [36] 31/32 [25] 3862L64Y 211/16 [68] 17/16 [36] 17/16 [36] 1 [25] FOR YOUR SAFETY IT IS SOLELY THE RESPONSIBILITY OF THE SYSTEM DESIGNER AND USER TO SELECT PRODUCTS SUITABLE FOR THEIR SPECIFIC APPLICATION REQUIREMENTS AND TO ENSURE PROPER INSTALLATION, OPERATION AND MAINTENANCE OF THESE PRODUCTS. MATERIAL COMPATIBILITY, PRODUCT RATINGS AND APPLICATION DETAILS SHOULD BE CONSIDERED IN THE SELECTION. IMPROPER SELECTION OR USE OF PRODUCTS DESCRIBED HEREIN CAN CAUSE PERSONAL INJURY OR PROPERTY DAMAGE. Formed Sampling Cylinders & Accessories 11

13 Formed Sampling Cylinders How to Collect Samples from Process Lines It is often difficult to obtain pure samples of process fluids for laboratory analysis. To insure accuracy and safety of your sample, DOT regulations, elimination of contaminates, cost and simplicity of operation must be considered. Here are four methods of collecting samples which we as manufacturers and suppliers of sampling cylinders and valves have seen successfully used. Method I Method II Method I: Water Displacement 1. Use a double-ended HOKE cylinder (either the LD or HD styles depending upon pressure requirements) with sufficient capacity and equip it with suitable HOKE valves. 2. Fill the cylinder with water so that all contaminates in the cylinder are removed by displacement. 3. Attach cylinder to process line and open process line stop valve. 4. Open both valves on sampling cylinder, the inlet valve wider than the outlet and allow the process fluid to displace the water in cylinder. 5. When cylinder is filled (this is indicated when process fluid begins flowing out cylinder outlet valve), close outlet valve and then both inlet and stop valves and remove cylinder from process line. 6. Transport cylinder to laboratory and bleed off samples as required. Method II: Evacuate Cylinder by Vacuum 1. Use either a double or single ended cylinder with valves, preferably packless type. Helium leak tested to insure leak tightness. 2. Evacuate the cylinder to remove contaminates. 3. Attach cylinder to process line. 4. Open inlet valve and draw off desired sample. 5. Close valve and remove cylinder from process line. 6. Draw samples from cylinder as required on mass spectrometer. Method III: In Line By-pass of Process Line 1. Establish by-pass line or parallel line to main process line with facilities to insert sampling cylinder. 2. Insert double-ended cylinder in by-pass line. 3. Open both inlet and outlet cylinder valves wide and allow process fluid to flow through by-pass line and cylinder. 4. Permit flow to continue running until accurate sample is established. 5. Close valves and remove cylinder from process line. 6. Draw sample from cylinder when required. Method III Method IV: Positive Displacement 1. Use a double-ended cylinder equipped with suitable valves. 2. Attach one end of the cylinder to the process line and the other to a positive displacement pump which draws uniformly over a period of time. 3. Open process line and cylinder valves and begin drawing off a uniform sample over an established period of time. 4. When time period is completed, close valves and remove cylinder from process line. 5. Sample gathered is an example of fluid passed through process line over a given period. Method IV 12 Formed Sampling Cylinders & Accessories

14 CIRCOR Instrumentation Technologies (CIT) is the logical choice for fluid control solutions. We provide the lowest cost of ownership, offering the best in class reliability and availability of our products. We have global coverage, delivering value in the form of local, flexible service to meet our customer s needs. CIT is a product group specializing in instrumentation with orifice sizes typically up to 2. PO Box 4866 Spartanburg, SC Tel Fax Sales-hoke@circor.com Our headquarters and ISO 9001:2008 certified manufacturing facilities are located at 405 Centura Court Spartanburg, SC, USA, Proudly Distributed By: 79008ENG 01/13 APS1224

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